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WO2010144070A3 - Method to produce nanoparticles of metal-oxygen system of the specified composition by electron beam evaporation and condensation in vacuum - Google Patents

Method to produce nanoparticles of metal-oxygen system of the specified composition by electron beam evaporation and condensation in vacuum Download PDF

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Publication number
WO2010144070A3
WO2010144070A3 PCT/UA2010/000027 UA2010000027W WO2010144070A3 WO 2010144070 A3 WO2010144070 A3 WO 2010144070A3 UA 2010000027 W UA2010000027 W UA 2010000027W WO 2010144070 A3 WO2010144070 A3 WO 2010144070A3
Authority
WO
WIPO (PCT)
Prior art keywords
vacuum
condensation
carrier
electron beam
nanoparticles
Prior art date
Application number
PCT/UA2010/000027
Other languages
French (fr)
Other versions
WO2010144070A2 (en
Inventor
Boris Paton
Boris Movchan
Iurii Karupov
Kostyantyn Yakovchuk
Original Assignee
Boris Paton
Boris Movchan
Iurii Karupov
Kostyantyn Yakovchuk
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Boris Paton, Boris Movchan, Iurii Karupov, Kostyantyn Yakovchuk filed Critical Boris Paton
Publication of WO2010144070A2 publication Critical patent/WO2010144070A2/en
Publication of WO2010144070A3 publication Critical patent/WO2010144070A3/en

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Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/14Methods for preparing oxides or hydroxides in general
    • C01B13/20Methods for preparing oxides or hydroxides in general by oxidation of elements in the gaseous state; by oxidation or hydrolysis of compounds in the gaseous state
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00Nanotechnology for materials or surface science, e.g. nanocomposites
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00Compounds of titanium
    • C01G23/04Oxides; Hydroxides
    • C01G23/047Titanium dioxide
    • C01G23/07Producing by vapour phase processes, e.g. halide oxidation
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G3/00Compounds of copper
    • C01G3/02Oxides; Hydroxides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G49/00Compounds of iron
    • C01G49/02Oxides; Hydroxides
    • C01G49/08Ferroso-ferric oxide [Fe3O4]
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G5/00Compounds of silver
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/80Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/88Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by thermal analysis data, e.g. TGA, DTA, DSC
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/01Particle morphology depicted by an image
    • C01P2004/03Particle morphology depicted by an image obtained by SEM
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/51Particles with a specific particle size distribution
    • C01P2004/52Particles with a specific particle size distribution highly monodisperse size distribution
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/64Nanometer sized, i.e. from 1-100 nanometer

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Nanotechnology (AREA)
  • Environmental & Geological Engineering (AREA)
  • Geology (AREA)
  • Physics & Mathematics (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Composite Materials (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)
  • Physical Vapour Deposition (AREA)

Abstract

The invention pertains to synthesis of new nanomaterials in vacuum. A method to produce nanoparticles of metal -oxygen system by electron beam evaporation and condensation in vacuum is proposed, which includes simultaneous heating and evaporation of solid initial material and solid carrier material from at least two separate vessels in the vacuum chamber, mixing of vapour flows of initial material and carrier, deposition of mixed vapour flow on the substrate in the condensation zone with fixing of initial material nanoparticles on the substrate by carrier material which solidifies, and formation of nanoparticle condensate in the carrier. Used as the carrier material fixing the nanoparticles is a solid, soluble in liquid and evaporable in vacuum without decomposition simple or complex inorganic material.
PCT/UA2010/000027 2009-06-10 2010-05-18 Method to produce nanoparticles of metal-oxygen system of the specified composition by electron beam evaporation and condensation in vacuum WO2010144070A2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
UAA200905985A UA92556C2 (en) 2009-06-10 2009-06-10 Method of obtaining nanoparticles of metal-oxygen system with given composition by electron beam evaporation and condensation in vacuum
UAA200905985 2009-06-10

Publications (2)

Publication Number Publication Date
WO2010144070A2 WO2010144070A2 (en) 2010-12-16
WO2010144070A3 true WO2010144070A3 (en) 2011-05-26

Family

ID=43064755

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/UA2010/000027 WO2010144070A2 (en) 2009-06-10 2010-05-18 Method to produce nanoparticles of metal-oxygen system of the specified composition by electron beam evaporation and condensation in vacuum

Country Status (2)

Country Link
UA (1) UA92556C2 (en)
WO (1) WO2010144070A2 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2523716C1 (en) * 2012-11-28 2014-07-20 Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Казанский национальный исследовательский технический университет им. А.Н. Туполева-КАИ" (КНИТУ-КАИ) Method of obtaining nanomodified polymer materials
RU2685564C1 (en) * 2018-01-09 2019-04-22 Всеволод Германович Кизнер Method of synthesis of metal nanoparticles by deposition on a porous carbon material

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5498446A (en) * 1994-05-25 1996-03-12 Washington University Method and apparatus for producing high purity and unagglomerated submicron particles
US20030207031A1 (en) * 2002-05-06 2003-11-06 Honeywell International, Inc. Methods to make nanolaminate thermal barrier coatings
US20050000444A1 (en) * 2001-09-10 2005-01-06 Hass Derek D Method and apparatus application of metallic alloy coatings
UA82448C2 (en) * 2007-02-26 2008-04-10 Институт электросварки им. Е.О. Патона национальной академии наук Украины Method for production of encapsulated nanopowders and unit for implementation thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5498446A (en) * 1994-05-25 1996-03-12 Washington University Method and apparatus for producing high purity and unagglomerated submicron particles
US20050000444A1 (en) * 2001-09-10 2005-01-06 Hass Derek D Method and apparatus application of metallic alloy coatings
US20030207031A1 (en) * 2002-05-06 2003-11-06 Honeywell International, Inc. Methods to make nanolaminate thermal barrier coatings
UA82448C2 (en) * 2007-02-26 2008-04-10 Институт электросварки им. Е.О. Патона национальной академии наук Украины Method for production of encapsulated nanopowders and unit for implementation thereof
US20080268178A1 (en) * 2007-02-26 2008-10-30 E.O.Paton Electric Welding Institute Of The National Academy Of Sciences Of Ukraine Method of producing encapsulated nanopowders and installation for its realization

Also Published As

Publication number Publication date
UA92556C2 (en) 2010-11-10
WO2010144070A2 (en) 2010-12-16

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