WO1998013534A3 - Verfahren zur phosphatierung von stahlband - Google Patents
Verfahren zur phosphatierung von stahlband Download PDFInfo
- Publication number
- WO1998013534A3 WO1998013534A3 PCT/EP1997/005091 EP9705091W WO9813534A3 WO 1998013534 A3 WO1998013534 A3 WO 1998013534A3 EP 9705091 W EP9705091 W EP 9705091W WO 9813534 A3 WO9813534 A3 WO 9813534A3
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- phosphating
- steel band
- ions
- phosphating solution
- ranging
- Prior art date
Links
- 229910000831 Steel Inorganic materials 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 3
- 239000010959 steel Substances 0.000 title abstract 3
- 239000002253 acid Substances 0.000 abstract 3
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 abstract 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 abstract 1
- AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical compound ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 abstract 1
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 abstract 1
- 229910002651 NO3 Inorganic materials 0.000 abstract 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 abstract 1
- PTFCDOFLOPIGGS-UHFFFAOYSA-N Zinc dication Chemical compound [Zn+2] PTFCDOFLOPIGGS-UHFFFAOYSA-N 0.000 abstract 1
- 239000000956 alloy Substances 0.000 abstract 1
- 229910045601 alloy Inorganic materials 0.000 abstract 1
- 229910052802 copper Inorganic materials 0.000 abstract 1
- 239000010949 copper Substances 0.000 abstract 1
- 238000007598 dipping method Methods 0.000 abstract 1
- 229910052748 manganese Inorganic materials 0.000 abstract 1
- 239000011572 manganese Substances 0.000 abstract 1
- 229910001437 manganese ion Inorganic materials 0.000 abstract 1
- 229910052759 nickel Inorganic materials 0.000 abstract 1
- -1 nitrate ions Chemical class 0.000 abstract 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 abstract 1
- 238000005507 spraying Methods 0.000 abstract 1
- 239000011701 zinc Substances 0.000 abstract 1
- 229910052725 zinc Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
- C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
- C23C22/07—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing phosphates
- C23C22/08—Orthophosphates
- C23C22/18—Orthophosphates containing manganese cations
- C23C22/182—Orthophosphates containing manganese cations containing also zinc cations
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
- C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
- C23C22/07—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing phosphates
- C23C22/08—Orthophosphates
- C23C22/18—Orthophosphates containing manganese cations
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
- C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
- C23C22/07—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing phosphates
- C23C22/08—Orthophosphates
- C23C22/18—Orthophosphates containing manganese cations
- C23C22/182—Orthophosphates containing manganese cations containing also zinc cations
- C23C22/184—Orthophosphates containing manganese cations containing also zinc cations containing also nickel cations
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
- C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
- C23C22/34—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides
- C23C22/36—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates
- C23C22/364—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates containing also manganese cations
- C23C22/365—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates containing also manganese cations containing also zinc and nickel cations
Landscapes
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Chemical Treatment Of Metals (AREA)
- Laminated Bodies (AREA)
- Analysing Materials By The Use Of Radiation (AREA)
Abstract
Verfahren zum Phosphatieren von Stahlband oder von ein- oder beidseitig verzinktem oder legierungsverzinktem Stahlband durch Spritz- oder Tauchbehandlung für eine Zeitdauer im Bereich von 2 bis 15 Sekunden mit einer sauren, zink- und manganhaltigen Phosphatierlösung mit einer Temperatur im Bereich von 40 bis 70 °C, dadurch gekennzeichnet, daß die Phosphatierlösung 1 bis 4 g/l Zinkionen, 0,8 bis 3,5 g/l Manganionen, 10 bis 30 g/l Phosphationen, 0,1 bis 3 g/l Hydroxylamin in freier, ionischer oder gebundener Form und nicht mehr als 1 g/l Nitrationen enthält, einen Gehalt an freier Säure im Bereich von 0,4 bis 4 Punkten und einen Gehalt an Gesamtsäure im Bereich von 12 bis 50 Punkten aufweist. Fakultativ enthält die Phosphatierlösung 0,8 bis 3,5 g/l Nickel oder 0,002 bis 0,2 g/l Kupfer.
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP97942941A EP0931179B1 (de) | 1996-09-26 | 1997-09-17 | Verfahren zur phosphatierung von stahlband |
| DE59702741T DE59702741D1 (de) | 1996-09-26 | 1997-09-17 | Verfahren zur phosphatierung von stahlband |
| AU44593/97A AU4459397A (en) | 1996-09-26 | 1997-09-17 | Method for phosphating a steel band |
| AT97942941T ATE197969T1 (de) | 1996-09-26 | 1997-09-17 | Verfahren zur phosphatierung von stahlband |
| CA002266625A CA2266625A1 (en) | 1996-09-26 | 1997-09-17 | Method for phosphating a steel band |
| JP51522798A JP2001508123A (ja) | 1996-09-26 | 1997-09-17 | スチールバンドをホスフェート化するための方法 |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19639596A DE19639596A1 (de) | 1996-09-26 | 1996-09-26 | Verfahren zur Phosphatierung von Stahlband |
| DE19639596.8 | 1996-09-26 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| WO1998013534A2 WO1998013534A2 (de) | 1998-04-02 |
| WO1998013534A3 true WO1998013534A3 (de) | 1998-08-27 |
Family
ID=7806984
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PCT/EP1997/005091 WO1998013534A2 (de) | 1996-09-26 | 1997-09-17 | Verfahren zur phosphatierung von stahlband |
Country Status (11)
| Country | Link |
|---|---|
| EP (1) | EP0931179B1 (de) |
| JP (1) | JP2001508123A (de) |
| KR (1) | KR20000048509A (de) |
| CN (1) | CN1231706A (de) |
| AT (1) | ATE197969T1 (de) |
| AU (1) | AU4459397A (de) |
| CA (1) | CA2266625A1 (de) |
| DE (2) | DE19639596A1 (de) |
| ES (1) | ES2153217T3 (de) |
| ID (1) | ID21474A (de) |
| WO (1) | WO1998013534A2 (de) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6179934B1 (en) | 1997-01-24 | 2001-01-30 | Henkel Corporation | Aqueous phosphating composition and process for metal surfaces |
| JPH10204649A (ja) * | 1997-01-24 | 1998-08-04 | Nippon Parkerizing Co Ltd | 金属表面のりん酸塩処理水溶液及び処理方法 |
| DE19740953A1 (de) * | 1997-09-17 | 1999-03-18 | Henkel Kgaa | Verfahren zur Phosphatierung von Stahlband |
| DE19808755A1 (de) | 1998-03-02 | 1999-09-09 | Henkel Kgaa | Schichtgewichtsteuerung bei Bandphosphatierung |
| DE19905479A1 (de) * | 1999-02-10 | 2000-08-17 | Metallgesellschaft Ag | Verfahren zur Phospatisierung von Zink- oder Aluminiumoberflächen |
| DE10110834B4 (de) * | 2001-03-06 | 2005-03-10 | Chemetall Gmbh | Verfahren zur Beschichtung von metallischen Oberflächen und Verwendung der derart beschichteten Substrate |
| DE10110833B4 (de) * | 2001-03-06 | 2005-03-24 | Chemetall Gmbh | Verfahren zum Aufbringen eines Phosphatüberzuges und Verwendung der derart phosphatierten Metallteile |
| RU2225895C2 (ru) * | 2002-01-14 | 2004-03-20 | Закрытое акционерное общество "ФК" | Способ нанесения фосфатирующего состава |
| CN104313579B (zh) * | 2014-11-11 | 2017-01-18 | 武汉钢铁(集团)公司 | 一种电镀锌镁合金钢板的生产方法 |
| CN105568274A (zh) * | 2015-12-31 | 2016-05-11 | 安徽红桥金属制造有限公司 | 一种环保的镀锌钝化剂及其制备方法 |
| CN105925985B (zh) * | 2016-07-19 | 2018-04-20 | 东莞市凯盟表面处理技术开发有限公司 | 一种不锈铁常温化学抛光液及其制备方法和使用方法 |
| CN111349867A (zh) * | 2020-04-10 | 2020-06-30 | 武汉钢铁有限公司 | 一种涂装友好的预磷化电镀锌汽车外板及其制备方法 |
| CN112226755B (zh) * | 2020-09-23 | 2023-06-23 | 山东大业股份有限公司 | 一种金属线材表面处理用磷化方法及装置 |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1994013856A1 (de) * | 1992-12-07 | 1994-06-23 | Henkel Kommanditgesellschaft Auf Aktien | Verfahren zur phosphatierung von metalloberflächen |
| WO1995007370A1 (de) * | 1993-09-06 | 1995-03-16 | Henkel Kommanditgesellschaft Auf Aktien | Nickelfreies phosphatierverfahren |
| US5516372A (en) * | 1992-08-27 | 1996-05-14 | Henkel Kommanditgesellschaft Auf Aktien | Process for phosphating steel strip galvanized on one side |
| WO1997030189A1 (de) * | 1996-02-19 | 1997-08-21 | Henkel Kommanditgesellschaft Auf Aktien | Zinkphosphatierung mit geringen gehalten an nickel und/oder cobalt |
-
1996
- 1996-09-26 DE DE19639596A patent/DE19639596A1/de not_active Withdrawn
-
1997
- 1997-09-17 KR KR1019990702409A patent/KR20000048509A/ko not_active Withdrawn
- 1997-09-17 CA CA002266625A patent/CA2266625A1/en not_active Abandoned
- 1997-09-17 JP JP51522798A patent/JP2001508123A/ja active Pending
- 1997-09-17 AT AT97942941T patent/ATE197969T1/de not_active IP Right Cessation
- 1997-09-17 ES ES97942941T patent/ES2153217T3/es not_active Expired - Lifetime
- 1997-09-17 WO PCT/EP1997/005091 patent/WO1998013534A2/de not_active Application Discontinuation
- 1997-09-17 ID IDW990112A patent/ID21474A/id unknown
- 1997-09-17 AU AU44593/97A patent/AU4459397A/en not_active Abandoned
- 1997-09-17 DE DE59702741T patent/DE59702741D1/de not_active Expired - Fee Related
- 1997-09-17 CN CN97198236A patent/CN1231706A/zh active Pending
- 1997-09-17 EP EP97942941A patent/EP0931179B1/de not_active Expired - Lifetime
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5516372A (en) * | 1992-08-27 | 1996-05-14 | Henkel Kommanditgesellschaft Auf Aktien | Process for phosphating steel strip galvanized on one side |
| WO1994013856A1 (de) * | 1992-12-07 | 1994-06-23 | Henkel Kommanditgesellschaft Auf Aktien | Verfahren zur phosphatierung von metalloberflächen |
| WO1995007370A1 (de) * | 1993-09-06 | 1995-03-16 | Henkel Kommanditgesellschaft Auf Aktien | Nickelfreies phosphatierverfahren |
| WO1997030189A1 (de) * | 1996-02-19 | 1997-08-21 | Henkel Kommanditgesellschaft Auf Aktien | Zinkphosphatierung mit geringen gehalten an nickel und/oder cobalt |
Also Published As
| Publication number | Publication date |
|---|---|
| KR20000048509A (ko) | 2000-07-25 |
| WO1998013534A2 (de) | 1998-04-02 |
| EP0931179B1 (de) | 2000-12-06 |
| JP2001508123A (ja) | 2001-06-19 |
| ES2153217T3 (es) | 2001-02-16 |
| CA2266625A1 (en) | 1998-04-02 |
| AU4459397A (en) | 1998-04-17 |
| ATE197969T1 (de) | 2000-12-15 |
| CN1231706A (zh) | 1999-10-13 |
| ID21474A (id) | 1999-06-17 |
| DE19639596A1 (de) | 1998-04-02 |
| DE59702741D1 (de) | 2001-01-11 |
| EP0931179A2 (de) | 1999-07-28 |
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