US9039907B2 - Methods for improving integrated photonic device uniformity - Google Patents
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- US9039907B2 US9039907B2 US13/552,506 US201213552506A US9039907B2 US 9039907 B2 US9039907 B2 US 9039907B2 US 201213552506 A US201213552506 A US 201213552506A US 9039907 B2 US9039907 B2 US 9039907B2
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/84—Systems specially adapted for particular applications
- G01N21/88—Investigating the presence of flaws or contamination
- G01N21/95—Investigating the presence of flaws or contamination characterised by the material or shape of the object to be examined
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L22/00—Testing or measuring during manufacture or treatment; Reliability measurements, i.e. testing of parts without further processing to modify the parts as such; Structural arrangements therefor
- H01L22/10—Measuring as part of the manufacturing process
- H01L22/12—Measuring as part of the manufacturing process for structural parameters, e.g. thickness, line width, refractive index, temperature, warp, bond strength, defects, optical inspection, electrical measurement of structural dimensions, metallurgic measurement of diffusions
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L22/00—Testing or measuring during manufacture or treatment; Reliability measurements, i.e. testing of parts without further processing to modify the parts as such; Structural arrangements therefor
- H01L22/20—Sequence of activities consisting of a plurality of measurements, corrections, marking or sorting steps
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01B—MEASURING LENGTH, THICKNESS OR SIMILAR LINEAR DIMENSIONS; MEASURING ANGLES; MEASURING AREAS; MEASURING IRREGULARITIES OF SURFACES OR CONTOURS
- G01B2210/00—Aspects not specifically covered by any group under G01B, e.g. of wheel alignment, caliper-like sensors
- G01B2210/56—Measuring geometric parameters of semiconductor structures, e.g. profile, critical dimensions or trench depth
Definitions
- This disclosure relates to methods for improving the uniformity and repeatability of the spectral response of integrated photonic devices.
- Integrated photonic devices fabricated in a high refractive index contrast material system such as, for example, a Si/SiO 2 material system are very sensitive to small variations in the device dimensions. Such devices are very sensitive to small variations in the thickness t and etch depth d, as well as to small variations in the linewidth w of the device structures made in the core material (e.g., Si) of the material system.
- FIG. 1 shows a cross section of an example photonic structure, illustrating thickness t, linewidth w and etch depth d. For example, a variation of 1 nanometer (nm) in the linewidth w can result in a shift in spectral response of wavelength selective photonic devices (such as e.g.
- Variations in the linewidth w and etch depth d of device structures may be mainly influenced by the patterning process, including photolithography and etching. Variations in the thickness t or height of the device structures may be determined by the substrate manufacturing process.
- integrated photonic devices can be fabricated in thin silicon-on-insulator (SOI) substrates (comprising e.g. a 220 nm thick silicon device layer on top of a 2000 nm thick silicon dioxide layer).
- SOI silicon-on-insulator
- the thickness variation of the silicon device layer of a silicon-on-insulator substrate may depend on the vendor specification. The thickness variation is typically 10% over the wafer or substrate. For a 220 nm thick silicon device layer, this means a variation of about 22 nm in thickness of the silicon device layer over the substrate. This may correspond to a shift or variation of about 22 nm to 44 nm in the spectral response of wavelength selective optical devices over the wafer. This shift or variation is unacceptable for commercial viable silicon photonic technology.
- a method for improving the thickness uniformity and reducing the surface roughness of thin films such as the top silicon film of a silicon-on-insulator wafer.
- the method uses a vacuum GCIB (Gas Cluster Ion Beam) etching and smoothing process.
- GCIB Gas Cluster Ion Beam
- the film thickness map information is fed into the GCIB beam-control apparatus as a data file.
- a mathematical algorithm is used to create a beam-dose contour to selectively remove surface material and thereby achieve a uniform film thickness.
- Example embodiments of the present disclosure provide methods for improving the uniformity of the spectral response of photonic devices over a wafer or substrate and for improving the repeatability of the spectral response of photonic devices from wafer to wafer and from batch to batch.
- the methods according to the present disclosure can in particular advantageously be used for integrated photonic devices fabricated in a high refractive index contrast material system.
- the present disclosure provides a method for improving the uniformity and repeatability of the spectral response of photonic devices fabricated in a thin device layer such as a silicon device layer of an SOI substrate, over a predetermined substrate area.
- the method comprises: (i) establishing an initial device layer thickness map for the predetermined area; (ii) establishing a linewidth map for the predetermined area; (iii) establishing an etch depth map for the predetermined area; (iv) based on the initial device layer thickness map, the linewidth map and the etch depth map, calculating an optimal device layer thickness map and a corresponding thickness correction map for the predetermined substrate area taking into account device design data; and (v) performing a location specific corrective etch process in accordance with the thickness correction map.
- establishing an initial device layer thickness map comprises measuring the initial thickness of the device layer over the predetermined substrate area as a function of x and y, where x and y are the spatial wafer coordinates.
- the initial device layer thickness can be measured by means of spectroscopic ellipsometry, e.g. with an accuracy better than 1 nm.
- the number of measurement points per wafer can for example be on the order of 300 to 400 points for a 200 mm wafer.
- the present disclosure is not limited thereto, and the number of measurement points per unit area can be higher or lower.
- establishing a linewidth map and establishing an etch depth map may comprise measuring the linewidth and etch depth over the predetermined substrate area as a function of x and y, where x and y are the spatial wafer coordinates. Measuring the linewidth and etch depth may, for example, be done by means of scatterometry.
- calculating an optimum device layer thickness map may comprise calculating as a function of the spatial wafer coordinates an optimum device layer thickness needed for matching a predetermined spectral response of a photonic device.
- the thickness correction map may be determined by calculating the difference between the optimum device layer thickness and the initial device layer thickness as a function of the spatial wafer coordinates. This difference corresponds to the thickness correction to be performed by the location specific corrective etch process.
- the location specific corrective etch process may for example be a Gas Cluster Ion Beam process, as for example described in U.S. Pat. No. 6,537,606.
- the method of the present disclosure may be particularly relevant and advantageous for integrated photonic devices fabricated in a high refractive index contrast material system, i.e. a material system having a high refractive index contrast between a waveguide core material and a cladding material (difference in refractive index between the core material and the cladding material larger than 1).
- Photonic devices fabricated in such material systems are highly sensitive to process variations. Examples of such high refractive index contrast material systems are Si/SiO 2 , SiN/SiO 2 , SiON/SiO 2 , TaO 2 /SiO 2 , Si(O)C/SiO 2 , InGaAsP/SiO 2 and Ge/Al 2 O 3 . Other examples are possible as well.
- the thickness correction map may be established before starting the fabrication of photonic device structures, and the location specific corrective etch process is performed before fabrication of the photonic device structures.
- Establishing the initial device layer thickness map may comprise measuring the initial thickness of the device layer on the non-processed substrate as a function of the spatial wafer coordinates in the predetermined area.
- Establishing a linewidth map and establishing an etch depth map may comprise estimating the linewidth and etch depth as a function of the spatial wafer coordinates in the predetermined area, based on data previously collected from process control.
- the thickness correction map may be established after fabricating the photonic device structures.
- Establishing the initial device layer thickness map may comprise measuring the thickness of the device layer on the processed substrate as a function of the spatial wafer coordinates in the predetermined area.
- Establishing a linewidth map and establishing an etch depth map may comprise measuring the linewidth and etch depth as a function of the spatial wafer coordinates in the predetermined area after fabrication of the photonic devices.
- additionally the optical response of the photonic devices can be measured and this optical response (such as bandwidth, maximum wavelength, resonance wavelength, and other optical responses) of the devices can be used as an additional input for calculating the thickness correction map.
- a thickness correction can be performed before fabricating the photonic device structures, according to the first aspect.
- a thickness correction may be performed according to the second aspect.
- FIG. 1 shows a cross section of an example photonic structure, illustrating thickness t, linewidth w and etch depth d.
- FIG. 2 schematically illustrates an example method according to the present disclosure, wherein a thickness correction is performed before photonic device fabrication.
- FIG. 3 schematically illustrates an example method according to the present disclosure, wherein a thickness correction is performed after photonic device fabrication.
- FIG. 4 schematically illustrates example methods according to the present disclosure, wherein the silicon device layer is thickened by epitaxial growth.
- FIG. 5 illustrates a method in accordance with an example of the present disclosure.
- the present disclosure provides methods for improving the uniformity, the repeatability and the controllability of the spectral response of integrated photonic devices, using a location specific corrective etch process, such as a GCIB-based thickness correction process. It is an advantage of methods according to the present disclosure that they result in a better or improved uniformity of the spectral response of photonic devices within a wafer, from wafer to wafer and from batch to batch, as compared to prior art methods.
- the non-uniformity of the spectral response of integrated photonic devices depends on three physical factors: linewidth, thickness or height, and refractive index. Since the refractive index of the device layer such as a silicon layer is uniform over a wafer, linewidth and height variation are the dominant sources of non-uniformities. Since these two factors are interlinked, a variation in one factor can be compensated by a variation in the other factor. For example, a variation in height can be compensated by a variation in linewidth or vice-versa, a variation in linewidth can be compensated by a variation in height or thickness.
- the thickness of the device(s) is corrected by using a location specific corrective etch process such as a Gas Cluster Ion Beam Process (GCIB), taking into account local linewidth and height data.
- GCIB Gas Cluster Ion Beam Process
- a tailor-made thickness profile is used that compensates for the other systematic within-wafer process variations, e.g. related to photolithography processes (e.g., mask quality, resist thickness, projection optics, etc.) or related to etch processes (e.g., such as plasma non-uniformities during dry etching).
- a pre-pattern thickness correction of the device layer e.g., of a SOI substrate
- a thickness correction is done before fabrication of the photonic devices.
- FIG. 2 A location specific thickness correction is performed based on a thickness correction map.
- additional data are taken into account. These additional data may comprise linewidth data and etch depth data previously collected from optical lithography and dry etch process control and device design data.
- the local linewidth variation and the local etch depth variation may be anticipated or estimated as a function of the spatial wafer coordinates, leading to an anticipated or estimated linewidth map and an anticipated or estimated etch depth map.
- a thickness correction map may be generated. This thickness correction map may be calculated based on the local device layer thickness needed for obtaining a predetermined spectral response of the photonic devices to be processed. A location specific thickness correction may be performed in accordance with the thickness correction map.
- this location specific thickness correction may not result in a device layer thickness that is as uniform as possible, but it results in a device layer thickness that is tuned for obtaining optimal device performance.
- the photonic devices may be processed, using e.g. optical lithography steps and dry etching steps. This beneficially leads to devices with uniform spectral response over the wafer.
- a post-pattern thickness correction of the device layer e.g., of a SOI substrate
- a thickness correction is done after fabrication of the photonic devices.
- FIG. 3 This example is schematically illustrated in FIG. 3 .
- a characterization of the local linewidth, etch depth and thickness of the fabricated structures may be performed as a function of the spatial wafer coordinates.
- the spectral response of the photonic devices can be measured.
- a thickness correction map may be generated. This thickness correction map may then be used to perform a location specific thickness correction.
- the ion beam may damage a surface portion of the silicon layer, extending about 10 nm to 20 nm from the silicon surface.
- the nature of this damage is twofold, firstly structural damage and secondly chemical damage. In the photonic devices, these damages may lead to absorption and scattering of propagating light, resulting in undesirable propagation losses.
- a thermal annealing step can be performed.
- the thermal annealing step may preferably be performed at a temperature above 600° C., e.g. at a temperature in the range between 800° C. and 1000° C., during 10 to 30 minutes. For higher annealing temperatures shorter annealing times can be used. It was shown that such thermal annealing step can reduce propagation losses by a factor of 10 and or more.
- the initial thickness of the device layer e.g. silicon layer
- the device layer can be increased by epitaxial growth before performing the location specific thickness correction according to the present disclosure, for example when the minimum initial thickness of the device layer is smaller than an optimum thickness of the device layer.
- FIG. 4 This example is schematically illustrated in FIG. 4 , where the device layer is assumed to be a silicon layer, e.g. a top layer of a silicon-on-insulator substrate.
- FIG. 4 schematically shows a diagram illustrating an example method of the present disclosure.
- a first aspect (( 1 ) in FIG. 4 ) an initial silicon thickness map of an incoming wafer is first established.
- the silicon layer thickness t Si can be described as a distribution ⁇ (x,y,T) where x and y are the spatial wafer coordinates and where T is the time.
- an optimum silicon thickness t Si — opti for obtaining a predetermined spectral response may be determined as a function of the spatial wafer coordinates x and y.
- the silicon thickness t Si — opt for the photonic devices to be fabricated is smaller than the minimum initial thickness t Si — min of the silicon layer, the silicon thickness can be increased by growth of an epitaxial silicon layer with thickness ⁇ t, and the location specific thickness correction (e.g., by a GCIB process) according to the present disclosure can be performed on the thickened wafer. If the optimum silicon thickness t Si — opti is larger than the minimum initial thickness t Si — min over the entire wafer, the method according to the present disclosure can be performed on the incoming wafer, without thickening by epitaxial growth.
- the wafer is processed first and a map of silicon thickness t Si , linewidth w and etch depth d is established as a function of the spatial wafer coordinates x and y.
- the optical response of the photonic devices may then be determined (e.g., insertion loss IL, bandwidth BW, ⁇ max , and so forth), and a map of optimum silicon thickness t Si — opti may be determined for optimized optical response.
- the difference between the initial silicon layer thickness t Si and the optimum silicon layer thickness t Si — opti corresponds to the amount of silicon that needs to be etched locally during the corrective etch process.
- the silicon thickness can be increased by growth of an epitaxial silicon layer with thickness ⁇ t, and the location specific thickness correction (e.g., by a GCIB process) according to the present disclosure can be performed on the thickened wafer. If the optimum silicon thickness t Si — opti is larger than the minimum initial thickness t Si — min over the entire wafer, the method according to the present disclosure can be performed on the incoming wafer, without thickening by epitaxial growth.
- a key parameter for fiber grating couplers is the wavelength ⁇ max at which maximum coupling is achieved between a fiber and an integrated waveguide on the substrate.
- ⁇ max ⁇ 0 + ⁇ *t Si +b*w+c*d where a, b and c are fitting parameters.
- ⁇ max is 1567 nm with a standard deviation of 3.9 nm wafer-to-wafer within a lot. Based on long term lot-to-lot repeatability measurements, it was found that the average ⁇ max can vary from 1552 nm up to 1578 nm, which is a difference of up to 26 nm.
- the method 500 includes, at step 502 , establishing an initial device layer thickness map for the predetermined area. Further, the method 500 includes, at step 504 , establishing a linewidth map for the predetermined area and, at step 506 , establishing an etch depth map for the predetermined area. Still further, the method 500 includes, at step 508 , based on (a) the initial device layer thickness map, (b) the linewidth map and (c) the etch depth map, calculating an optimal device layer thickness map and a corresponding thickness correction map for the predetermined substrate area, taking into account photonic device design data. Yet still further, the method 500 includes, at step 510 , performing a location specific corrective etch process in accordance with the thickness correction map.
- a system for improving the uniformity over a predetermined substrate area of a spectral response of photonic devices fabricated in a thin device layer may be provided.
- the system may be configured to (i) establish an initial device layer thickness map for the predetermined area, (ii) establish a linewidth map for the predetermined area, and (iii) establish an etch depth map for the predetermined area.
- the system may further be configured to, based on the initial device layer thickness map, the linewidth map and the etch depth map, calculate an optimal device layer thickness map and a corresponding thickness correction map for the predetermined substrate area taking into account photonic device design data.
- the system may be configured to perform a location specific corrective etch process in accordance with the thickness correction map.
- the system may include a processor and data storage, each of which may take various forms.
- the processor could be one or more general purpose microprocessors and/or dedicated signal processors.
- data storage could be volatile and/or non-volatile memory, such as flash memory.
- the data storage may comprise instructions executable by the processor to (i) establish an initial device layer thickness map for the predetermined area, (ii) establish a linewidth map for the predetermined area, (iii) establish an etch depth map for the predetermined area, (iv) based on the initial device layer thickness map, the linewidth map and the etch depth map, calculate an optimal device layer thickness map and a corresponding thickness correction map for the predetermined substrate area taking into account photonic device design data, and (v) initiate or perform a location specific corrective etch process in accordance with the thickness correction map.
- the system may comprise an etch apparatus configured to perform a location specific corrective etch process in accordance with the thickness correction map.
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Abstract
Description
λmax=λ0 +α*t Si +b*w+c*d
where a, b and c are fitting parameters.
λmax≅1300.9+1931.8*t Si−205.2*w−1151.1*d
wherein λmax, tSi, w and d are expressed in nm.
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US8953239B2 (en) | 2012-09-05 | 2015-02-10 | University Of Utah Research Foundation | Nanophotonic scattering structure |
US20170005013A1 (en) | 2015-06-30 | 2017-01-05 | Varian Semiconductor Equipment Associates, Inc. | Workpiece Processing Technique |
WO2025054334A1 (en) * | 2023-09-06 | 2025-03-13 | Quantinuum Llc | Systems, apparatuses, and methods for film thickness control for integrated photonics |
DE102023130181A1 (en) * | 2023-10-31 | 2025-04-30 | Q.ant GmbH | Method for producing an integrated photonic circuit and an integrated photonic circuit |
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