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WO2010077039A3 - 유리 요오드 저감 폴리아릴렌 설파이드 제조 방법 - Google Patents

유리 요오드 저감 폴리아릴렌 설파이드 제조 방법 Download PDF

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Publication number
WO2010077039A3
WO2010077039A3 PCT/KR2009/007831 KR2009007831W WO2010077039A3 WO 2010077039 A3 WO2010077039 A3 WO 2010077039A3 KR 2009007831 W KR2009007831 W KR 2009007831W WO 2010077039 A3 WO2010077039 A3 WO 2010077039A3
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WO
WIPO (PCT)
Prior art keywords
polyarylene sulphide
production method
free iodine
sulphide
polyarylene
Prior art date
Application number
PCT/KR2009/007831
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English (en)
French (fr)
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WO2010077039A2 (ko
Inventor
신용준
김성기
임재봉
조준상
차일훈
Original Assignee
에스케이케미칼주식회사
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 에스케이케미칼주식회사 filed Critical 에스케이케미칼주식회사
Priority to ES09836360.9T priority Critical patent/ES2601363T3/es
Priority to JP2011543437A priority patent/JP5702731B2/ja
Priority to US13/142,932 priority patent/US9163119B2/en
Priority to EP09836360.9A priority patent/EP2383308B1/en
Priority to CN2009801577117A priority patent/CN102341434A/zh
Publication of WO2010077039A2 publication Critical patent/WO2010077039A2/ko
Publication of WO2010077039A3 publication Critical patent/WO2010077039A3/ko
Priority to US14/831,360 priority patent/US20150353687A1/en

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/14—Polysulfides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/14—Polysulfides
    • C08G75/16—Polysulfides by polycondensation of organic compounds with inorganic polysulfides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02—Polythioethers
    • C08G75/0204—Polyarylenethioethers
    • C08G75/0209—Polyarylenethioethers derived from monomers containing one aromatic ring
    • C08G75/0213—Polyarylenethioethers derived from monomers containing one aromatic ring containing elements other than carbon, hydrogen or sulfur
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02—Polythioethers
    • C08G75/0204—Polyarylenethioethers
    • C08G75/025—Preparatory processes
    • C08G75/0263—Preparatory processes using elemental sulfur
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02—Polythioethers
    • C08G75/0204—Polyarylenethioethers
    • C08G75/025—Preparatory processes
    • C08G75/0268—Preparatory processes using disulfides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02—Polythioethers
    • C08G75/04—Polythioethers from mercapto compounds or metallic derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02—Polythioethers
    • C08G75/06—Polythioethers from cyclic thioethers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/18—Manufacture of films or sheets

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)

Abstract

본 발명은 유리 요오드 함량이 저감된 폴리아릴렌 설파이드(polyarylene sulfide)를 제조하는 방법에 관한 것으로서, 구체적으로 디요오드 방향족 화합물과 황 화합물을 포함하는 반응물을 중합 반응하여, 폴리아릴렌 설파이드를 중합하는 단계; 및 상기에서 중합된 폴리아릴렌 설파이드를 100 내지 260°C에서 히트-세팅(heat setting)하는 단계를 포함한다. 본 발명에 따른 제조방법은 폴리아릴렌 설파이드 내의 유리 요오드 함량을 효과적으로 낮추어 후공정 설비의 부식을 방지할 수 있고, 제조된 폴리아릴렌 설파이드의 열 안정성 등의 물성도 개선하여, 폴리아릴렌 설파이드의 제조에 관한 산업 분야에 유용하게 응용될 수 있다.
PCT/KR2009/007831 2008-12-31 2009-12-28 유리 요오드 저감 폴리아릴렌 설파이드 제조 방법 WO2010077039A2 (ko)

Priority Applications (6)

Application Number Priority Date Filing Date Title
ES09836360.9T ES2601363T3 (es) 2008-12-31 2009-12-28 Procedimiento para la preparación de sulfuros de poliarileno con un contenido reducido de yodo libre
JP2011543437A JP5702731B2 (ja) 2008-12-31 2009-12-28 遊離ヨウ素が低減されたポリアリーレンスルフィドの製造方法
US13/142,932 US9163119B2 (en) 2008-12-31 2009-12-28 Method for preparing polyarylene sulfide with reduced free iodine content
EP09836360.9A EP2383308B1 (en) 2008-12-31 2009-12-28 Method for preparing polyarylene sulfide with reduced free iodine content
CN2009801577117A CN102341434A (zh) 2008-12-31 2009-12-28 制备自由碘含量降低的聚芳撑硫醚的方法
US14/831,360 US20150353687A1 (en) 2008-12-31 2015-08-20 Method for preparing polyarylene sulfide with reduced free iodine content

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR10-2008-0137680 2008-12-31
KR1020080137680A KR101554010B1 (ko) 2008-12-31 2008-12-31 유리 요오드 저감 폴리아릴렌 설파이드의 제조 방법

Related Child Applications (2)

Application Number Title Priority Date Filing Date
US13/142,932 A-371-Of-International US9163119B2 (en) 2008-12-31 2009-12-28 Method for preparing polyarylene sulfide with reduced free iodine content
US14/831,360 Division US20150353687A1 (en) 2008-12-31 2015-08-20 Method for preparing polyarylene sulfide with reduced free iodine content

Publications (2)

Publication Number Publication Date
WO2010077039A2 WO2010077039A2 (ko) 2010-07-08
WO2010077039A3 true WO2010077039A3 (ko) 2010-10-14

Family

ID=42310361

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/KR2009/007831 WO2010077039A2 (ko) 2008-12-31 2009-12-28 유리 요오드 저감 폴리아릴렌 설파이드 제조 방법

Country Status (8)

Country Link
US (2) US9163119B2 (ko)
EP (1) EP2383308B1 (ko)
JP (1) JP5702731B2 (ko)
KR (1) KR101554010B1 (ko)
CN (2) CN104861163A (ko)
ES (1) ES2601363T3 (ko)
HK (1) HK1209144A1 (ko)
WO (1) WO2010077039A2 (ko)

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Publication number Priority date Publication date Assignee Title
KR101554010B1 (ko) * 2008-12-31 2015-09-18 에스케이케미칼 주식회사 유리 요오드 저감 폴리아릴렌 설파이드의 제조 방법
KR101457745B1 (ko) * 2011-08-19 2014-11-03 주식회사 엘지화학 폴리페닐렌 설파이드 제조 방법 및 이로부터 제조된 폴리페닐렌 설파이드
JP6062924B2 (ja) * 2012-03-30 2017-01-18 株式会社クレハ 粒状ポリアリーレンスルフィド及びその製造方法
WO2014025190A1 (ko) * 2012-08-07 2014-02-13 에스케이케미칼주식회사 폴리아릴렌 설파이드 수지 및 그의 제조 방법
JP6397412B2 (ja) * 2012-09-19 2018-09-26 エスケー ケミカルズ カンパニー リミテッド ポリアリーレンスルフィド系樹脂組成物および成形品
US9688817B2 (en) 2013-03-25 2017-06-27 DIC Corporation (Tokyo) Method for producing polyarylene sulfide resin and polyarylene sulfide resin composition
KR20160042939A (ko) * 2013-08-09 2016-04-20 디아이씨 가부시끼가이샤 폴리아릴렌설피드 수지 조성물 및 그 성형품
KR20160048129A (ko) * 2013-08-30 2016-05-03 디아이씨 가부시끼가이샤 다층 성형체 및 그것을 사용한 연료용 부품
WO2015049941A1 (ja) * 2013-10-01 2015-04-09 Dic株式会社 ポリアリーレンスルフィド樹脂組成物及びその成形品、並びに電気自動車部品
US10174199B2 (en) * 2014-02-24 2019-01-08 Teijin Limited Resin composition
TWI723082B (zh) * 2015-11-23 2021-04-01 南韓商Ｓｋ化學公司 聚芳硫醚及其製備方法
JP7100222B2 (ja) * 2015-11-23 2022-07-13 エスケー ケミカルズ カンパニー リミテッド ポリアリーレンスルフィド系樹脂組成物および成形品
KR102492258B1 (ko) * 2016-04-26 2023-01-26 에이치디씨폴리올 주식회사 내가수분해성이 우수한 폴리아릴렌 설파이드 수지 조성물
KR102503262B1 (ko) * 2016-05-19 2023-02-22 에이치디씨폴리올 주식회사 내화학성이 우수한 폴리아릴렌 설파이드 수지 조성물
KR20220161370A (ko) * 2020-03-26 2022-12-06 디에스엠 아이피 어셋츠 비.브이. 사출 성형 부품
KR20220007274A (ko) * 2020-07-10 2022-01-18 에이치디씨폴리올 주식회사 폴리아릴렌 설파이드 공중합체, 이의 제조방법, 및 이로부터 제조된 성형품

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KR101554010B1 (ko) * 2008-12-31 2015-09-18 에스케이케미칼 주식회사 유리 요오드 저감 폴리아릴렌 설파이드의 제조 방법

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Publication number Priority date Publication date Assignee Title
US4786713A (en) * 1987-11-06 1988-11-22 Eastman Kodak Company Copoly(arylene sulfidex-disulfide)
US4945155A (en) * 1989-05-11 1990-07-31 Eastman Kodak Company Preparation of low color copoly(arylene sulfide) by heating copoly(arylene sulfide)
US5256715A (en) * 1991-09-19 1993-10-26 Phillips Petroleum Company Poly(arylene sulfide) resin composition
KR20080018770A (ko) * 2006-08-24 2008-02-28 에스케이케미칼주식회사 폴리아릴렌 설파이드의 제조방법

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Title
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Also Published As

Publication number Publication date
ES2601363T3 (es) 2017-02-14
US20150353687A1 (en) 2015-12-10
EP2383308A4 (en) 2015-08-12
CN104861163A (zh) 2015-08-26
EP2383308B1 (en) 2016-09-07
KR20100079253A (ko) 2010-07-08
US20110269935A1 (en) 2011-11-03
CN102341434A (zh) 2012-02-01
JP2012514068A (ja) 2012-06-21
EP2383308A2 (en) 2011-11-02
WO2010077039A2 (ko) 2010-07-08
US9163119B2 (en) 2015-10-20
HK1209144A1 (en) 2016-03-24
JP5702731B2 (ja) 2015-04-15
KR101554010B1 (ko) 2015-09-18

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