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WO1999026553A1 - Procede de formation d'ouvrages de restauration dentaire a partir de composites condensables - Google Patents

Procede de formation d'ouvrages de restauration dentaire a partir de composites condensables Download PDF

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Publication number
WO1999026553A1
WO1999026553A1 PCT/US1998/024864 US9824864W WO9926553A1 WO 1999026553 A1 WO1999026553 A1 WO 1999026553A1 US 9824864 W US9824864 W US 9824864W WO 9926553 A1 WO9926553 A1 WO 9926553A1
Authority
WO
WIPO (PCT)
Prior art keywords
composite
condensable
kit
amalgam
flowable
Prior art date
Application number
PCT/US1998/024864
Other languages
English (en)
Inventor
Bruce Alpert
Original Assignee
Jeneric Pentron Incorporated
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US09/023,643 external-priority patent/US5997302A/en
Application filed by Jeneric Pentron Incorporated filed Critical Jeneric Pentron Incorporated
Priority to AU15954/99A priority Critical patent/AU1595499A/en
Priority to EP98960336A priority patent/EP1033944A1/fr
Publication of WO1999026553A1 publication Critical patent/WO1999026553A1/fr

Links

Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61C—DENTISTRY; APPARATUS OR METHODS FOR ORAL OR DENTAL HYGIENE
    • A61C19/00—Dental auxiliary appliances
    • A61C19/005—Devices for the manual mixing of small quantities of materials, e.g. trays for mixing dental porcelain
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61C—DENTISTRY; APPARATUS OR METHODS FOR ORAL OR DENTAL HYGIENE
    • A61C3/00—Dental tools or instruments
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61C—DENTISTRY; APPARATUS OR METHODS FOR ORAL OR DENTAL HYGIENE
    • A61C5/00—Filling or capping teeth
    • A61C5/30—Securing inlays, onlays or crowns
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61C—DENTISTRY; APPARATUS OR METHODS FOR ORAL OR DENTAL HYGIENE
    • A61C5/00—Filling or capping teeth
    • A61C5/60—Devices specially adapted for pressing or mixing capping or filling materials, e.g. amalgam presses
    • A61C5/62—Applicators, e.g. syringes or guns
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61C—DENTISTRY; APPARATUS OR METHODS FOR ORAL OR DENTAL HYGIENE
    • A61C2202/00—Packaging for dental appliances

Definitions

  • This invention relates to dental restorations.
  • this invention relates to a method and kit for the formation of dental restorations from condensable composites that have the feel of an amalgam.
  • Dental restorative materials include materials used to repair damaged teeth or to replace missing teeth. Conventionally, teeth are treated for decay by removing the decayed material grinding, and then replacing the decayed tooth portion with a dental restorative material.
  • One commonly-used restorative material is an alloy of silver mixed with mercury, often referred to as dental amalgam.
  • amalgam Dentists and dental technicians have become accustomed to working with amalgam, which allows the dentist or dental technician to restructure and reshape the tooth surface by packing and molding the amalgam material.
  • the characteristic of amalgam that allows such packing and molding is referred to as condensability.
  • the condensability of amalgam is largely related to the ability of such material to respond to force applied in directions other than the direction of the applied force. This permits the application of a downward pressure of a dental tool to cause such material to respond laterally and conform to a lateral mold.
  • mercury is forced from the amalgam and removed by mopping such that the mercury content of the amalgam content is actually reduced.
  • Dentists have accordingly looked for alternatives to amalgam, and in recent years a variety of filled polymeric materials have become available which are often referred to as composites.
  • Dental composites are compatible with enamel and dentine, may be colored to match the surrounding dentition, and posses high durability.
  • Dental composites most commonly comprise reinforcing inorganic fillers in the form of particulates, bound together by a polymeric matrix.
  • the polymeric matrix may be comprised of an acrylic or epoxy resin or other types of carbon-based polymers.
  • polymeric materials (resins) suitable for use as dental composites are set forth in U.S. Pat. Nos. 3,066,112, U.S. Pat. No. 3,179,623, and U.S. Patent. No. 4,744,759 to Bowen, all of which are herein incorporated by reference.
  • Fillers for dental composites include finely divided solids such as silica, glass, zirconium, aluminum oxide, crystalline quartz, glass beads, or mixtures of glass beads and quartz. Filler strength, content, shape, and size determine the physical and mechanical properties of the restoration material.
  • composites comprising particulate fillers occasionally have some shortcomings when used as posterior restoration materials.
  • a composite acceptable for posterior use must achieve a high filler loading in the polymeric matrix, and meet certain physical and mechanical properties. Some do not possess the wear resistance of conventional amalgams.
  • Particulate-based composites also suffer from the disadvantage of the lack of the condensability found in conventional amalgams, and thus are not amenable to use with the techniques developed in connection with amalgams.
  • a new class of condensable composites has therefore been developed, comprising a polymeric matrix and various alternative forms of inorganic filler. Ehrnford in U.S. Pat. Nos.
  • a composite having the feel and workability of amalgams may be made using densified, embrittled fibers.
  • This material is commercially available under the trademark ALERT from Jeneric/Pentron, Inc., Wallingford, CT.
  • ALERT from Jeneric/Pentron, Inc., Wallingford, CT.
  • a prepared tooth cavity is preferably etched; optionally treated with a primer/adhesive and then cured; optionally treated with a flowable composite and then cured; and then filled with a condensable composite, using techniques and instruments developed for use with amalgams.
  • Such techniques include transferring the composite with an amalgam carrier, and shaping and packing the composite with an amalgam plugger.
  • the amalgam carrier is preferable made of a high-impact plastic rather than metal.
  • the dental restoration may optionally be further etched and sealed.
  • the kit of the present invention comprises at least a condensable composite and a high-impact plastic amalgam carrier.
  • the condensable composite is further provided in premeasured amounts, that is, in amounts of one spill, two spills, or three spills.
  • the kit further comprises a flowable composite material
  • the kit further comprises a flowable composite material and dispenser, an etchant, a primer/adhesive, a plugger, and brush tips.
  • the kit is especially useful in forming posterior dental restorations that are aesthetic, strongly-bonded, and wear-resistant. The restorations have negligible shrinkage upon polymerization.
  • FIGURE 1 is a plan view of an amalgam carrier suitable for use in the present invention.
  • FIGURE 2 is a plan view of an amalgam plugger suitable for use in the present invention.
  • FIGURE 3 is a plan view of a container for use in the present invention, comprising a plurality of tabs suitable for use with condensable composite.
  • FIGURE 4 is a side view of a container for use with the present invention, comprising a plurality of tabs suitable for use with condensable composite.
  • the method according to the present invention is useful for making dental restorations such as fillings, facings, artificial teeth and the like.
  • the method is characterized by use of a condensable dental composite.
  • condensable and condensability refer to the characteristic wherein the feel and workability of the composite is similar to that of amalgam, and thus amenable to application using clinical techniques similar to, or the same as, those developed for use with amalgam.
  • Non- condensable composites are those known in the art which are to some extent thixotropic or flowable, and applied using a syringe or compule.
  • Condensable composites are those which are not thixotropic and which do not flow, and which are applied using an amalgam carrier and amalgam plugger.
  • a prepared tooth cavity is etched; optionally treated with a primer/adhesive which is usually then cured; optionally treated with a flowable composite which is usually then cured; and then filled with a condensable composite, using techniques and instruments developed for use with amalgams.
  • Such techniques include transferring the composite with an amalgam carrier, and shaping and packing the composite with an amalgam plugger.
  • the amalgam carrier is preferably made of a high-impact plastic rather than metal.
  • the dental restoration may optionally be further etched and sealed. Such dental restorations possess mechanical, physical and aesthetic properties which closely conform to the natural tooth structure. In addition, such restorations have negligible shrinkage upon polymerization.
  • tooth cavities e.g., for posterior fillings
  • Carbide friction-grip burs and cavo surface beveling i.e., Class V are recommended in order to increase retention by greater enamel surface etching, and to minimize marginal leakage and ultimately improve marginal adaptability. It is further recommended that if a metal band is used, the inside of the metal band be lubricated using either wax or cavity varnish in order to prevent adhesion of the bonding materials to the band.
  • Acid etching of the enamel can be effected by applying an aqueous orthophosphoric acid solution or gel containing about 10-40%, preferably 37% by weight of orthophosphoric acid.
  • the solution is applied to the enamel surface with a brush or small cotton pellet for about twenty seconds.
  • the area should be washed well with water, and excess water should be removed either by blotting or by treating with a stream of air for about two seconds.
  • the tooth surface should be left moist, as dry surfaces may result in poor bond strength and post-operative sensitivity.
  • the enamel should, if possible, be conditioned at least one millimeter beyond the margin of the cavity preparation.
  • the etched area should be at least as wide as the tooth structure being replaced, but not less than two millimeters.
  • a thin layer of a primer, primer/adhesive, or adhesive is then applied to the tooth cavity.
  • Primers, primer/adhesives, and adhesives and methods of application therefor are well-known in the art.
  • a particularly suitable primer/adhesive is available under the trademark BOND-1 from Jeneric/Pentron, Inc., Wallingford, CT.
  • BOND-1 is an unfilled methacrylate-based primer/adhesive that provides strong bonds of up to about 31.0 Mpa, while also reducing tooth sensitivity.
  • the bonding agent is preferably applied as two consecutive coats applied within ten seconds of each other, treated with air to remove solvent, and then polymerized by exposure to the visible light source for about 10 seconds, or until cure is substantially complete.
  • An adhesive available under the trademark BOND-IT, available from Jeneric/Pentron, Inc., Wallingford, CT is also useful in the practice of the present invention.
  • a thin (0.5 to 1.0 mm) layer of a flowable dental composite material is then placed in the cavity by means known in the art, for example, a syringe or compule.
  • a low-viscosity flowable resin is used in order to ensure that all surfaces of the cavity are wetted, and to provide microscopic adaptation of the condensable composite to the tooth cavity.
  • a suitable low viscosity flowable composite resin is available under the trademark FLOW-IT from Jeneric/Pentron, Inc., Wallingford, CT.
  • the flowable composite is then light cured for about 40 seconds, or until cure is substantially complete. Condensable composite resin is then placed and packed into the cavity using mechanical transfer and packing techniques.
  • the foregoing description is presently the preferred method of forming a dental restoration using a condensable composite
  • various of the above-described steps may be omitted, or other steps known in the art may be added to the procedure.
  • other cavity preparation steps may be added, or the acid etch step may omitted.
  • the prepared cavity is acid etched; treated with a primer/adhesive or adhesive; and then the condensable composite is applied directly without use of the flowable composite.
  • the prepared cavity is acid etched; treated with a flowable composite; and then the condensable composite is applied.
  • the condensable composite is first placed into the cavity using an amalgam carrier 10 as shown in FIG. 1.
  • the amalgam carrier is not metal or metal- surfaced, but rather a high-impact plastic or other material which will not result in discoloration of the composite.
  • the carrier must be high-strength, that is, capable of withstanding the forces placed on the carrier by the dentist or technician while in use.
  • Composite is loaded into hollow tip 12 of carrier 10 by pressing tip 12 directly into the composite without dragging or sliding tip 12 over the surface of the composite.
  • the composite is ejected into the cavity by pressing plunger 14.
  • the composite is then packed into the cavity using, e.g., the amalgam packer 22 and carver 24 shown generally as plugger 20 in FIG. 2.
  • Suitable amalgam pluggers are known in the art, and available in a variety of forms.
  • the application of force to the condensable composite in the presence of the flowable composite during packing results in microscopic adaptation of the filling to the tooth cavity, and thus enhanced bonding in the final restoration.
  • occlusal form is created by pushing the carver portion 24 of amalgam plugger 20.
  • the restoration is cured by suitable means.
  • a preferred condensable composite for use in the present method is available under the trademark ALERT from Jeneric/Pentron, Inc, Wallingford, CT. Complete cure of ALERT by visible light to a 5 mm depth is achieved within about 40 seconds. Interproximal areas may be cured for an additional twenty seconds each. Where the preparation exceeds a depth of about 5.0 mm, an initial increment of condensable composite is placed, packed and light cured. A coat of a primer, primer/adhesive, or adhesive is then applied to the cured restoration, air dried as before, and light cured. A final increment of condensable composite is then placed and packed into the cavity, occlusal form is created, and the restoration cured.
  • the restoration is polished using conventional polishing materials and techniques, such as disks, composite polishing pastes, and polish-impregnated wheels and cups, and the like.
  • the surface of the restoration may be sealed to increase wear resistance and ensure the marginal integrity of the restoration.
  • a suitable sealant is available under the trademark PROTECT-IT from Jeneric/Pentron, Inc., Wallingford, CT. Application of this sealant requires first etching with an etchant such as phosphoric acid out to about 2 mm of enamel adjacent the restoration margin for about twenty seconds. The etchant is then removed by thorough washing. Sealant is then applied over the entire restoration surface, thinned using a jet of air, and cured. Subsequent polishing is usually not necessary.
  • the kit of the present invention comprises at least a condensable composite and a nonmetal-surfaced amalgam carrier such as that shown in FIG. 1.
  • Amalgam carriers are well-known in the art, and other types of amalgam carrier may be suitable for use in the practice of the present invention.
  • use of metal or metal-surfaced carriers may result in discoloration of the condensable composite, and so their use is preferably avoided.
  • the condensable composite is preferably provided in premeasured amounts similarly to amalgam, that is, in amounts of one spill, two spills, or three spills.
  • a container suitable for providing the premeasured amounts of condensable composite is shown in FIGS. 3 and 4.
  • Container 30 generally comprises a plurality of tabs 32, 34, 36, 38, 40, 42 each tab having a holder portion 44 and a depression portion 46.
  • Holder portion 44 optionally has an essentially square ridge portion 48 to aid the user in gripping and holding the tab, as illustrated in FIGS. 3 and 4.
  • This optional ridge portion 48 may take the form of any shape to provide increased gripping capability.
  • Depression portion 46 is sized so as to contain one spill, two spills, or three spills of condensable composite.
  • Each tab 32, 34, 36, 38, 40, 42 is preferably detachably adhered to at least one additional tab, such that the tab is conveniently removed by the dentist or technician upon use. As shown in FIG. 3, for example, tab 32 is detachably adhered to tab 34 by score 50 extending longitudinally between tabs 32, 34.
  • Each tab 32, 34, 36, 38, 40, 42 further comprises a removable cover made of foil or other flexible material to protect the composite during shipping and storage (not shown).
  • the kit further comprises a flowable composite material
  • the kit further comprises a flowable composite material and dispenser such as a syringe or compule, and at least one or all of an etchant, a primer/adhesive, a sealant, an amalgam plugger/carver, and brush tips.
  • a flowable composite material and dispenser such as a syringe or compule, and at least one or all of an etchant, a primer/adhesive, a sealant, an amalgam plugger/carver, and brush tips.
  • the elements of the kit are used as described above in connection with the method of the present invention.
  • the kit is especially useful in forming posterior dental restorations that are aesthetic, strongly-bonded, and wear-resistant. While preferred embodiments have been shown and described, various modifications and substitutions may be made thereto without departing from the spirit and scope of the invention. Accordingly, it is to be understood that the present invention has been described by way of illustrations and not limitation. What is claimed is:

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  • Health & Medical Sciences (AREA)
  • Oral & Maxillofacial Surgery (AREA)
  • Dentistry (AREA)
  • Epidemiology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Dental Tools And Instruments Or Auxiliary Dental Instruments (AREA)

Abstract

Procédé et kit. Le procédé consiste: à mordancer une cavité dentaire; à la traiter au moyen d'un décapant/adhésif que l'on photopolymérise; à la traiter au moyen d'un composite coulant que l'on photopolymérise; à la remplir d'un composite condensable, à l'aide de techniques et d'instruments conçus pour être utilisés conjointement avec des amalgames. Lesdites techniques consistent à transférer le composite à l'aide d'un porte-amalgame, à le façonner et à le tasser à l'aide d'un fouloir à amalgame. L'ouvrage de restauration dentaire peut éventuellement être encore mordancé et scellé. Ledit kit comprend au moins un composite condensable et un porte-amalgame. Le composite condensable est ensuite produit en doses prémesurées, c'est-à-dire, à raison d'une, deux ou trois décharges. Dans un autre mode de réalisation, le kit comprend également un matériau composite coulant, et dans encore un autre mode de réalisation, il comprend un matériau composite coulant et un distributeur, un mordanceur, un décapant/adhésif, un fouloir et des embouts à brosse. Ledit kit est particulièrement utile dans la formation d'ouvrages de restauration dentaire postérieurs qui sont esthétiques, bien scellés et résistent à l'usure. Lesdits ouvrages de restauration font preuve d'un retrait négligeable lors de la polymérisation.
PCT/US1998/024864 1997-11-26 1998-11-23 Procede de formation d'ouvrages de restauration dentaire a partir de composites condensables WO1999026553A1 (fr)

Priority Applications (2)

Application Number Priority Date Filing Date Title
AU15954/99A AU1595499A (en) 1997-11-26 1998-11-23 Method for the formation of dental restorations from condensable composites
EP98960336A EP1033944A1 (fr) 1997-11-26 1998-11-23 Procede de formation d'ouvrages de restauration dentaire a partir de composites condensables

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US6679997P 1997-11-26 1997-11-26
US60/066,799 1997-11-26
US09/023,643 US5997302A (en) 1997-11-26 1998-02-13 Method for the formation of dental restorations from condensable composites
US09/023,643 1998-02-13

Publications (1)

Publication Number Publication Date
WO1999026553A1 true WO1999026553A1 (fr) 1999-06-03

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AU (1) AU1595499A (fr)
WO (1) WO1999026553A1 (fr)

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3066112A (en) 1959-01-30 1962-11-27 Rafael L Bowen Dental filling material comprising vinyl silane treated fused silica and a binder consisting of the reaction product of bis phenol and glycidyl acrylate
US3179623A (en) 1959-01-30 1965-04-20 Rafael L Bowen Method of preparing a monomer having phenoxy and methacrylate groups linked by hydroxy glyceryl groups
US4381918A (en) 1976-03-16 1983-05-03 Ehrnford Lars E M Method of producing a composite resin, preferably for use as a dental material
DE3416083A1 (de) * 1984-04-30 1985-10-31 Ernst Dipl.-Kaufm. 2000 Hamburg Mühlbauer Verpackung fuer verwendungsportionen von plastischer zahnfuellmasse
US4744759A (en) 1986-05-13 1988-05-17 American Dental Association Health Foundation Inserts for composite dental restorations
US4892481A (en) * 1987-04-07 1990-01-09 Dentsply Research & Development Corp. Dental composite carrier and composite package
US4952530A (en) 1988-12-01 1990-08-28 Erico International Corporation Dental composite material and process
WO1996003090A1 (fr) * 1994-07-25 1996-02-08 Ernst Mühlbauer KG Conditionnement pour matieres dentaires
US5621035A (en) 1995-02-08 1997-04-15 M.E.D. Usa Ceramic fused fiber enhanced dental materials

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3066112A (en) 1959-01-30 1962-11-27 Rafael L Bowen Dental filling material comprising vinyl silane treated fused silica and a binder consisting of the reaction product of bis phenol and glycidyl acrylate
US3179623A (en) 1959-01-30 1965-04-20 Rafael L Bowen Method of preparing a monomer having phenoxy and methacrylate groups linked by hydroxy glyceryl groups
US4381918A (en) 1976-03-16 1983-05-03 Ehrnford Lars E M Method of producing a composite resin, preferably for use as a dental material
US4392828A (en) 1976-03-16 1983-07-12 Ehrnford Lars E M Method for restoring a tooth
DE3416083A1 (de) * 1984-04-30 1985-10-31 Ernst Dipl.-Kaufm. 2000 Hamburg Mühlbauer Verpackung fuer verwendungsportionen von plastischer zahnfuellmasse
US4744759A (en) 1986-05-13 1988-05-17 American Dental Association Health Foundation Inserts for composite dental restorations
US4892481A (en) * 1987-04-07 1990-01-09 Dentsply Research & Development Corp. Dental composite carrier and composite package
US4952530A (en) 1988-12-01 1990-08-28 Erico International Corporation Dental composite material and process
WO1996003090A1 (fr) * 1994-07-25 1996-02-08 Ernst Mühlbauer KG Conditionnement pour matieres dentaires
US5621035A (en) 1995-02-08 1997-04-15 M.E.D. Usa Ceramic fused fiber enhanced dental materials

Also Published As

Publication number Publication date
AU1595499A (en) 1999-06-15
EP1033944A1 (fr) 2000-09-13

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