FR2766169A1 - THERMOPLASTIC CONTAINER DEFLECTION STERILIZATION INSTALLATION - Google Patents

Abstract

Installation for sterilization in the process of preforms intended for the manufacture, by blow molding or stretch blow molding, of sanitized containers made of thermoplastic material, comprising: a station 25 for rinsing the interior and exterior of the inverted preforms 28, then for draining 29 of the rinsed preforms; a sterilization station 34 with filling means 36 to the brim with the preforms straightened with sterilizing product, and means 35, 38, 41 for moving the preforms for at least the time necessary for sterilization of the internal wall of the preforms in contact sterilizing liquid; an emptying and drying station 40 for the returned preforms with internal and external spraying of a pressurized gas to discharge traces of liquid; finally means 55 for straightening the sterilized preforms and taking them to the next station.

Description

Sterilization installation on parade of preforms of thermoplastic containers.

 The present invention relates to the field of packaging liquids in containers under sterile conditions and, more particularly, the invention relates to improvements made during the sterilization stage of the containers upstream from the filling-capping station.

 A major drawback presented by the process of sterilizing the very containers intended to contain the sterile liquid resides in the large developed surface presented by each container, and therefore in the relatively large quantity (proportional to the surface to be treated) of sterilizing product which must be sprayed (internally and externally) on the container. However, although the sterilizing product (generally liquid) is recycled after each use and then reused, it is relatively expensive: the treatment of the containers themselves therefore requires the expensive implementation, in sterilizing product and in material, of a large reserve sterilizer product, associated with a pumping and projection circuit at high flow, and a large capacity recycling device for the used product.

 Under these conditions, the invention aims to improve the sterilization installation associated with a packaging of sterile liquid in containers made of thermoplastic material, such as polyethylene terephthalate (PET), not by treating the containers themselves immediately by upstream of the filling-capping station, but by processing, much higher in the production line, the preforms intended for the manufacture of said containers by a blowing or stretch-blowing operation.

 Admittedly, in an installation designed on such a base, it is necessary to maintain in a sterile atmosphere all the treatment stations included between the preform sterilization installation up to the filling station filling station (in other words in particular the installation of sterilization itself, the preform heating ovens, the blowing or stretch-blowing installation producing the containers, possibly additional devices such as accumulators of sterilized preforms or containers, the filling-capping installation, as well as all means of transfer from one position to another).

 However, the realization of a global installation thus designed does not pose any major difficulty: the preform and receptacle processing stations can be closed, the transfer means can also be closed by cowlings (tunnels), and the atmosphere sterile can be maintained by overpressure by blowing air (or a gas) treated to sterilize it.

 Under these conditions, the purpose of the invention is more particularly to propose a system for sterilizing the preforms of thermoplastic material intended for the production, by blow molding or stretch blow molding, of sanitized containers which must be filled with a sterile liquid.

To this end, such an installation is essentially characterized, being arranged in accordance with the invention, in that it comprises a) a station for rinsing the parade of
preforms arranged neck down, comprising means for
projection of a rinse aid, inside and outside
outside of the preforms, then for draining
rinsed preforms b) transfer means for removing said preforms
leaving the rinsing-draining station and bring them to the
next post, while straightening them to bring them col
above said next item; c) a sterilization station at the parade of preforms available
necks up, including filling means
preforms to the brim with sterilizer, then
transfer means suitable for moving the said
preforms filled for at least a period of time
preset to provide sterilization of the
inner wall of preforms in contact with liquid
sterilizer, d) an emptying and drying station receiving the preforms
fulfilled, including
- means for turning the preforms for
place the neck down to empty them of the product
sterilizer and
means for spraying gas under pressure a
the outside and inside of each preform and
spraying gas under pressure to discharge the liquid
sterilizer remaining on the outer walls and
internal of the preform towards the opening of the
preform, e) finally means for transferring and turning
preforms to recover preforms sterilized with
exit from the emptying and drying station and take them away,
turning them upside down, towards a
next heating and blowing installation or
stretch blow molding for the manufacture of containers.

 Preferably, separation means partition said rinsing station and the following sterilization station located in the sterile zone, said separation means being arranged to be traversed by the transfer means, and sterile air circulation means are provided for cause an air flow from the drying compartment to the rinsing station from where it is evacuated, in particular by suction.

 Preferably also, means are provided for moving pressurized gas spraying means arranged to move the latter from the bottom of the preform to the opening of the preform in order to gradually discharge the sterilizing liquid onto the walls of the preform. .

 Advantageously, the rinsing and draining station and the emptying and drying station each comprise at least one rotating wheel for supporting the preforms on at least a fraction of a turn which is rinsed and draining, respectively emptying and drying, the two rotating wheels can be designed identically.

 In a first possible exemplary embodiment, it is envisaged that the sterilization station comprises at least one rotating wheel for supporting the preforms on at least a fraction of a turn of rotation from which the preforms are filled to the brim and maintained preforms in the filled state during the aforementioned predetermined duration of time specific to sterilization, said wheel having a diameter and a rotation speed suitable for obtaining said predetermined duration of transfer to the emptying and drying station.

 To reduce the bulk when the sterilization time is significant (for example of the order of 60 to 100 seconds in practice), it is possible, according to a second embodiment, to have recourse to the fact that the sterilization station comprises a wheel support for preforms, on a fraction of a turn which fills to the brim, then transfer means for the preforms filled with a vertical displacement component towards the emptying and drying station located at a level different from the filling station. In this case, it is in practice required that the transfer means with vertical displacement component are, at one and / or the other of their ends, associated with substantially horizontal transfer means so as to confer duration of predetermined sterilization. It is also conceivable that the transfer means with a vertical displacement component comprise several successive stages.

 Provision may be made for the means for projecting rinse aid to the outside of the preforms comprising at least two jets ramps extending in a helix, located face to face on each side of the path followed by the preforms.

 It is also possible to provide that the means for spraying gas inside the preform for drying the internal wall comprise a cannula having a diameter slightly smaller than the internal diameter of the preforms, said cannula forming, in conjunction with the internal wall of the preforms, a venturi accelerating the gas flow and making more efficient the delivery of liquid on the wall of the preforms.

 It can also be provided that the means for spraying gas outside each preform for drying the external wall comprise external blowing means in the form of a clamp surrounding the preform.

In the case where this arrangement is combined with the previous one, it is desirable for said gas blowing means inside and outside the preform to be vertically movable in a mutually enslaved manner, so that one achieves a complete evacuation of the sterilizing liquid present on the internal and external walls of the preform and an effective ejection of the final drops of liquid on the edge of the rim of the preform, in particular in conjunction with the start of the inversion operation of the preform this.

The invention will be better understood on reading the detailed description which follows of certain preferred embodiments given solely by way of nonlimiting examples. In these drawings, reference is made to the accompanying drawings in which
- Figure 1 is a schematic plan view of the entire installation for bottling a sterile liquid, from the arrival of the preforms to the outlet of the filled and capped containers;
- Figures 2 and 3 are schematic views from above respectively of a first and of a second embodiment of a sterilization installation entering the bottling installation shown in Figure 1
- Figures 4 and 5 are diagrams illustrating the operating mode respectively of the rinsing station at the entrance to the installation of Figures 2 and 3 and the drying station at the exit of the installation of Figs. 2 and 3; and
FIGS. 6 and 7 are schematic views, respectively from the side and from above, illustrating the constitution and the operating mode of a device for drying the preforms at the outlet of the installation of FIGS. 2 and 3.

 Referring first to Figure 1, there is shown an example of installation of bottling sterile liquid product using a preform sterilization installation according to the invention.

 The installation includes a hopper 1 for receiving the preforms brought in loose (arrow 2) which is followed by a slide 3 delivering the preforms one after the other, neck at the top, itself followed by a device for step 4 spacing the preforms by a predetermined step. A conveyor 5 then brings the preforms to a sterilization installation 6 which will be discussed in more detail below.

 At the outlet of the sterilization installation 6, a conveyor 7 brings the sterilized preforms into an installation 8 for the production of the containers which comprises in particular an oven 9 for heating the preforms followed by a blow-molding or stretch-blow molding machine 10 producing containers with the required shape. These are then evacuated by a conveyor 11, possibly through additional devices such as a storage device 12 forming a buffer between the blowing machine and the next station, up to a filling machine 13. This comprises in particular a station 14 for filling the containers followed by a station 15 for capping the filled containers, which receives plugs from an ancillary installation 16 provided with a receiving funnel 17, a sorter 18, a machine 19 for sterilizing the plugs and for a conveyor 20 for supplying the plugs to the plugging station 15.

 Finally, the filled and capped containers are evacuated (arrow 21) by a conveyor 22 leaving the filling machine 13.

 It will be noted that the installation is maintained in a sterile atmosphere from the sterilization installation 6 to the exit of the containers from the filling machine 13, including the transporters. As can be clearly seen in FIG. 1, all the workstations are closed and the conveyors are hooded (tunnel conveyor), and the interior spaces are for example kept under overpressure by injecting pre-treated air flow (treatment machine not shown).

 As regards more specifically the sterilization machine 6, it comprises, as illustrated in FIG. 2, immediately after the entry 23 of the preforms brought up by the conveyor 5, a rinsing station 25 arranged for rinsing with parade of preforms. This station can include a rotating wheel 26 provided on its periphery with gripping and preform support members.

 On either side of the trajectory 26 in an arc followed by the preforms 28, means 27 for spraying a rinsing product are disposed (for example a composition based on hydrogen peroxide marketed under the name OXONIA active or peracetic acid) on the external surface of the preforms being scrolled; preferably, to be sure of covering the entire external surface of the preforms, the projection means 27 comprise at least two sets or ramps of projection nozzles which are arranged in inclined alignments on the horizontal (arrangement in helix section ) and which are located face to face on each side of the path followed by the preforms 28. To be sure that the preforms 28 are correctly rinsed externally and therefore correctly receive the jets of liquid projected by the means 27, the support wheel 25 is arranged to support the preforms 28 angularly spaced from each other with a relatively large pitch as shown clearly in Figure 2, this external rinsing may be the only treatment performed on the external face of the preforms during the sterilization process.

 Simultaneously, rinse aid is sprayed inside the preforms (vertical jets of rinse aid and / or rinse cannulas introduced into each preform) to rinse the interior surface.

 In addition, so that the rinse product polluted by contact with the surface of the preforms does not stagnate therein and simply flows by gravity without any other operation, the preforms are treated in the neck down position. To this end, the wheel 25 is arranged so that the preforms 28, as soon as they are placed thereon in the feeding position with the neck at the top, are turned over at 24 to be arranged neck at the bottom and then be rinsed in this position. At the outlet of the rinsing, the preforms are kept neck down to facilitate the draining of the rinsing product at 29, then they are turned over at 30 to be brought back to the neck up position before leaving this rinsing station. draining.

 In FIG. 4, the various phases of the process which has just been commented on are very schematically represented by angular sectors with different hatching, the angular lengths of these sectors being representative of the relative durations of the phases; the same numerical references as in FIG. 2 have been kept (reference 27 being here used to designate the whole of the rinsing, internal and external).

 Given the large splashes of liquid occurring during this phase, a rollover 31 can surround the path followed by the preforms.

 It will be noted that the rinsing step constitutes a simple operation for preparing the preforms, intended to remove the bulk of the impurities and preceding the sterilization operation proper. Therefore, a separation (partition 33) is provided between the rinsing station and the sterile downstream part of the circuit followed by the preforms, and in particular the sterilization station which immediately follows it, to prevent the air flow mentioned above , which circulates from a drying station (located downstream near the outlet of the sterilization installation 6 of which question below) towards the rinsing station 25, does not return to the stations located in front where the preforms are more more clean.

 At the outlet of the wheel 25, the rinsed preforms 28 are transferred by a conveyor 32, which passes through the sealed partition 33, into the sterilization station 34 proper. Because the sterilization treatment is carried out mainly on the single internal wall of the preforms 28, the preforms can be spaced, here, by a smaller step and the conveyor 32 is arranged to bring the preforms closer to one another as it appears clearly in Figure 2.

 The sterilization treatment consists in maintaining the internal wall of the preforms with a sterilization product for at least a predetermined duration. By way of example and to fix ideas, the preforms (which are arranged in the neck-up position) are filled to the brim with a solution of a sterilization product, such as hydrogen peroxide (active OXONIA) or peracefic acid, and are kept filled for a period of about 80 seconds. Since the entire packaging of the preforms is carried out in line with the blowing and filling stations, it is necessary that the steps of filling, sterilization and emptying of the preforms also take place during the parade while the preforms are moving. Thus, the preforms filled with sterilizer must be moved, with the same speed as in the entire installation, for the predetermined time necessary for sterilization (for example 80 seconds) before being emptied.

 This displacement can be carried out by any means known to those skilled in the art, capable of avoiding shaking so that the preforms remain filled to the brim and that the neck drinker also undergoes the sterilization process in a perfect manner. However, it is understandable that a linear conveyor, or even a serpentine trajectory, is a large consumer of space; as such, it is desirable to consider less expensive solutions.

 A first embodiment, illustrated in FIG. 2, consists in using a rotary conveyor in which a horizontal succession of circular trajectories or in suitably arranged arcs of circle makes it possible to reduce the space requirement on the ground while providing the required developed trajectory . In the example shown in Figure 2, the preforms 28 supplied by the conveyor 32 are transferred to a support wheel 35 of large diameter. After their filling at 36 carried out at the start of their rotary course, the filled preforms perform approximately three-quarters of a turn, then are taken up by a transfer wheel 37 and repositioned on a second support wheel 38 which, in the example considered, is identical to the wheel 35 and of the same diameter. After a course of approximately three-quarters of a turn on the wheel 38, the preforms are transferred to a conveyor 39 which brings them to a dumping station 40.

 Of course, the configuration of the wheels can be adapted according to the space available and the duration of the sterilization process. A single wheel of very large diameter may be suitable if a square space of sufficient size can be reserved for this function; a larger number of wheels (three, four, ...) can be envisaged if the duration of the treatment is long, with however, during transfers, an increased risk of vibrations or shocks of the preforms, overflow of the liquid and therefore of a sterile less reliable around the drink of the preforms.

 Another possible embodiment, represented in FIG. 3, consists in associating one or more rotary conveyors situated on different levels with, between them, a vertical conveyor. In FIG. 3, the same reference numerals have been kept to designate the parts or members identical to those of FIG. 2. The rinsing station 25 is arranged in the same way as in the installation of FIG. 2 and is separated from the next post by a partition 33 crossed by the conveyor 32 (here two screw conveyors in series). The preforms 28 are transferred to a wheel 35 of relatively large diameter and are filled, at the start of the rotary path at 36, with sterilizing liquid. After a course of approximately three-quarters of a turn, they are transferred to an elevating device designated as a whole by the reference 41.

 The lifting device 41 can be of any type known to those skilled in the art, suitable for vertically transferring the preforms from one level to another different level, for example to a higher level. An example of a lifting device suitable for use in the context of the installation of FIG. 3 is that which is the subject of the joint patent application, entitled "Device for continuous vertical transfer of containers", filed on the same day. in the name of the Applicant. In short, this lifting device essentially consists of a rotary plate 42 at the periphery of which the preforms are supported by supports which are movable vertically, between a low position (for example level of zone 35 in FIG. 3) and a position high, by cooperation with a cam in an arc of an ascending profile (portion of course 43). For example, the supports may be integral with vertical rods supported with free vertical sliding by the above-mentioned plate 41, the lower end of these rods being in abutment against the above-mentioned cam. In Figure 3, there is shown only the parts of the installation located in the lower part, while in Figure 3A are shown only the bodies located in the upper part.

 Arrived at the high level (FIG. 3A), the preforms are transferred to a second wheel 38 which is coaxial with the wheel 35 and integral in rotation with the latter, and which can have substantially the same diameter.

 After a path of about three-quarters of a turn of the wheel 38, the preforms are taken up by a conveyor 39 (here a set of two screw conveyors in series) and brought to the emptying / drying station 40 which, in this mode of achievement, is therefore located at the high level.

 The use of a lifting device such as that which has just been described briefly (reference may be made to the aforementioned document for more complete information) allows a considerable saving of space due to the superposition of the wheels 35 and 38, a simplification of the mechanisms for driving said wheels in rotation due to their coaxiality (the same is true for transfer wheels on the two levels), and finally a possibility of multiplying the number of stages to increase the duration of transfer of the preforms up to at the emptying / drying station and / or for superimposing stations (for example placing the emptying / drying station above the wheels 35, 38).

 It will also be noted that the use of an elevating device of the aforementioned type safeguards the reliability of the sterilization treatment in the event of the liquid filling the preforms overflowing: the preforms at the end of treatment are at the upper level and cannot be polluted, while their overflow causes a flow of polluted liquid in the preforms located at the lower level and which are only at the beginning of the sterilization treatment.

 As regards the emptying / drying station 40, reference will now be made either to FIGS. 2 or 3A. This station is arranged for emptying and drying the parades of the preforms which are brought to it, neck up, filled with the sterilizing liquid. The station 40 can be arranged, in general, on the same model as the above-mentioned rinsing station 25. A wheel 44, which can be analogous to the wheel 26 of the rinsing station 25, receives the preforms 28 on mobile support members which are tilted at 45 to reverse the preforms and bring them into the neck down position.

 Thereafter, each preform 28, emptied, is dried by blowing a gas, in particular air, previously treated, possibly hot. This operation extends over at least half a revolution of the wheel 44.

To this end, it is advantageous to have recourse to the means illustrated in FIGS. 6 and 7.

 To dry the external wall of the preform, an external drying device 46 in the form of a U-shaped clamp is used, surrounding the preform 28 and projecting onto it several air jets 47. The device 46 is movable vertically and is first of all brought up to the bottom of the preform, located at the top, then is lowered along the preform (arrow 48) to first dry the body of the preform (phase 49 in Figures 2 and 3A), then finally the neck of the preform (phase 50 in FIGS. 2 and 3A).

 To dry the internal wall of the preform, an internal drying device in the form of a cannula 51 is used which is introduced into the preform and which delivers an annular jet of pressurized air 52. The cannula 51 is first brought to the bottom of the preform, then lowered (arrow 53) along the body of the preform to dry it first (phase 49 in Figures 2 and 3A), then finally the neck of the preform (phase 50 in the figures 2 and 3A).

 The movements of the U-shaped clamp 46 and the cannula 51 are synchronized and can be subject to a common motor member.

 It will also be noted that at its base 54, the cannula has an enlarged diameter close to the internal diameter of the preform so that the opposite faces of the base 54 of the cannula and of the internal wall of the preform define an annular narrowing forming Venturi annular. An acceleration zone of the annular air flow is thus obtained which is favorable for effectively repelling the liquid towards the neck of the preform.

 Finally the sterilized and dry preform is again turned over (phase 55 in FIGS. 2 and 3A) to be brought back up, before being taken up by a conveyor 7 which takes it to the oven.

 Note that the inversion operation (phase 55) of the preforms begins while the drying devices 46 and 51 are still in action at the neck. Thus, the last drops of discharged liquid appear on the collar of the collar while the preform begins to be inclined and then slide along the collar towards the lower part of it to be finally detached and projected by the air jets without risk hitting the opposite wall of the preform: this ensures complete and effective drying.

 To better define the ideas, a diagram has been shown in FIG. 5, established in the same manner as that of FIG. 4, which gives the exact relative durations of the various emptying / drying operations, the numerical references appearing in FIGS. 2 and 3A being included here.

 It will also be noted that the operation of drying the preforms from the outside requires increased spacing of the preforms: the conveyor 39 is therefore arranged to modify this pitch between the exit from the sterilization station and the entry from the emptying / drying station.

 Means for circulating sterile air (not shown in FIG. 1) are also provided to cause an air flow against the direction of movement of the preforms, from the drying station 40 to the rinsing station 25 of where it is evacuated, in particular by aspiration. This avoids displacements of non-sterile air towards the final station where the preforms are sterile.

 As is obvious and as already follows from the above, the invention is in no way limited to those of its modes of application and embodiments which have been more particularly envisaged; on the contrary, it embraces all its variants.

Claims (12)

 1. Installation for sterilization in the process of preforms intended for the manufacture, by blowing or stretch-blowing, of aseptic containers made of thermoplastic material, characterized in that it comprises a) a station (25) for rinsing in the process of  preforms (28) arranged neck down, comprising  means (27) for spraying a rinsing product,  inside and outside of the preforms and then for  the draining (29) of the rinsed preforms b) transfer means for removing said preforms  leaving the rinsing-draining station and bring them to the  next post, while straightening them (30) for  bring neck up to said station following c) a station (34) for sterilization in the process of the preforms  neck collar at the top, including filling means  sage (36) of preforms to the brim in sterilized product  tor, then transfer means (35, 38; 35, 38, 41)  suitable for displacing said preforms filled during  minus a predetermined duration of time suitable for providing  sterilization of the inner wall of the preforms at  sterilizer liquid contact, d) an emptying and drying station (40) receiving the  filled preforms, comprising - means (45) for turning over the preforms for the  place the neck down to empty them of the product  sterilizer and - means (46, 51) for spraying gas under pressure at  the outside and inside of each preform and  spraying gas under pressure to discharge the liquid  sterilizer remaining on the outer walls and  internal of the preform towards the opening of the  preform, e) finally means (55) for transferring and turning  preforms to recover preforms sterilized with  exit from the emptying and drying station and take them away,  turning them upside down, towards a  next heating and blowing installation or  stretch blow molding for the manufacture of containers.  2. Sterilization installation according to claim 1, characterized in that separation means (33) partition said rinsing station (25) and the following sterilization station (34) located in a sterile zone, said separation means being arranged for be crossed by the transfer means, and in that sterile air circulation means are provided to cause an air flow from the drying station (40) to the rinsing station (25) from where it is evacuated, in particular by aspiration.  3. Sterilization installation according to any one of the preceding claims, characterized in that means are provided for moving means (46, 51) for spraying pressurized gas arranged to move the latter from the bottom of the preform (28 ) until the preform opens to gradually push the sterilizing liquid back onto the walls of the preform.  4. Sterilization installation according to any one of the preceding claims, characterized in that the rinsing and draining station (25, 29) and the emptying and drying station (40) each comprise at least one wheel rotary (25, 44) for supporting the preforms on at least a fraction of a rotational rotation from which rinsing and draining takes place, respectively emptying and drying.  5. Sterilization installation according to any one of the preceding claims, characterized in that the sterilization station (34) comprises at least one rotating wheel (35, 38) for supporting the preforms on at least a fraction of a rotation turn of which is carried out filling (36) to the brim with the preforms and maintaining the preforms in the filled state during the said predetermined period of time specific to sterilization, said wheel having a diameter and a rotation speed specific to the obtaining said predetermined transfer time to the emptying and drying station (40).  6. sterilization installation according to any one of claims 1 to 4, characterized in that the sterilization station (34) comprises a rotating wheel (35) for supporting the preforms, on a fraction of a rotation turn of which s' performs the filling (36) to the brim, then means (41) for transferring the preforms filled with a vertical displacement component towards the emptying and drying station (40) located at a level different from the filling station.  7. Sterilization installation according to claim 6, characterized in that the means (41) for transfer with vertical displacement component are, at one and / or the other of their ends, associated with transfer means substantially horizontal (38) so as to confer the predetermined sterilization time.  8. Sterilization installation according to claim 7, characterized in that the transfer means with vertical displacement component (41) comprise several successive stages.  9. Sterilization installation according to any one of the preceding claims, characterized in that the means (27) for projecting rinse aid outside the preforms comprise at least two jets ramps extending in a helix, located opposite opposite each side of the path followed by the preforms.  10. Sterilization installation according to any one of the preceding claims, characterized in that the means for spraying gas inside each preform for drying the internal wall comprise a cannula (51) having a diameter slightly less than the internal diameter of the preforms (28), said cannula (51) forming, in conjunction with the internal wall of the preforms, a venturi accelerating the flow of gas and making more efficient the delivery of liquid on the wall of the preforms.  11. Sterilization installation according to any one of the preceding claims, characterized in that the means (46) for spraying gas outside each preform for drying the external wall comprise external blowing means in the form of forceps surrounding the preform.  12. Sterilization installation according to any one of the preceding claims, characterized in that said means (46, 51) for blowing gas inside and outside the preform are vertically movable in a mutually controlled manner.