US4825684A - Method of testing semiconductor pressure sensor - Google Patents
Method of testing semiconductor pressure sensor Download PDFInfo
- Publication number
- US4825684A US4825684A US07/110,863 US11086387A US4825684A US 4825684 A US4825684 A US 4825684A US 11086387 A US11086387 A US 11086387A US 4825684 A US4825684 A US 4825684A
- Authority
- US
- United States
- Prior art keywords
- semiconductor pressure
- pressure sensor
- wafer
- wafer stage
- testing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000004065 semiconductor Substances 0.000 title claims abstract description 83
- 238000010998 test method Methods 0.000 title claims description 13
- 230000035945 sensitivity Effects 0.000 claims abstract description 20
- 239000000523 sample Substances 0.000 claims description 14
- 239000000463 material Substances 0.000 claims description 8
- 239000011148 porous material Substances 0.000 claims description 5
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 claims description 4
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims description 4
- 229920003002 synthetic resin Polymers 0.000 claims description 4
- 239000000057 synthetic resin Substances 0.000 claims description 4
- 239000005062 Polybutadiene Substances 0.000 claims description 2
- 239000011521 glass Substances 0.000 claims description 2
- 229910052751 metal Inorganic materials 0.000 claims description 2
- 239000002184 metal Substances 0.000 claims description 2
- 229920002857 polybutadiene Polymers 0.000 claims description 2
- 239000003566 sealing material Substances 0.000 claims description 2
- 229920002379 silicone rubber Polymers 0.000 claims description 2
- 239000004945 silicone rubber Substances 0.000 claims description 2
- 229920005989 resin Polymers 0.000 claims 1
- 239000011347 resin Substances 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 18
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 6
- 229910052710 silicon Inorganic materials 0.000 description 6
- 239000010703 silicon Substances 0.000 description 6
- 238000005259 measurement Methods 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- 239000013078 crystal Substances 0.000 description 3
- 238000009792 diffusion process Methods 0.000 description 3
- 238000003825 pressing Methods 0.000 description 3
- 230000007423 decrease Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000002344 surface layer Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 239000004793 Polystyrene Substances 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000005468 ion implantation Methods 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 230000008447 perception Effects 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01L—MEASURING FORCE, STRESS, TORQUE, WORK, MECHANICAL POWER, MECHANICAL EFFICIENCY, OR FLUID PRESSURE
- G01L9/00—Measuring steady of quasi-steady pressure of fluid or fluent solid material by electric or magnetic pressure-sensitive elements; Transmitting or indicating the displacement of mechanical pressure-sensitive elements, used to measure the steady or quasi-steady pressure of a fluid or fluent solid material, by electric or magnetic means
- G01L9/08—Measuring steady of quasi-steady pressure of fluid or fluent solid material by electric or magnetic pressure-sensitive elements; Transmitting or indicating the displacement of mechanical pressure-sensitive elements, used to measure the steady or quasi-steady pressure of a fluid or fluent solid material, by electric or magnetic means by making use of piezoelectric devices, i.e. electric circuits therefor
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01L—MEASURING FORCE, STRESS, TORQUE, WORK, MECHANICAL POWER, MECHANICAL EFFICIENCY, OR FLUID PRESSURE
- G01L9/00—Measuring steady of quasi-steady pressure of fluid or fluent solid material by electric or magnetic pressure-sensitive elements; Transmitting or indicating the displacement of mechanical pressure-sensitive elements, used to measure the steady or quasi-steady pressure of a fluid or fluent solid material, by electric or magnetic means
- G01L9/0041—Transmitting or indicating the displacement of flexible diaphragms
- G01L9/0051—Transmitting or indicating the displacement of flexible diaphragms using variations in ohmic resistance
- G01L9/0052—Transmitting or indicating the displacement of flexible diaphragms using variations in ohmic resistance of piezoresistive elements
- G01L9/0054—Transmitting or indicating the displacement of flexible diaphragms using variations in ohmic resistance of piezoresistive elements integral with a semiconducting diaphragm
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01L—MEASURING FORCE, STRESS, TORQUE, WORK, MECHANICAL POWER, MECHANICAL EFFICIENCY, OR FLUID PRESSURE
- G01L9/00—Measuring steady of quasi-steady pressure of fluid or fluent solid material by electric or magnetic pressure-sensitive elements; Transmitting or indicating the displacement of mechanical pressure-sensitive elements, used to measure the steady or quasi-steady pressure of a fluid or fluent solid material, by electric or magnetic means
- G01L9/02—Measuring steady of quasi-steady pressure of fluid or fluent solid material by electric or magnetic pressure-sensitive elements; Transmitting or indicating the displacement of mechanical pressure-sensitive elements, used to measure the steady or quasi-steady pressure of a fluid or fluent solid material, by electric or magnetic means by making use of variations in ohmic resistance, e.g. of potentiometers, electric circuits therefor, e.g. bridges, amplifiers or signal conditioning
- G01L9/06—Measuring steady of quasi-steady pressure of fluid or fluent solid material by electric or magnetic pressure-sensitive elements; Transmitting or indicating the displacement of mechanical pressure-sensitive elements, used to measure the steady or quasi-steady pressure of a fluid or fluent solid material, by electric or magnetic means by making use of variations in ohmic resistance, e.g. of potentiometers, electric circuits therefor, e.g. bridges, amplifiers or signal conditioning of piezo-resistive devices
Definitions
- the present invention relates to a method of testing a semiconductor pressure sensor and more specifically to a method of testing the pressure sensitivity of a diaphragm type semiconductor pressure sensor typical of a semiconductor pressure sensor fitted to the tip of a catheter for medical use.
- the process of making such a semiconductor pressure sensor comprises the steps of forming strain gauge resistors formed by diffusion of impurity ions on the surface layer of a silicon single crystal, assembling four of the strain gauge resistors into a Wheatstone bridge, forming a recess in the back surface of the silicon single crystal to use a thin portion thereof as a diaphragm, and disposing pads in suitable places on the front surface except for the diaphragm.
- the diaphragm is deformed and the resistance value of the strain gauge resistor changes to a greater extent because of the piezoelectric resistance effect, so that a bridge output proportional to the pressure is obtainable.
- the aforesaid semiconductor pressure sensor is extremely small in size and, particularly in the case of a semiconductor pressure sensor for medical use, a plurality of semiconductor pressure sensors are fitted on the tip of a catheter and inserted into a body. Accordingly, even in a semiconductor pressure sensor incorporating peripheral circuits such as a temperature compensating circuit, a pressure sensitivity compensating circuit and the like, a side of a chip should be about 1 mm or smaller in length.
- the conventional testing method for a semiconductor pressure sensor under the wafer process comprises mounting a wafer of the semiconductor pressure sensor on a wafer stage and making the electrodes built in the surface of the wafer contact a measuring probe without applying pressure so that only electrical measurement is effected.
- an object of the present invention is to provide a method of testing a semiconductor pressure sensor under the wafer process so that the measurement of the pressure sensitivity of the semiconductor pressure sensor can be easily conducted irrespectively of the chip size.
- the method of testing a semiconductor pressure sensor comprises the steps of boring at least one evacuating hole in a wafer stage, evacuating air existing between the back surface side of a diaphragm type semiconductor pressure sensor and the wafer stage through the hole to deform the diaphragm, and measuring the pressure sensitivity of the semiconductor pressure sensor from the surface side of the semiconductor pressure sensor.
- An intermediate member made of porous material may be held between the back surface side of the diaphragm type semiconductor pressure sensors and the wafer stage provided with the evacuating holes to deform all diaphragms facing the intermediate member by making vacuum suction to the semiconductor pressure sensors simultaneously through the holes.
- the wafer is mounted on the wafer stage and the diaphragm is subjected to vacuum suction from the back surface side of the semiconductor pressure sensor by making use of the hole bored in the wafer stage, whereby the diaphragm is subjected to negative pressure and deformed.
- the electrical output of the semiconductor pressure sensor with the diaphragm thus deformed, i.e., the pressure sensitivity of the semiconductor pressure sensor can be measured using the electrodes formed on the surface thereof.
- the negative pressure equivalent to the pressure applied to the surface of the diaphragm is generated through the vacuum suction of the diaphragm at the back surface side and the electrical output is measured, whereby the pressure sensitivity of the semiconductor pressure sensor can be measured under the wafer process.
- the back surface of the wafer is subjected to vacuum suction through the intermediate member made of porous material by utilizing a plurality of holes bored in the wafer stage to deform all diaphragms formed in the semiconductor pressure sensors opposite to the intermediate member by the negative pressure, whereby the electrical output of the semiconductor pressure sensor in that deformed state, i.e., the pressure sensitivity of the semiconductor pressure sensor can be measured from the surface side of the wafer by means of the measuring probe.
- FIG. 1 is a schematic sectional view showing a method of measuring a semiconductor pressure sensor according to a first embodiment of the present invention.
- FIGS. 2(a) and 2(b) are top and elevational sectional views of the semiconductor pressure sensor, respectively.
- FIG. 3 is a diagram showing a stage wherein pressure has been applied to the semiconductor pressure sensor.
- FIG. 4 is an electric circuit diagram showing an electrical arrangement in the semiconductor pressure sensor.
- FIG. 5 is a schematic sectional view showing a method of measuring a semiconductor pressure sensor according to a second embodiment of the present invention.
- FIGS. 2(a) and 2(b) show a semiconductor pressure sensor 1 which is small with a thickness of about 400 ⁇ m.
- Strain gauge resistors 121, 122, 123, 124 are formed by diffusion in the surface layer of a silicon monocrystal 11 and the four strain gauge resistors are connected in series with a diffused lead part 13 which communicates with aluminum (hereinafter Al pads) pads 141, 142, 143, 144 and 145.
- Al pads aluminum pads
- a recess 15 is formed in the back surface of the silicon single crystal 11 and the thin portion thereof (having a thickness less than 30 ⁇ m) used as a diaphragm 16.
- FIG. 1 is a schematic sectional view showing, a method of measuring a semiconductor pressure sensor according to a first embodiment of the present invention, wherein a wafer stage 2 has a vacuum leakage preventing seal material 22 of soft synthetic resin (for example, styrene, butadiene or silicone rubber) with a thickness in order of 10 ⁇ m, which is formed on a plate material 21 of stainless or synthetic resin. Moreover, at least one through-hole 3 is bored in a suitable place of the wafer stage 2 to make vacuum suction to the recess 15 of the semiconductor pressure sensor 1.
- soft synthetic resin for example, styrene, butadiene or silicone rubber
- a measuring probe 4 is located above the throughhole 3 and the recess 15 of the semiconductor pressure sensor 1 and also located above the through-hole 3.
- the measuring probe contracts the Al pads 141, 145 and the Al pad 143 (across the input terminal of a bridge), and the Al pad 142 and the Al pad 141 (across the output terminal of the bridge).
- the wafer 5 may be moved while the wafer stage 2 and the measuring probe 4 are set still or the wafer stage 2 and the measuring probe 4 may be shifted while the wafer 5 is set still.
- the wafer 5 is mounted on the wafer stage 2 and the recess 15 formed in the back surface of the semiconductor pressure sensor 1 is subjected to vacuum suction through the through-hole 3.
- the sealing material 22 on the wafer stage 2 prevents vacuum leakage from the connection portion between the silicon monocrystal 11 and the wafer stage 2.
- the diaphragm 16 is then deformed as in the case where it receives pressure from its surface side so that the pressure sensitivity can be measured, because the negative pressure equivalent to what is applied from its surface side is generated in the recess 15 of the semiconductor pressure sensor 1.
- FIG. 3 shows a state wherein the diaphragm 16 has been deformed.
- the strain gauge resistors 121, 123 diffused in the center of the diaphragm out of the four strain gauge resistors 121, 122, 123 and 124 constituting a bridge circuit shown in FIG. 4 are compressed as the diaphragm 16 deforms and the strain gauge resistors 122, 124 diffused on the periphery of the diaphragm 16 are extended as the diaphragm 16 deforms.
- strain gauge resistors With respect to the strain gauge resistors, use is made of those whose resistance value increases proportionally to the stress. Given the resistance values of the strain gauge resistors 121, 122, 123 and 124 respectively at R1, R2, R3 and R4, R2 and R4 increases whereas R1 and R3 decreases as the diaphragm 16 deforms. In other words, the potential V 1 across the terminals of R2 increases, whereas the potential V 2 across the terminals of R3 decreases.
- the bridge output i.e., V 1 -V 2 increases in proportion to the deformation of the diaphragm 16.
- the pressure sensitivity of the semiconductor pressure sensor 1 can simply be tested irrespective of the chip size, before the wafer 5 is cut out on a chip basis, by measuring the bridge output with the measuring probe 4 using the Al pads of the semiconductor pressure sensor 1.
- the electrical measurement is made from the surface side of the semiconductor pressure sensor 1 and the pressure is applied from the back surface side thereof, whereby the pressure sensitivity of the semiconductor pressure sensor 1 is tested under the wafer process.
- FIG. 5 is a schematic sectional view showing a method of measuring a semiconductor pressure sensor according to a second embodiment of the present invention, wherein like reference characters designate like members of FIG. 1.
- the wafer stage 2 is constructed of a plate material 21 of stainless or synthetic resin and made slightly wider than the bottom surface of a wafer 5.
- a recess 220 slightly smaller than the bottom surface of the wafer 5 is formed in the surface of the wafer stage 2 and an intermediate member 40 is installed in the recess 220, whereas at least one evacuating through-hole 3 is bored in the bottom surface of the recess 220.
- the intermediate member 40 installed in the recess 220 is made of porous material (for example, a foamed metal or glass material or hard foamed material such as polystyrene).
- the wafer 5 is mounted on the intermediate member 40 installed on the wafer stage 2 and vacuum-sucked through the through-hole 3 so that the through-hole 3 and the back surface of the wafer 5 are communicated with each other because of the pores of the intermediate member 40. Accordingly, negative pressure is uniformly generated over the whole back surface of the wafer 5.
- the negative pressure applied to the recesses 15 of all semiconductor sensors 1 formed in the wafer 5 is substantially made uniform.
- the diaphragms 16 formed in all semiconductor pressure sensors can be deformed as in the case where they are subjected to pressure from their surface side and, by making the measuring probe 4 contact the Al pads 144, 145 and the Al pad 143 (across the input terminal of a bridge), and the Al pad 142 and the Al pad 144 (across the output terminal of the bridge), electrical power can be supplied to the bridge and its output (pressure sensitivity) can be measured.
- the present invention is not limited to the aforesaid embodiments.
- the installation of the measuring probe 4 at a position corresponding to each Al pad of all semiconductor pressure sensors formed in the wafer 5 make it possible to measure all semiconductor pressure sensors at once.
- the negative pressure corresponding to the pressure applied to the surface of the diaphragm is produced at the back side of the diaphragm to deform the diaphragm of the semiconductor pressure sensor. This is done by using of the evacuating hole bored in the wafer stage. By measuring the electrical output in this state, the pressure sensitivity of the semiconductor pressure sensor can be measured under the wafer process, whereby the measuring process for a semiconductor pressure sensor is simplified with the effect of reducing production costs.
- the negative pressure corresponding to the pressure applied to the surface of the diaphragm can be produced substantially uniformly over all diaphragms of the semiconductor pressure sensors by using the porous intermediate member. Since the pressure sensitivity thereof can be tested by the measuring probe in the aforesaid state, the wafer need not be moved relatively to the wafer stage, whereby the measuring process for a semiconductor pressure sensor is simplified with the effect of reducing production costs.
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- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Measuring Fluid Pressure (AREA)
- Pressure Sensors (AREA)
Abstract
Description
Claims (7)
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP61-257977 | 1986-10-28 | ||
JP61257976A JPS63110671A (en) | 1986-10-28 | 1986-10-28 | Measurement method of semiconductor pressure sensor |
JP61257977A JPS63110672A (en) | 1986-10-28 | 1986-10-28 | Measurement of semiconductor pressure sensor |
JP61-257976 | 1986-10-28 |
Publications (1)
Publication Number | Publication Date |
---|---|
US4825684A true US4825684A (en) | 1989-05-02 |
Family
ID=26543481
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US07/110,863 Expired - Fee Related US4825684A (en) | 1986-10-28 | 1987-10-21 | Method of testing semiconductor pressure sensor |
Country Status (6)
Country | Link |
---|---|
US (1) | US4825684A (en) |
EP (1) | EP0265816B1 (en) |
KR (1) | KR910001249B1 (en) |
AU (1) | AU595945B2 (en) |
CA (1) | CA1308933C (en) |
DE (1) | DE3772514D1 (en) |
Cited By (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5131259A (en) * | 1991-02-01 | 1992-07-21 | Fel-Pro Incorporated | Calibration fixture and method of calibrating contact sensors |
US5668305A (en) * | 1996-03-29 | 1997-09-16 | Motorola, Inc. | Method and apparatus for over pressure testing pressure sensitive devices on a wafer |
US5677477A (en) * | 1996-02-20 | 1997-10-14 | Motorola, Inc. | Hermetic pressure sensor test chamber |
DE4239132C2 (en) * | 1991-11-20 | 2002-06-06 | Denso Corp | Method of fabricating an integrated pressure sensor |
WO2002101348A1 (en) * | 2001-06-11 | 2002-12-19 | Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e. V. | Method and device for testing or calibrating a pressure sensor on a wafer |
DE10000133C2 (en) * | 2000-01-04 | 2003-06-26 | Karl Suss Dresden Gmbh | Prober for pressure sensors |
US20050116729A1 (en) * | 2001-06-11 | 2005-06-02 | Oliver Koester | Method and device for testing or calibrating a pressure sensor on a wafer |
US20060021418A1 (en) * | 2004-07-27 | 2006-02-02 | Tekscan Incorporated | Sensor equilibration and calibration system and method |
US20060053862A1 (en) * | 2004-08-17 | 2006-03-16 | Felix Mayer | Method and device for calibration sensors |
US20060201232A1 (en) * | 2005-03-08 | 2006-09-14 | Denso Corporation | Inspection device for humidity sensor and method for adjusting sensor characteristics of humidity sensor |
US20060230815A1 (en) * | 2005-04-19 | 2006-10-19 | Borzabadi Hamid R | Leak-testing technique for differential pressure sensor array |
DE102006062222A1 (en) * | 2006-12-22 | 2008-06-26 | Endress + Hauser Gmbh + Co. Kg | Differential pressure sensor, has silicon chip with deformation-dependent resistor units of measuring circuits positioned so that deformation-dependent signals of circuits have different dependency ratios of static and differential pressure |
US20100192266A1 (en) * | 2007-03-12 | 2010-07-29 | Purdue Research Foundation | System and method for improving the precision of nanoscale force and displacement measurements |
US20100310343A1 (en) * | 2009-06-04 | 2010-12-09 | Felix Mayer | Method and apparatus for processing individual sensor devices |
US20110092955A1 (en) * | 2009-10-07 | 2011-04-21 | Purdy Phillip D | Pressure-Sensing Medical Devices, Systems and Methods, and Methods of Forming Medical Devices |
US8643361B2 (en) | 2010-07-14 | 2014-02-04 | Sensirion Ag | Needle head |
US20150135857A1 (en) * | 2012-07-26 | 2015-05-21 | Murata Manufacturing Co., Ltd. | Pressing Force Sensor |
US9366720B2 (en) | 2011-01-27 | 2016-06-14 | Sensirion Ag | Sensor protection |
US10315013B2 (en) | 2001-07-13 | 2019-06-11 | Endophys Holdings, Llc | Sheath with sensing capabilities |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4809536A (en) * | 1986-11-06 | 1989-03-07 | Sumitomo Electric Industries, Ltd. | Method of adjusting bridge circuit of semiconductor pressure sensor |
US7216547B1 (en) * | 2006-01-06 | 2007-05-15 | Honeywell International Inc. | Pressure sensor with silicon frit bonded cap |
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JPS5749276A (en) * | 1980-09-09 | 1982-03-23 | Mitsubishi Electric Corp | Manufacture of semiconductor pressure sensor |
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DE3376760D1 (en) * | 1983-11-10 | 1988-06-30 | Kristal Instr Ag | Transducer element, method for its manufacture and its use in a pressure pick-up device |
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-
1987
- 1987-10-20 EP EP87115355A patent/EP0265816B1/en not_active Expired - Lifetime
- 1987-10-20 DE DE8787115355T patent/DE3772514D1/en not_active Expired - Lifetime
- 1987-10-21 US US07/110,863 patent/US4825684A/en not_active Expired - Fee Related
- 1987-10-23 KR KR1019870011773A patent/KR910001249B1/en not_active IP Right Cessation
- 1987-10-27 CA CA000550325A patent/CA1308933C/en not_active Expired - Lifetime
- 1987-10-27 AU AU80186/87A patent/AU595945B2/en not_active Ceased
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US1302028A (en) * | 1914-07-13 | 1919-04-29 | Westinghouse Electric & Mfg Co | Sheet-handling implement. |
US3224106A (en) * | 1961-05-31 | 1965-12-21 | David G Way | Method and apparatus for use in assembling ring sections about a shaft with their end faces co-planar |
US3608946A (en) * | 1968-11-19 | 1971-09-28 | Dow Chemical Co | Device for handling of a filter membrane |
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DE2628488A1 (en) * | 1976-06-25 | 1978-01-05 | Siemens Ag | Heat- and chemical-resistant ends for suction tongs - are joined to the tube by adjustable locking couplings |
DE2631502A1 (en) * | 1976-07-13 | 1978-01-19 | Siemens Ag | Suction type forceps for small components - have passage from union to nozzle formed by groove covered by plate |
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JPS5433678A (en) * | 1977-08-22 | 1979-03-12 | Hitachi Ltd | Vacuum pincette |
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Cited By (33)
Publication number | Priority date | Publication date | Assignee | Title |
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Also Published As
Publication number | Publication date |
---|---|
EP0265816B1 (en) | 1991-08-28 |
EP0265816A2 (en) | 1988-05-04 |
AU595945B2 (en) | 1990-04-12 |
CA1308933C (en) | 1992-10-20 |
DE3772514D1 (en) | 1991-10-02 |
KR880005446A (en) | 1988-06-29 |
KR910001249B1 (en) | 1991-02-26 |
EP0265816A3 (en) | 1989-06-21 |
AU8018687A (en) | 1988-05-05 |
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