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WO1998013534A3 - Procede pour la phosphatation d'un feuillard d'acier - Google Patents

Procede pour la phosphatation d'un feuillard d'acier Download PDF

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Publication number
WO1998013534A3
WO1998013534A3 PCT/EP1997/005091 EP9705091W WO9813534A3 WO 1998013534 A3 WO1998013534 A3 WO 1998013534A3 EP 9705091 W EP9705091 W EP 9705091W WO 9813534 A3 WO9813534 A3 WO 9813534A3
Authority
WO
WIPO (PCT)
Prior art keywords
phosphating
steel band
ions
phosphating solution
ranging
Prior art date
Application number
PCT/EP1997/005091
Other languages
German (de)
English (en)
Other versions
WO1998013534A2 (fr
Inventor
Joerg Riesop
Reinhard Seidel
Original Assignee
Henkel Kgaa
Joerg Riesop
Reinhard Seidel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Henkel Kgaa, Joerg Riesop, Reinhard Seidel filed Critical Henkel Kgaa
Priority to JP51522798A priority Critical patent/JP2001508123A/ja
Priority to DE59702741T priority patent/DE59702741D1/de
Priority to CA002266625A priority patent/CA2266625A1/fr
Priority to EP97942941A priority patent/EP0931179B1/fr
Priority to AU44593/97A priority patent/AU4459397A/en
Priority to AT97942941T priority patent/ATE197969T1/de
Publication of WO1998013534A2 publication Critical patent/WO1998013534A2/fr
Publication of WO1998013534A3 publication Critical patent/WO1998013534A3/fr

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/07—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing phosphates
    • C23C22/08—Orthophosphates
    • C23C22/18—Orthophosphates containing manganese cations
    • C23C22/182—Orthophosphates containing manganese cations containing also zinc cations
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/07—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing phosphates
    • C23C22/08—Orthophosphates
    • C23C22/18—Orthophosphates containing manganese cations
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/07—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing phosphates
    • C23C22/08—Orthophosphates
    • C23C22/18—Orthophosphates containing manganese cations
    • C23C22/182—Orthophosphates containing manganese cations containing also zinc cations
    • C23C22/184—Orthophosphates containing manganese cations containing also zinc cations containing also nickel cations
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/34—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides
    • C23C22/36—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates
    • C23C22/364—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates containing also manganese cations
    • C23C22/365—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates containing also manganese cations containing also zinc and nickel cations

Landscapes

  • Chemical & Material Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Chemical Treatment Of Metals (AREA)
  • Laminated Bodies (AREA)
  • Analysing Materials By The Use Of Radiation (AREA)

Abstract

L'invention concerne un procédé pour la phosphatation d'un feuillard d'acier ou d'un feuillard d'acier galvanisé ou pourvu d'un dépôt d'alliage sur une face ou sur ces deux faces, consistant à traiter par pulvérisation ou par immersion, pendant 2 à 15 secondes, au moyen d'une solution de phosphatage acide contenant du zinc et du manganèse, présentant une température comprise entre 40 et 70 °C, ledit procédé se caractérisant en ce que la solution de phosphatage contient 1 à 4 g/l d'ions zinc, 0,8 à 3,5 g/l d'ions manganèse, 10 à 30 g/l d'ions phosphate, 0,1 à 3 g/l d'hydroxylamine sous forme libre, ionique ou liée, et au maximum 1 g/l d'ions nitrate, et présente une teneur en acide libre comprise entre 0,4 et 4 points et une teneur totale en acide comprise entre 12 et 50 points. Ladite solution de phosphatation peut éventuellement contenir 0,8 à 3,5 g/l de nickel ou 0,002 à 0,2 g/l de cuivre.
PCT/EP1997/005091 1996-09-26 1997-09-17 Procede pour la phosphatation d'un feuillard d'acier WO1998013534A2 (fr)

Priority Applications (6)

Application Number Priority Date Filing Date Title
JP51522798A JP2001508123A (ja) 1996-09-26 1997-09-17 スチールバンドをホスフェート化するための方法
DE59702741T DE59702741D1 (de) 1996-09-26 1997-09-17 Verfahren zur phosphatierung von stahlband
CA002266625A CA2266625A1 (fr) 1996-09-26 1997-09-17 Procede pour la phosphatation d'un feuillard d'acier
EP97942941A EP0931179B1 (fr) 1996-09-26 1997-09-17 Procede pour la phosphatation d'un feuillard d'acier
AU44593/97A AU4459397A (en) 1996-09-26 1997-09-17 Method for phosphating a steel band
AT97942941T ATE197969T1 (de) 1996-09-26 1997-09-17 Verfahren zur phosphatierung von stahlband

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19639596A DE19639596A1 (de) 1996-09-26 1996-09-26 Verfahren zur Phosphatierung von Stahlband
DE19639596.8 1996-09-26

Publications (2)

Publication Number Publication Date
WO1998013534A2 WO1998013534A2 (fr) 1998-04-02
WO1998013534A3 true WO1998013534A3 (fr) 1998-08-27

Family

ID=7806984

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP1997/005091 WO1998013534A2 (fr) 1996-09-26 1997-09-17 Procede pour la phosphatation d'un feuillard d'acier

Country Status (11)

Country Link
EP (1) EP0931179B1 (fr)
JP (1) JP2001508123A (fr)
KR (1) KR20000048509A (fr)
CN (1) CN1231706A (fr)
AT (1) ATE197969T1 (fr)
AU (1) AU4459397A (fr)
CA (1) CA2266625A1 (fr)
DE (2) DE19639596A1 (fr)
ES (1) ES2153217T3 (fr)
ID (1) ID21474A (fr)
WO (1) WO1998013534A2 (fr)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6179934B1 (en) 1997-01-24 2001-01-30 Henkel Corporation Aqueous phosphating composition and process for metal surfaces
JPH10204649A (ja) * 1997-01-24 1998-08-04 Nippon Parkerizing Co Ltd 金属表面のりん酸塩処理水溶液及び処理方法
DE19740953A1 (de) * 1997-09-17 1999-03-18 Henkel Kgaa Verfahren zur Phosphatierung von Stahlband
DE19808755A1 (de) 1998-03-02 1999-09-09 Henkel Kgaa Schichtgewichtsteuerung bei Bandphosphatierung
DE19905479A1 (de) * 1999-02-10 2000-08-17 Metallgesellschaft Ag Verfahren zur Phospatisierung von Zink- oder Aluminiumoberflächen
DE10110833B4 (de) * 2001-03-06 2005-03-24 Chemetall Gmbh Verfahren zum Aufbringen eines Phosphatüberzuges und Verwendung der derart phosphatierten Metallteile
DE10110834B4 (de) * 2001-03-06 2005-03-10 Chemetall Gmbh Verfahren zur Beschichtung von metallischen Oberflächen und Verwendung der derart beschichteten Substrate
RU2225895C2 (ru) * 2002-01-14 2004-03-20 Закрытое акционерное общество "ФК" Способ нанесения фосфатирующего состава
CN104313579B (zh) * 2014-11-11 2017-01-18 武汉钢铁(集团)公司 一种电镀锌镁合金钢板的生产方法
CN105568274A (zh) * 2015-12-31 2016-05-11 安徽红桥金属制造有限公司 一种环保的镀锌钝化剂及其制备方法
CN105925985B (zh) * 2016-07-19 2018-04-20 东莞市凯盟表面处理技术开发有限公司 一种不锈铁常温化学抛光液及其制备方法和使用方法
CN111349867A (zh) * 2020-04-10 2020-06-30 武汉钢铁有限公司 一种涂装友好的预磷化电镀锌汽车外板及其制备方法
CN112226755B (zh) * 2020-09-23 2023-06-23 山东大业股份有限公司 一种金属线材表面处理用磷化方法及装置

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1994013856A1 (fr) * 1992-12-07 1994-06-23 Henkel Kommanditgesellschaft Auf Aktien Procede de phosphatation de surfaces metalliques
WO1995007370A1 (fr) * 1993-09-06 1995-03-16 Henkel Kommanditgesellschaft Auf Aktien Procedes de phosphatage sans nickel
US5516372A (en) * 1992-08-27 1996-05-14 Henkel Kommanditgesellschaft Auf Aktien Process for phosphating steel strip galvanized on one side
WO1997030189A1 (fr) * 1996-02-19 1997-08-21 Henkel Kommanditgesellschaft Auf Aktien Procede de phosphatisation au zinc a l'aide de faibles teneurs en nickel et/ou en cobalt

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5516372A (en) * 1992-08-27 1996-05-14 Henkel Kommanditgesellschaft Auf Aktien Process for phosphating steel strip galvanized on one side
WO1994013856A1 (fr) * 1992-12-07 1994-06-23 Henkel Kommanditgesellschaft Auf Aktien Procede de phosphatation de surfaces metalliques
WO1995007370A1 (fr) * 1993-09-06 1995-03-16 Henkel Kommanditgesellschaft Auf Aktien Procedes de phosphatage sans nickel
WO1997030189A1 (fr) * 1996-02-19 1997-08-21 Henkel Kommanditgesellschaft Auf Aktien Procede de phosphatisation au zinc a l'aide de faibles teneurs en nickel et/ou en cobalt

Also Published As

Publication number Publication date
AU4459397A (en) 1998-04-17
ID21474A (id) 1999-06-17
CN1231706A (zh) 1999-10-13
JP2001508123A (ja) 2001-06-19
ATE197969T1 (de) 2000-12-15
CA2266625A1 (fr) 1998-04-02
DE19639596A1 (de) 1998-04-02
DE59702741D1 (de) 2001-01-11
KR20000048509A (ko) 2000-07-25
EP0931179B1 (fr) 2000-12-06
ES2153217T3 (es) 2001-02-16
EP0931179A2 (fr) 1999-07-28
WO1998013534A2 (fr) 1998-04-02

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