WO2008100325A3 - Procédé de production de nanotubes de carbone - Google Patents
Procédé de production de nanotubes de carbone Download PDFInfo
- Publication number
- WO2008100325A3 WO2008100325A3 PCT/US2007/072098 US2007072098W WO2008100325A3 WO 2008100325 A3 WO2008100325 A3 WO 2008100325A3 US 2007072098 W US2007072098 W US 2007072098W WO 2008100325 A3 WO2008100325 A3 WO 2008100325A3
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- carbon
- chirality
- component
- catalyst component
- cylindrical
- Prior art date
Links
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title abstract 8
- 238000000034 method Methods 0.000 title abstract 4
- 239000002041 carbon nanotube Substances 0.000 title 1
- 229910021393 carbon nanotube Inorganic materials 0.000 title 1
- 239000003054 catalyst Substances 0.000 abstract 4
- 229910052799 carbon Inorganic materials 0.000 abstract 3
- 239000002109 single walled nanotube Substances 0.000 abstract 2
- 238000004140 cleaning Methods 0.000 abstract 1
- 239000002071 nanotube Substances 0.000 abstract 1
- 239000000758 substrate Substances 0.000 abstract 1
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/74—Iron group metals
- B01J23/745—Iron
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
- B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
- B01J23/85—Chromium, molybdenum or tungsten
- B01J23/88—Molybdenum
- B01J23/881—Molybdenum and iron
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/90—Regeneration or reactivation
- B01J23/94—Regeneration or reactivation of catalysts comprising metals, oxides or hydroxides of the iron group metals or copper
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J38/00—Regeneration or reactivation of catalysts, in general
- B01J38/04—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
- B01J38/12—Treating with free oxygen-containing gas
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y40/00—Manufacture or treatment of nanostructures
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/158—Carbon nanotubes
- C01B32/16—Preparation
- C01B32/162—Preparation characterised by catalysts
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
- B01J21/02—Boron or aluminium; Oxides or hydroxides thereof
- B01J21/04—Alumina
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
- B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
- B01J21/08—Silica
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
- B01J23/24—Chromium, molybdenum or tungsten
- B01J23/28—Molybdenum
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
- B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
- B01J23/46—Ruthenium, rhodium, osmium or iridium
- B01J23/462—Ruthenium
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/74—Iron group metals
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/02—Impregnation, coating or precipitation
- B01J37/0201—Impregnation
- B01J37/0203—Impregnation the impregnation liquid containing organic compounds
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/02—Impregnation, coating or precipitation
- B01J37/0234—Impregnation and coating simultaneously
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2202/00—Structure or properties of carbon nanotubes
- C01B2202/02—Single-walled nanotubes
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2202/00—Structure or properties of carbon nanotubes
- C01B2202/04—Nanotubes with a specific amount of walls
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2202/00—Structure or properties of carbon nanotubes
- C01B2202/06—Multi-walled nanotubes
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/10—Particle morphology extending in one dimension, e.g. needle-like
- C01P2004/13—Nanotubes
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/584—Recycling of catalysts
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Nanotechnology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Physics & Mathematics (AREA)
- Composite Materials (AREA)
- Manufacturing & Machinery (AREA)
- Inorganic Chemistry (AREA)
- Carbon And Carbon Compounds (AREA)
- Catalysts (AREA)
Abstract
La présente invention concerne des procédés de préparation de structures de carbone cylindriques, notamment de nanotubes de carbone à paroi unique, présentant une chiralité souhaitée. Les procédés comprennent les étapes de fourniture d'un composant catalytique sur un substrat et d'un composant de carbone, et de mise en contact du composant catalytique et du composant de carbone pour produire une structure de carbone cylindrique. On ne fournit ensuite plus de composant de carbone et on détermine la chiralité de la structure de carbone cylindrique. Le composant catalytique est ensuite nettoyé et le processus est répété jusqu'à ce que la structure de carbone cylindrique remplisse une caractéristique souhaitée, comme la longueur. La chiralité du nanotube de carbone à paroi unique produit après le nettoyage du composant catalytique est la même que celle du nanotube produit initialement.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2009518504A JP5358045B2 (ja) | 2006-06-28 | 2007-06-26 | カーボンナノチューブの製造方法 |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US11/475,919 | 2006-06-28 | ||
US11/475,919 US20100239491A1 (en) | 2006-06-28 | 2006-06-28 | Method of producing carbon nanotubes |
Publications (2)
Publication Number | Publication Date |
---|---|
WO2008100325A2 WO2008100325A2 (fr) | 2008-08-21 |
WO2008100325A3 true WO2008100325A3 (fr) | 2008-10-30 |
Family
ID=39661384
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US2007/072098 WO2008100325A2 (fr) | 2006-06-28 | 2007-06-26 | Procédé de production de nanotubes de carbone |
Country Status (3)
Country | Link |
---|---|
US (1) | US20100239491A1 (fr) |
JP (1) | JP5358045B2 (fr) |
WO (1) | WO2008100325A2 (fr) |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20100081568A1 (en) * | 2008-04-21 | 2010-04-01 | Lockheed Martin Corporation | Methods for producing carbon nanotubes with controlled chirality and diameter and products therefrom |
US9174847B2 (en) * | 2008-05-01 | 2015-11-03 | Honda Motor Co., Ltd. | Synthesis of high quality carbon single-walled nanotubes |
US8591858B2 (en) * | 2008-05-01 | 2013-11-26 | Honda Motor Co., Ltd. | Effect of hydrocarbon and transport gas feedstock on efficiency and quality of grown single-walled nanotubes |
BR112012002233A2 (pt) | 2009-07-31 | 2019-09-24 | Massachustts Institute Of Tech | sietmas e métodos relacionados à formação de nanoestruturas a base de carbono. |
FR2949075B1 (fr) | 2009-08-17 | 2013-02-01 | Arkema France | Catalyseur fe/mo supporte, son procede de preparation et utilisation pour la fabrication de nanotubes |
WO2011066288A2 (fr) * | 2009-11-25 | 2011-06-03 | Massachusetts Institute Of Technology | Systèmes et procédés d'amélioration de la croissance de nanostructures à base de carbone |
US9663368B2 (en) | 2010-10-28 | 2017-05-30 | Massachusetts Institute Of Technology | Carbon-based nanostructure formation using large scale active growth structures |
EP2961535B1 (fr) | 2013-02-28 | 2018-01-17 | N12 Technologies, Inc. | Distribution à base de cartouche de film de nanostructure |
JP6039534B2 (ja) | 2013-11-13 | 2016-12-07 | 東京エレクトロン株式会社 | カーボンナノチューブの生成方法及び配線形成方法 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5037785A (en) * | 1989-11-17 | 1991-08-06 | Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of Energy, Mines And Resources | Catalyst regeneration process using laser radiation |
WO2000063115A1 (fr) * | 1999-04-16 | 2000-10-26 | Commonwealth Scientific And Industrial Research Organisation | Films de nanotubes de carbone a multiples couches |
Family Cites Families (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2000516708A (ja) * | 1996-08-08 | 2000-12-12 | ウィリアム・マーシュ・ライス・ユニバーシティ | ナノチューブ組立体から作製された巨視的操作可能なナノ規模の装置 |
JP3441923B2 (ja) * | 1997-06-18 | 2003-09-02 | キヤノン株式会社 | カーボンナノチューブの製法 |
US6835366B1 (en) * | 1998-09-18 | 2004-12-28 | William Marsh Rice University | Chemical derivatization of single-wall carbon nanotubes to facilitate solvation thereof, and use of derivatized nanotubes |
CA2344577C (fr) * | 1998-09-18 | 2009-12-08 | William Marsh Rice University | Derivation chimique de nanotubes de carbone a paroi unique pour faciliter leur solvatation, et utilisation de nanotubes ainsi derives |
AU2002307283A1 (en) * | 2001-04-12 | 2002-10-28 | Honda Giken Kogyo Kabushiki Kaisha | Purification of carbon filaments and their use in storing hydrogen |
WO2003040446A2 (fr) * | 2001-06-15 | 2003-05-15 | The Pennsylvania State Research Foundation | Procede de purification de nanotubes et de nanofibres par rayonnement electromagnetique |
US20030124717A1 (en) * | 2001-11-26 | 2003-07-03 | Yuji Awano | Method of manufacturing carbon cylindrical structures and biopolymer detection device |
US7214361B2 (en) * | 2002-11-26 | 2007-05-08 | Honda Giken Kogyo Kabushiki Kaisha | Method for synthesis of carbon nanotubes |
JP2007504086A (ja) * | 2003-09-03 | 2007-03-01 | 本田技研工業株式会社 | 一次元炭素ナノ構造体の製造方法 |
JP2005343744A (ja) * | 2004-06-03 | 2005-12-15 | Matsushita Electric Ind Co Ltd | カーボンナノチューブ半導体の製造方法およびカーボンナノチューブ構造体 |
US20060057388A1 (en) * | 2004-09-10 | 2006-03-16 | Sungho Jin | Aligned and open-ended nanotube structure and method for making the same |
JP4868726B2 (ja) * | 2004-09-14 | 2012-02-01 | 富士通株式会社 | カーボンナノチューブの構造を制御する方法 |
JP4780546B2 (ja) * | 2004-11-08 | 2011-09-28 | 学校法人 名城大学 | カーボンナノチューブの作製方法及び電流制御素子の作製方法 |
US7727504B2 (en) * | 2004-12-01 | 2010-06-01 | William Marsh Rice University | Fibers comprised of epitaxially grown single-wall carbon nanotubes, and a method for added catalyst and continuous growth at the tip |
-
2006
- 2006-06-28 US US11/475,919 patent/US20100239491A1/en not_active Abandoned
-
2007
- 2007-06-26 WO PCT/US2007/072098 patent/WO2008100325A2/fr active Application Filing
- 2007-06-26 JP JP2009518504A patent/JP5358045B2/ja active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5037785A (en) * | 1989-11-17 | 1991-08-06 | Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of Energy, Mines And Resources | Catalyst regeneration process using laser radiation |
WO2000063115A1 (fr) * | 1999-04-16 | 2000-10-26 | Commonwealth Scientific And Industrial Research Organisation | Films de nanotubes de carbone a multiples couches |
Non-Patent Citations (3)
Title |
---|
HATA K ET AL: "Water-Assisted Highly Efficient Synthesis of Impurity-Free Single-Walled Carbon Nanotubes", SCIENCE, WASHINGTON, DC, vol. 306, 19 November 2004 (2004-11-19), pages 1362 - 1364, XP002993037, ISSN: 0036-8075 * |
HE MAOSHUAI ET AL: "Iron catalysts reactivation for efficient CVD growth of SWNT with base-growth mode on surface", J PHYS CHEM B; JOURNAL OF PHYSICAL CHEMISTRY B AUG 26 2004, vol. 108, no. 34, 26 August 2004 (2004-08-26), pages 12665 - 12668, XP002491259 * |
WANG Y ET AL: "Continued growth of Single-Walled Carbon Naontubes", NANO LETTERS, ACS, WASHINGTON, DC, US, vol. 5, no. 6, 1 June 2005 (2005-06-01), pages 997 - 1002, XP002379119, ISSN: 1530-6984 * |
Also Published As
Publication number | Publication date |
---|---|
US20100239491A1 (en) | 2010-09-23 |
JP2010503595A (ja) | 2010-02-04 |
JP5358045B2 (ja) | 2013-12-04 |
WO2008100325A2 (fr) | 2008-08-21 |
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