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WO2013060662A3 - Verfahren zur beschichtung von metallischen oberflächen mit einer wässerigen zusammensetzung aus vielen komponenten - Google Patents

Verfahren zur beschichtung von metallischen oberflächen mit einer wässerigen zusammensetzung aus vielen komponenten Download PDF

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Publication number
WO2013060662A3
WO2013060662A3 PCT/EP2012/070929 EP2012070929W WO2013060662A3 WO 2013060662 A3 WO2013060662 A3 WO 2013060662A3 EP 2012070929 W EP2012070929 W EP 2012070929W WO 2013060662 A3 WO2013060662 A3 WO 2013060662A3
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WO
WIPO (PCT)
Prior art keywords
coating
composition
water
compound
pretreatment
Prior art date
Application number
PCT/EP2012/070929
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English (en)
French (fr)
Other versions
WO2013060662A2 (de
Inventor
Thomas Kolberg
Peter Schubach
Manfred Walter
Carola Komp
Michael DRÖGE
Original Assignee
Chemetall Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=47049176&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=WO2013060662(A3) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Priority to JP2014537573A priority Critical patent/JP6305340B2/ja
Priority to IN3778CHN2014 priority patent/IN2014CN03778A/en
Priority to US14/353,164 priority patent/US10378120B2/en
Priority to EP12775501.5A priority patent/EP2771499B1/de
Priority to CN201280063864.7A priority patent/CN104271799B/zh
Application filed by Chemetall Gmbh filed Critical Chemetall Gmbh
Priority to MX2014004933A priority patent/MX353928B/es
Priority to RU2014120920A priority patent/RU2661643C2/ru
Priority to BR112014009860-3A priority patent/BR112014009860B1/pt
Priority to ES12775501.5T priority patent/ES2556967T3/es
Publication of WO2013060662A2 publication Critical patent/WO2013060662A2/de
Publication of WO2013060662A3 publication Critical patent/WO2013060662A3/de
Priority to ZA2014/03569A priority patent/ZA201403569B/en

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1229—Composition of the substrate
    • C23C18/1241—Metallic substrates
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1204—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material inorganic material, e.g. non-oxide and non-metallic such as sulfides, nitrides based compounds
    • C23C18/122—Inorganic polymers, e.g. silanes, polysilazanes, polysiloxanes
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/34—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/78—Pretreatment of the material to be coated
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/78—Pretreatment of the material to be coated
    • C23C22/80—Pretreatment of the material to be coated with solutions containing titanium or zirconium compounds
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/82—After-treatment
    • C23C22/83—Chemical after-treatment
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D13/00—Electrophoretic coating characterised by the process
    • C25D13/20—Pretreatment
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D5/00—Electroplating characterised by the process; Pretreatment or after-treatment of workpieces
    • C25D5/34—Pretreatment of metallic surfaces to be electroplated
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D5/00—Electroplating characterised by the process; Pretreatment or after-treatment of workpieces
    • C25D5/34—Pretreatment of metallic surfaces to be electroplated
    • C25D5/36—Pretreatment of metallic surfaces to be electroplated of iron or steel
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D5/00—Electroplating characterised by the process; Pretreatment or after-treatment of workpieces
    • C25D5/34—Pretreatment of metallic surfaces to be electroplated
    • C25D5/42—Pretreatment of metallic surfaces to be electroplated of light metals
    • C25D5/44—Aluminium
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C2222/00—Aspects relating to chemical surface treatment of metallic material by reaction of the surface with a reactive medium
    • C23C2222/20—Use of solutions containing silanes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/31504—Composite [nonstructural laminate]
    • Y10T428/31652—Of asbestos
    • Y10T428/31663—As siloxane, silicone or silane

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Electrochemistry (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
  • Paints Or Removers (AREA)
  • Chemical Treatment Of Metals (AREA)

Abstract

Die Erfindung betrifft ein Verfahren zur Verbesserung des Umgriffs einer Elektrotauchlack-Beschichtung durch Beschichten von metallischen Oberflächen mit einer Silan/Silanol/Siloxan/Polysiloxan enthaltenden Vorbehandlungs-Zusammensetzung, wobei diese Zusammensetzung neben Wasser a) mindestens eine Verbindung a) ausgewählt aus Silanen, Silanolen, Siloxanen und Polysiloxanen enthält, von denen mindestens eine dieser Verbindungen noch kondensieren kann, und b) mindestens eine Titan-, Hafnium- oder/und Zirkonium-haltige Verbindung b) sowie c) mindestens eine Art Kationen c) ausgewählt aus Kationen von Metallen der 1. bis 3. und 5. bis 8. Nebengruppe einschließlich Lanthaniden sowie der 2. Hauptgruppe des Periodensystems der Elemente oder/und mindestens eine entsprechende Verbindung c) oder/und d) mindestens eine organische Verbindung d) enthält ausgewählt aus Monomeren, Oligomeren, Polymeren, Copolymeren und Blockcopolymeren, wobei die mit dieser Zusammensetzung frisch aufgebrachte Beschichtung zumindest einmal mit Wasser gespült wird, wobei a) mindestens eine Wasserspülung einen Gehalt an Tensid aufweist oder/und wobei b) die Substrate vor der Silan-basierten Vorbehandlung mindestens einmal mit einer eisenhaltigen wässerigen Zusammensetzung behandelt werden, wobei nach dem Spülen mit Wasser eine Elektrotauchlack-Beschichtung aufgebracht wird und wobei die mit dieser Zusammensetzung frisch aufgebrachte Beschichtung bis zu diesem Spülen nicht durchgetrocknet wird, so dass die mindestens eine kondensationsfähige Verbindung a) bis zum Spülen der Vorbehandlungs-Beschichtung mit Wasser oder/und bis zum Beschichten mit einem Elektrotauchlack nicht stark kondensiert.
PCT/EP2012/070929 2011-10-24 2012-10-23 Verfahren zur beschichtung von metallischen oberflächen mit einer wässerigen zusammensetzung aus vielen komponenten WO2013060662A2 (de)

Priority Applications (10)

Application Number Priority Date Filing Date Title
ES12775501.5T ES2556967T3 (es) 2011-10-24 2012-10-23 Procedimiento para el recubrimiento de superficies metálicas con una composición acuosa de múltiples componentes
IN3778CHN2014 IN2014CN03778A (de) 2011-10-24 2012-10-23
US14/353,164 US10378120B2 (en) 2011-10-24 2012-10-23 Method for coating metallic surfaces with a multi-component aqueous composition
EP12775501.5A EP2771499B1 (de) 2011-10-24 2012-10-23 Verfahren zur beschichtung von metallischen oberflächen mit einer wässerigen zusammensetzung aus vielen komponenten
CN201280063864.7A CN104271799B (zh) 2011-10-24 2012-10-23 用多组分水性组合物涂覆金属表面的方法
JP2014537573A JP6305340B2 (ja) 2011-10-24 2012-10-23 多種の成分からなる水性組成物による金属表面の被覆方法
MX2014004933A MX353928B (es) 2011-10-24 2012-10-23 Metodo para recubrir superficies metalicas con una composicion acuosa con multiples componentes.
RU2014120920A RU2661643C2 (ru) 2011-10-24 2012-10-23 Способ покрытия металлических поверхностей водной композицией из многих компонентов
BR112014009860-3A BR112014009860B1 (pt) 2011-10-24 2012-10-23 processo para aperfeiçoamento do poder de arremesso de um revestimento por eletrodeposição, e, uso de substratos metálicos revestidos e de uma composição de tratamento prévio aquosa
ZA2014/03569A ZA201403569B (en) 2011-10-24 2014-05-16 Method for coating metallic surfaces with a multi-component aqueous composition

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102011085091 2011-10-24
DE102011085091.0 2011-10-24

Publications (2)

Publication Number Publication Date
WO2013060662A2 WO2013060662A2 (de) 2013-05-02
WO2013060662A3 true WO2013060662A3 (de) 2013-11-14

Family

ID=47049176

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2012/070929 WO2013060662A2 (de) 2011-10-24 2012-10-23 Verfahren zur beschichtung von metallischen oberflächen mit einer wässerigen zusammensetzung aus vielen komponenten

Country Status (12)

Country Link
US (1) US10378120B2 (de)
EP (1) EP2771499B1 (de)
JP (1) JP6305340B2 (de)
CN (1) CN104271799B (de)
BR (1) BR112014009860B1 (de)
DE (1) DE102012219296A1 (de)
ES (1) ES2556967T3 (de)
IN (1) IN2014CN03778A (de)
MX (1) MX353928B (de)
RU (1) RU2661643C2 (de)
WO (1) WO2013060662A2 (de)
ZA (1) ZA201403569B (de)

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PL3682042T3 (pl) * 2017-09-14 2022-04-04 Chemetall Gmbh Sposób wstępnej obróbki materiałów aluminiowych, w szczególności kół aluminiowych
JP7410388B2 (ja) * 2019-10-17 2024-01-10 日本製鉄株式会社 塗装めっき鋼板
CN113818015A (zh) * 2021-09-22 2021-12-21 浙江大学 安全环保硅烷处理液及其应用
CN116004118B (zh) * 2021-10-22 2023-09-29 中国石油化工股份有限公司 一种涂层处理液及其制备方法和应用
CN114074063A (zh) * 2021-11-22 2022-02-22 深圳市深赛尔股份有限公司 一种用多组分水性组合物涂覆金属表面的方法
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ZA201403569B (en) 2015-07-29
BR112014009860A2 (pt) 2017-04-18
MX353928B (es) 2018-02-06
IN2014CN03778A (de) 2015-09-04
RU2014120920A (ru) 2015-12-10
EP2771499B1 (de) 2015-10-14
RU2661643C2 (ru) 2018-07-18
DE102012219296A1 (de) 2013-04-25
CN104271799B (zh) 2017-03-08
BR112014009860B1 (pt) 2021-01-19
EP2771499A2 (de) 2014-09-03
US20140255706A1 (en) 2014-09-11
US10378120B2 (en) 2019-08-13
WO2013060662A2 (de) 2013-05-02
CN104271799A (zh) 2015-01-07
ES2556967T3 (es) 2016-01-21
JP2015503021A (ja) 2015-01-29
MX2014004933A (es) 2014-10-17

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