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WO2007012689A2 - Utilisation de compositions attractives pour l'elimination des tephritides - Google Patents

Utilisation de compositions attractives pour l'elimination des tephritides Download PDF

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Publication number
WO2007012689A2
WO2007012689A2 PCT/ES2006/000446 ES2006000446W WO2007012689A2 WO 2007012689 A2 WO2007012689 A2 WO 2007012689A2 ES 2006000446 W ES2006000446 W ES 2006000446W WO 2007012689 A2 WO2007012689 A2 WO 2007012689A2
Authority
WO
WIPO (PCT)
Prior art keywords
ammonium acetate
composition according
trimethylamine
attractant
attractive
Prior art date
Application number
PCT/ES2006/000446
Other languages
English (en)
Spanish (es)
Other versions
WO2007012689A3 (fr
Inventor
Eduardo Primo Yufera
Jaime Primo Millo
Vicente Navarro Llopis
Pilar Moya Sanz
Original Assignee
Universidad Politécnica De Valencia
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Universidad Politécnica De Valencia filed Critical Universidad Politécnica De Valencia
Publication of WO2007012689A2 publication Critical patent/WO2007012689A2/fr
Publication of WO2007012689A3 publication Critical patent/WO2007012689A3/fr

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Classifications

    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
    • A01N33/02—Amines; Quaternary ammonium compounds
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01M—CATCHING, TRAPPING OR SCARING OF ANIMALS; APPARATUS FOR THE DESTRUCTION OF NOXIOUS ANIMALS OR NOXIOUS PLANTS
    • A01M1/00—Stationary means for catching or killing insects
    • A01M1/20—Poisoning, narcotising, or burning insects
    • A01M1/2005—Poisoning insects using bait stations
    • A01M1/2016—Poisoning insects using bait stations for flying insects
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
    • A01N33/16—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds containing nitrogen-to-oxygen bonds
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/02—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
    • A01N43/36—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings

Definitions

  • This invention is part of the technical field of pest control methods.
  • the most widely used traps in these systems contain parapheromones or pheromones that are male-specific attractants.
  • paramedic pheromone (1-carboxylic acid tert-butyl-4-chloro-2-methylcyclohexane) that captures Mediterranean fly (Ceratitis capitata Wied.) And fly Natal fruit (Ceratitis rosa Karsch).
  • the para-pheromone methyleneugenol captures a large number of Bactrocera species, including the Bactrocera zonata (Saunders) peach fly, the Bactrocera dorsalis (Hendel) or Bactrocera musae (Tryon) Oriental fruit fly.
  • pheromone l, 7-dioxaspiro- (5,5) -undecane captures fly of the olive tree B. oleae (Gmelin).
  • baits to capture female fruit flies are based on food attractants or kairomonas.
  • protein baits such as yeast hydrolysates (Greany et al., 1977) and protein hydrolysates (McPhail, 1939) have been used to capture a wide range of different fruit fly species. Liquid protein baits capture both male and female, the percentage of females captured being higher, since these require proteins to ensure fertility. The use, however, of these baits entails a number of drawbacks.
  • application GB-2356144 discloses a method for selectively attracting fruit flies of the Tephritidae family to a particular place where an attractant mixture formed by a pyrazine, preferably 2,5-dimethylpyrazine, is found, in combination with ammonium salts and putrescine (1,4-diaminobutane). It also reports that the attractive combination can be used in combination with an insecticide, biopesticide or chemosterilizer.
  • Patent application P200400664 discloses the design of a semi-solid food bait, with phago-stimulant, toxic and specific attraction properties for the species of tefritid to be fought and which, due to its physical-chemical characteristics, is capable of maintaining its properties during, at least twelve months in field conditions.
  • the semi-solid gel is a specific tool to be used exclusively in the "attract and kill” technique, preferably using a sterilizer as a toxic ingredient; understood as toxic ingredient that which causes death or some disorder of development or reproductive process in insects.
  • the attractant consists of new attractant combinations, based on chemical food stimuli, similar to those protected in this invention.
  • the attractant in the case of application P200400664, the attractant is necessarily included in the semi-solid gel or, in a particular embodiment, in an adjacent position.
  • the attractant is independent of any other component of the system and, contrary to what happens with application P200400664, can be used for both population monitoring and control purposes.
  • the attractive composition disclosed in WO9807316A1 (ammonium acetate + trimethylamine + putrescine) is effective, mainly for the capture of Ceratitis capitata, it carries rigged an important problem that is its high cost. This fact derives not only from the high price of the product in the market but, in addition, a high density of traps is required for the mass capture technique to be effective in the field (between 50-60 traps / hectare). To this we must add that the useful life of these attractants in the field does not exceed 45 days, which implies several replenishments throughout the campaign. From a practical point of view, monitoring populations with this product is, although expensive, acceptable.
  • the present invention provides a series of combinations of food attractants, more potent than those currently available in the market, and which can be used in the detection, monitoring and control of the populations of tephritides of economic interest, with special reference to the Mediterranean fruit fly, Ceratitis capitata. Control will be exercised, preferably through the mass capture technique.
  • said attractant combinations formulated in the appropriate emitter support, can at least double the field life of the attractants currently marketed.
  • the present invention relates to the use of an attractive composition for the early detection, monitoring and / or control of populations of tephritid insects, characterized in that the composition comprises N-methyl-pyrrolidine together with one of the following compounds or combinations: - ammonium acetate
  • Said composition may further comprise one or more compounds preferably selected from ethyl acetate, acetic acid, ethanol, furyl alcohol, 5-methyl-3-heptanone, geranyl butyrate, linalool, 1,3-diethylbenzene, 2- nonanone, (E) -2-Hexeenoic acid, ammonium phosphate, biamonic phosphate, ammonium bicarbonate and one or more nitrogen compounds selected from free amines, amines in the form of salts and in the form of their amides, such as dimethylacetamide.
  • compounds preferably selected from ethyl acetate, acetic acid, ethanol, furyl alcohol, 5-methyl-3-heptanone, geranyl butyrate, linalool, 1,3-diethylbenzene, 2- nonanone, (E) -2-Hexeenoic acid, ammonium phosphate, biamonic phosphate, ammonium bicarbonate and one or more nitrogen compounds selected
  • amines there may be mentioned, for example, methylamine, dimethylamine, ethylmethylamine, propylmethylamine, isopropylamine, tert-butylamine, diethylamine, 1,3-propylenediamine, hexamethylenediamine and heptamethylenediamine.
  • the components may be adsorbed on an emitting support selected from one or more organic materials, one or more inorganic materials and mixtures thereof.
  • the components may be adsorbed on the emitting supports, separately or in combination.
  • the emitting material can be a material selected from microporous silicates, mesoporous silicates, microporous silicoaluminatos, mesoporous silicoaluminatos, microporous phosphoaluminatos, mesoporous phosphoalumininates and mixtures thereof.
  • said composition can be used in combination with at least one toxic ingredient, preferably a pyrethroid, and more preferably the pyrethroid is emptintrin or deltamerrin.
  • the term "in combination” means that it is used together with the toxic ingredient, but which is not normally part of the composition itself.
  • the composition may further comprise one or more volatile compounds of a fruit or a host plant, preferably borneol and p-cimeno.
  • the tefritid specific arctant is a combination of ammonium acetate + 1-methylpyrrolidine + trimethylamine + putrescine or a combination of ammonium acetate + 1-methylpyrrolidine + trimethylamine + cadaverine.
  • the rental composition may comprise one or more specific attractants that may be adsorbed (separately or in combination) on a controlled speed emitting material, selected from one or more organic materials, one or more inorganic materials, and mixtures of them, according to the state of the art.
  • a controlled speed emitting material selected from one or more organic materials, one or more inorganic materials, and mixtures of them, according to the state of the art.
  • emitting materials such as those disclosed in applications WO9944420 and WO0002448 can be used.
  • the arrantee, or specific attractants is preferably adsorbed on a material selected from microporous silicates, mesoporous silicates, microporous silicoaluminatos, mesoporous silicoaluminatos, microporous phosphoaluminatos, mesoporous phosphoaluminatos and mixtures of them.
  • the specific harness or attractants, adsorbed on the emitting support can be formulated, depending on the required emission rate, in a form selected from powder, agglomerated with different granulometries or tablets of different sizes and shapes.
  • the composition comprising the attractants ammonium acetate + n-methylpyrrolidine + trimethylamine + putrescine, or ammonium acetate + n-methylpyrrolidine + trimethylamine + putrescine is adsorbed on an emitting support, in this case, a magnesium silicate and said attractants They are compacted in a hydraulic press to obtain tablets of different sizes.
  • the emission rate of the attractants provided by ammonium acetate, that is, ammonia and acetic acid, as well as n-methylpyrrolidine can be modulated, depending on the requirements, varying the size or geometry of the tablets, its compaction pressure, the percentage of emitting support in the tablet, etc.
  • the ammonium acetate is compacted to form a tablet with an approximate weight of 1O g. and an average emission rate is obtained, under laboratory conditions, of approximately 20 mg / day.
  • the n-methylpyrrolidine, compacted in a 10 g tablet. emits with an average speed of approximately 4 mg / day.
  • traps are placed inside traps, according to the state of the art, for the capture of the different species of tefritids.
  • traps such as Tephri, OBT, McPhail, Multilure, etc. can be used, as recommended in the "Trapping Guidelines for Area-Wide Fruit FIy Programs" International Atomic Energy Agency, Vienna, 2003.
  • the selected trap will be primed with the selected synthesis attractant combination, preferably ammonium acetate + 1- methylpyrrolidine + trimethylamine + putrescine or ammonium acetate + 1-methylpyrrolidine + trimethylamine + cadaverine, and will be preferably combined with a insecticide (trap with side holes) to prevent the escape of captured insects.
  • the insecticides will be selected according to the state of the art. By way of example, without being restrictive, there may be mentioned malathion or naled solutions impregnated in dental cottons or DDVP tablets or sheets (dichlorvos).
  • the use of pyrethroids selected in function of having a relatively high vapor pressure, is proposed.
  • the pyrethroids can be formulated on state-of-the-art speed-controlled emitting brackets, preferably, but without being restrictive, emitting materials such as those disclosed in WO9944420 and WO0002448 can be used.
  • the pyrethroid preferably empentrine or deltamethrin, is adsorbed on an emitting support selected from microporous silicates, mesoporous silicates, microporous silicoaluminatos, mesoporous silicoaluminates, microporous phosphoaluminates, mesoporous phospho-aluminates, mesoporuminous mixtures from them.
  • an emitting support selected from microporous silicates, mesoporous silicates, microporous silicoaluminatos, mesoporous silicoaluminates, microporous phosphoaluminates, mesoporous phospho-aluminates, mesoporuminous mixtures from them.
  • a further object of the present invention is the use of an ardent combination, as defined above, to monitor and combat insects.
  • the insects are from the Tephritidae family.
  • insects of the family Tephritidae are insects of species belonging to the genera Bactrocera spp., Ceratitis spp., Anastrepha spp. and Rhagoletis spp.
  • the present invention has as an additional object an ardent composition for the early detection, monitoring and / or control of populations of tephritid insects, characterized in that it comprises N-methyl-pyrrolidine together with one of the following compounds or combinations:
  • Said additive composition may further comprise one or more compounds preferably selected from ethyl acetate, acetic acid, ethanol, diethylamine, dimethylacetamide, furyl alcohol, 5-methyl-3-heptanone, butyrate geranyl, linalool, 1,3-diethylbenzene, 2-nonanone, (E) -2-hexenoic acid, ammonium phosphate, biamonic phosphate, ammonium bicarbonate and one or more nitrogen compounds selected from free amines, salt-shaped amines and in Shape of their amides.
  • compounds preferably selected from ethyl acetate, acetic acid, ethanol, diethylamine, dimethylacetamide, furyl alcohol, 5-methyl-3-heptanone, butyrate geranyl, linalool, 1,3-diethylbenzene, 2-nonanone, (E) -2-hexenoic acid, ammonium phosphate, biamonic phosphat
  • Figure 1 shows the evolution of the catches of C. capitata for each issuer as a function of time.
  • the first attractant is the commercial 3-component Biolure of the Suterra house composed of three emitters of ammonium acetate, trimethylamine and putrescine (Type A Attractant).
  • the second attractant was composed of two sepiolite emitters, one containing 5.5 g. ammonium acetate and the second with 1.0 g of n-methylpyrrolidine (Type B Attractant).
  • the test was carried out in a field of White Citrus reticulata clementines in the municipality of Sagunto (Valencia).
  • the field is isolated and has a total extension of 60 hectares that is subdivided into two plots of 30 hectares.
  • the two types of attractants were placed, together with a DDVP tablet, in Tephripe trap in the two adjacent plots, at a density of 50 traps per hectare.
  • the traps were placed 45 days before the date of collection.
  • the effectiveness of the attractants was measured indirectly as a percentage of damaged fruit in each of the plots. For this, the fruit is sampled in 5 points of each plot, the same day of the harvest, obtaining an average of damaged fruit in each of the plots treated with the two types of attractants.
  • Table 1 shows the efficacy of the ammonium acetate (AA) + n-methylpyrrolidine combination in the massive capture against the 3-component Biolure of Suterra SLL. The effectiveness is assessed based on the percentage of
  • Attractant N 0 samples Sampled fruits% of damaged fruit
  • Example 2 Comparative study of attractants for Ceratitis capitata (Wiedemann) The objective was to compare 4 types of attractants for Ceratitis capitata
  • the emitting support of the compounds is a silicAT
  • the comparative test of the emitters was carried out in an orange grove in the Sagunto area (Valencia). The trial began on October 14, 2004 and the end of the trial on January 14, 2005. The different attractants, together with a vapona pill, were placed inside Tephri-trap traps. 5 blocks were established in the test zone, each consisting of the 4 Tephri-trap traps. Weekly readings of the traps were made and they were relocated in order to prevent the effect of trap location from influencing the catches. The minimum distance between traps was 15 meters and between blocks of 100 meters. The captures were grouped and the statistical analysis of the data was performed using the Statgraphics 5.1 program. The ANOVA tool was used, establishing as a dependent variable the total catches and as an independent variable the type of issuer. P-value values greater than 0.05 indicate that there are no significant differences between the catches for each issuer.
  • Table 2 and Figure 2 show the evolution of catches depending on the type of issuer. Issuers that have the same letter in parentheses imply that no significant differences were found in the catches for each of them. Table 2.- Total captures of C. capitata for each issuer.
  • Figure 1 shows the evolution of the catches of C. capitata for each issuer.
  • Example 3 A field test has been carried out to verify the efficacy of different attractant mixtures.
  • the attractants tested were: emitter of 5.5 grams of ammonium acetate, emitter of 125 mg of hexamethylenediamine and an emitter with one of the following compositions: A) 5-5-5
  • the three numbers of each composition correspond to the percentage, in percent, of dimethylamine, trimethylamine and 1-methylpyrrolidine respectively, the total weight of each emitter being 10 grams.
  • ammonium acetate, hexamethylenediamine and each of the aforementioned compositions form four types of attractants that are tested in the field to see which of them attracts more flies.
  • the attractants are introduced in Tephri-trap type flycatchers with a DDVP tablet.
  • each block 4 traps are introduced, one with each type of attractant, placed 30 meters away from each other. 4 blocks of traps are placed for the test. Weekly the number of flies captured by each flycatcher is checked and rotated in a clockwise direction within each block. Each of the readings of each block is considered as an efficacy value, which gives us 4 weekly repetitions for 6 weeks.
  • N number of repetitions of each measurement
  • n test weeks Capture levels with different letters differ significantly with P ⁇ 0.05.
  • Attractant A is composed of. three emitters of sepiolite with the following components: ammonium acetate 5.5 grams, methylpyrrolidine 1.0 g and hexamethylenediamine 125 mg.
  • A is composed of four sepiolite emitters with the following amounts of substances: ammonium acetate 5.5 grams, trimethylamine hydrochloride 2.5 g, methylpyrrolidine 0.5 g and putrescine 100 mg, and attractant B is formed only by ammonium acetate, trimethylamine hydrochloride and putrescine in the same concentrations as in attractant A.

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  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Wood Science & Technology (AREA)
  • Environmental Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • General Health & Medical Sciences (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Agronomy & Crop Science (AREA)
  • Toxicology (AREA)
  • Insects & Arthropods (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Catching Or Destruction (AREA)

Abstract

La présente invention concerne une série de compositions d'agents attractifs qui peuvent être utilisées dans la détection, le suivi et l'élimination des populations de téphritides présentant un intérêt économique, s'adressant notamment à la mouche des fruits du bassin méditerranéen appelée Ceratitis capitata. L'élimination s'effectue de préférence par une technique de capture massive.
PCT/ES2006/000446 2005-07-29 2006-07-28 Utilisation de compositions attractives pour l'elimination des tephritides WO2007012689A2 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
ES200501992A ES2265299B1 (es) 2005-07-29 2005-07-29 Nuevas convinaciones atrayentes para el control de tefritidos.
ESP200501992 2005-07-29

Publications (2)

Publication Number Publication Date
WO2007012689A2 true WO2007012689A2 (fr) 2007-02-01
WO2007012689A3 WO2007012689A3 (fr) 2007-04-12

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PCT/ES2006/000446 WO2007012689A2 (fr) 2005-07-29 2006-07-28 Utilisation de compositions attractives pour l'elimination des tephritides

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WO (1) WO2007012689A2 (fr)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014037936A1 (fr) * 2012-09-04 2014-03-13 The State Of Israel, Ministry Of Agriculture & Rural Development, Agricultural Research Organization (Aro) (Volcani Center) Système pour capturer et compter de façon automatique des insectes volants
IL237575B (en) * 2012-09-04 2021-10-31 The State Of Israel Ministry Of Agriculture & Rural Development Agricultural Res Organization Aro Vo A system for the automatic capture and counting of flying insects

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3127426A4 (fr) * 2014-03-31 2017-11-15 AO Midori Biocontrol S.L. Diffuseur de substances attractives d'insectes

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5766617A (en) * 1996-08-23 1998-06-16 The United States Of America As Represented By The Secretary Of Agriculture Trapping system for mediterranean fruit flies
ES2156492B1 (es) * 1998-07-08 2002-02-01 Univ Valencia Politecnica Procedimiento de obtencion de sepiolitas modificadas y uso de sepiolitas en la obtencion de emisores de semioquimicos con velocidad de emision controlada.
ES2239548B1 (es) * 2004-03-11 2007-02-01 Universidad Politecnica De Valencia Un cebo alimentario con atrayente especifico para combatir insectos tefritidos.

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014037936A1 (fr) * 2012-09-04 2014-03-13 The State Of Israel, Ministry Of Agriculture & Rural Development, Agricultural Research Organization (Aro) (Volcani Center) Système pour capturer et compter de façon automatique des insectes volants
IL237575B (en) * 2012-09-04 2021-10-31 The State Of Israel Ministry Of Agriculture & Rural Development Agricultural Res Organization Aro Vo A system for the automatic capture and counting of flying insects

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Publication number Publication date
ES2265299B1 (es) 2008-02-01
ES2265299A1 (es) 2007-02-01
WO2007012689A3 (fr) 2007-04-12

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