WO2008136058A1 - レーザ脱離イオン化用サンプルプレート及び該サンプルプレートを用いた質量分析装置 - Google Patents
レーザ脱離イオン化用サンプルプレート及び該サンプルプレートを用いた質量分析装置 Download PDFInfo
- Publication number
- WO2008136058A1 WO2008136058A1 PCT/JP2007/000456 JP2007000456W WO2008136058A1 WO 2008136058 A1 WO2008136058 A1 WO 2008136058A1 JP 2007000456 W JP2007000456 W JP 2007000456W WO 2008136058 A1 WO2008136058 A1 WO 2008136058A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- sample plate
- layer
- laser desorption
- pores
- desorption ionization
- Prior art date
Links
- 238000001698 laser desorption ionisation Methods 0.000 title abstract 2
- 239000011148 porous material Substances 0.000 abstract 3
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 abstract 2
- 229910052593 corundum Inorganic materials 0.000 abstract 2
- 239000002184 metal Substances 0.000 abstract 2
- 229910052751 metal Inorganic materials 0.000 abstract 2
- 229910001845 yogo sapphire Inorganic materials 0.000 abstract 2
- 238000007743 anodising Methods 0.000 abstract 1
- 238000009413 insulation Methods 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 150000002739 metals Chemical class 0.000 abstract 1
- 239000010409 thin film Substances 0.000 abstract 1
Classifications
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J49/00—Particle spectrometers or separator tubes
- H01J49/02—Details
- H01J49/04—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components
- H01J49/0409—Sample holders or containers
- H01J49/0418—Sample holders or containers for laser desorption, e.g. matrix-assisted laser desorption/ionisation [MALDI] plates or surface enhanced laser desorption/ionisation [SELDI] plates
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N35/00—Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor
- G01N35/02—Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor using a plurality of sample containers moved by a conveyor system past one or more treatment or analysis stations
- G01N35/028—Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor using a plurality of sample containers moved by a conveyor system past one or more treatment or analysis stations having reaction cells in the form of microtitration plates
Landscapes
- Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Electron Tubes For Measurement (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
Abstract
Al板である基体(21)の上に断熱層として径が20~30nm程度の細孔(23)を多数有するAl2O3層(22)を形成し、その表面にTi層(24a)とPt層(24b)とから成る2層金属薄膜(24)を形成することにより、レーザ脱離イオン化のためのサンプルプレート(20)を得る。Ti/Ptの異種金属の組み合わせは高いH+付加触媒能を発揮するため、従来のように大きな径の細孔(23)を設けなくても高いイオン化効率を得ることができる。これにより、Al2O3層(22)を形成する際のアノーダイジング処理の時間は短くて済み、径の大きな細孔(23)を形成するための特殊な処理も不要である。それにより、製造が容易であってコストを抑制することができる。
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PCT/JP2007/000456 WO2008136058A1 (ja) | 2007-04-25 | 2007-04-25 | レーザ脱離イオン化用サンプルプレート及び該サンプルプレートを用いた質量分析装置 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PCT/JP2007/000456 WO2008136058A1 (ja) | 2007-04-25 | 2007-04-25 | レーザ脱離イオン化用サンプルプレート及び該サンプルプレートを用いた質量分析装置 |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2008136058A1 true WO2008136058A1 (ja) | 2008-11-13 |
Family
ID=39943183
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/JP2007/000456 WO2008136058A1 (ja) | 2007-04-25 | 2007-04-25 | レーザ脱離イオン化用サンプルプレート及び該サンプルプレートを用いた質量分析装置 |
Country Status (1)
Country | Link |
---|---|
WO (1) | WO2008136058A1 (ja) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109585254A (zh) * | 2018-11-15 | 2019-04-05 | 复旦大学 | 一种基质辅助激光解析质谱大批量上样装置 |
EP3474310A1 (en) | 2017-10-18 | 2019-04-24 | Shimadzu Corporation | Information management device for mass spectrometer |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2003536073A (ja) * | 2000-06-05 | 2003-12-02 | カイロン コーポレイション | プロテオミクス分析を実施するためのマイクロアレイ |
WO2006046697A1 (ja) * | 2004-10-29 | 2006-05-04 | Japan Science And Technology Agency | Maldi-tof ms用基板及びそれを用いた質量分析方法 |
-
2007
- 2007-04-25 WO PCT/JP2007/000456 patent/WO2008136058A1/ja active Application Filing
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2003536073A (ja) * | 2000-06-05 | 2003-12-02 | カイロン コーポレイション | プロテオミクス分析を実施するためのマイクロアレイ |
WO2006046697A1 (ja) * | 2004-10-29 | 2006-05-04 | Japan Science And Technology Agency | Maldi-tof ms用基板及びそれを用いた質量分析方法 |
Non-Patent Citations (1)
Title |
---|
SHOJI OKUNO: "Requirements for Laser-Induced Desortion/Ionization on Submicrometer Structures", ANALYTICAL CHEMISTRY, vol. 77, no. 16, 2005, pages 5364 - 5369, XP003012113 * |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP3474310A1 (en) | 2017-10-18 | 2019-04-24 | Shimadzu Corporation | Information management device for mass spectrometer |
US12176197B2 (en) | 2017-10-18 | 2024-12-24 | Shimadzu Corporation | Information management device for mass spectrometer |
CN109585254A (zh) * | 2018-11-15 | 2019-04-05 | 复旦大学 | 一种基质辅助激光解析质谱大批量上样装置 |
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