US2453709A - Grinding oil composition - Google Patents
Grinding oil composition Download PDFInfo
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- US2453709A US2453709A US628352A US62835245A US2453709A US 2453709 A US2453709 A US 2453709A US 628352 A US628352 A US 628352A US 62835245 A US62835245 A US 62835245A US 2453709 A US2453709 A US 2453709A
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- grinding
- oil
- wheel
- sus
- steel
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M101/00—Lubricating compositions characterised by the base-material being a mineral or fatty oil
- C10M101/02—Petroleum fractions
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
- C10M2203/1006—Petroleum or coal fractions, e.g. tars, solvents, bitumen used as base material
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
- C10M2203/102—Aliphatic fractions
- C10M2203/1025—Aliphatic fractions used as base material
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
- C10M2203/104—Aromatic fractions
- C10M2203/1045—Aromatic fractions used as base material
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
- C10M2203/106—Naphthenic fractions
- C10M2203/1065—Naphthenic fractions used as base material
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
- C10M2203/108—Residual fractions, e.g. bright stocks
- C10M2203/1085—Residual fractions, e.g. bright stocks used as base material
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/40—Fatty vegetable or animal oils
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/40—Fatty vegetable or animal oils
- C10M2207/404—Fatty vegetable or animal oils obtained from genetically modified species
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
- C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/10—Phosphatides, e.g. lecithin, cephalin
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/22—Metal working with essential removal of material, e.g. cutting, grinding or drilling
Definitions
- Patented Nov. is, 1.948
- the steel gets too hot during such a grinding operation with a worn wheel, the steel becomes discolored.
- the color may or may not indicate a deterioration in the quality of the steel, but it is undesirable commercially.
- it is necessary to redress the grinding wheel, 1. e., toresurface it by running a diamond point over the wheel surface to even out rough and worn spots.
- the efllciency of grinding operations may be considerably increased by the use of a new grinding oil composition, so that considerably more grinding can be done before redressing the grinding tool.
- the oil of this invention moreover, delays the temper color formation sumciently to allow grinding to'proceed to a point where the wheel approaches more nearly its limit of usefulness as far as its surface is concerned. This oil, therefore, allows grinding to a point of greater deterioration of the wheel, because it helps prolong the use of .the wheel before formation of temper color and need for redressing.
- Grinding oils are to be distinguished from cutting oils. Some oils which are good for cutting purposes are not good for grinding and vice versa. steel or other metal with a cutting tool, such as A cutting oil is generally used in cutting Application November 13, 1945, Serial No. 628,352
- Weight Per Weight For Weight Per i g t eav e lum see 4300 Us s gggggs at F at 100 F. at 100 F 100 None None 76 4, 300 65 35 None 210 3,380 None 100 None 4, 300 None None 100 200 3, 720
- the mixture of light'and heavy oils shows a lower force component than any of theothers, and may be viewed merely as illustrative of one .of the preferred embodiments of the invention.
- a grinding oil composition was made up in accordance with the invention and consisted of 65 weight percent of straw paraflln oilhavinga viscosity of 75 SUS at 100 F. and weight percent of bright stock having a viscosity of 4300 SUS at 100 F.; the viscosity of the grinding oil composition was 210 SUS at 100.
- 0115 having ordinary vlseoslties in the range of 175-275 SUS at 100 E which might becompared with the mixture of -oilsimade in accordance with the invention, have a limited effectiveness because they are too light in body to lubricate effectively under the intense conditions encountered in grinding.
- the heavy oil in our composition is believed to be the-active-lubrieant which lubricates the abrasive and steel surfaces because a major or substantial portion has a boiling point higher than that of the grinding temperature, and it is not the grinding.
- the heavyoil itself is believed to be the-active-lubrieant which lubricates the abrasive and steel surfaces because a major or substantial portion has a boiling point higher than that of the grinding temperature, and it is not the grinding.
- the heavyoil itself is believed to be the-active-lubrieant which lubricates the abrasive and steel surfaces because a major or substantial portion has a boiling point higher than that of the grinding temperature, and it is not the grinding.
- the heavyoil itself is believed to be the-active-lubrieant which lubricates the abrasive and steel surfaces because a major or substantial portion has a boiling point higher than that of the grinding temperature, and it is not the grinding.
- the heavyoil itself is believed to be the-active-lubrieant which
- the light oil alone would not be a very efllcient ,1 lubricant, and furthermore, it is sufilciently volatile so that it flashes ,off to a certain extent at the very point where the abrasive touches the metal, dueto the heat generated in the grinding operation.
- the light oil is light enough to flow into the fine space between the two surfaces.
- the light oil carries the heavy lubricating oil into the space to perform its lubricating function.
- the vaporization of the light cil' is not sufiicient to cause any appreciable thickening of the grinding oil.
- the oil is recycled in the grinding operation, losses being replenished by the addition of'new 011%
- the grinding wheel hereinbefore referred to is illustrative of a bonded abrasive.
- a method of grinding which comprises grinding steel with a bonded abrasive in the presence of an oil-at least 90 weight per cent of which is composed of a mixture of an amount 'of a mineral oil of to 100 SUs at 100 F. within the range of 53 to 78 weight per cent and an amount of a mineral oil of 2000 to 6000 SUS at 100 F. within the range of 47 to 22 weight per cent to provide a mixture having a viscosity in the range of 150 to ⁇ 300 SUS at 100 F.
- a method of grinding which comprises grinding steel with a bonded abrasive in the presence of anoil at least, 90 weight per cent of which is composed oi a mixture of about weight per cent of a mineral oil of viscosity of about SUS at F. and about 35 weight percent of a mineral oil of viscosity of about 4300 BUS at 100' R. which mixture has a viscosity of about 210 sUs at 100 F.
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- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
Description
Patented Nov. is, 1.948
um'rizo STATE GRINDING on. COMPOSITION,
J Everett 0. Hughes, Cleveland Heights, and Franklin Veatch, Cleveland, Ohio, asslgnors to The Standard Oil Company, Cleveland, Ohio, a corporation of Ohio.
No Drawing.
steel gets too hot during such a grinding operation with a worn wheel, the steel becomes discolored. The color may or may not indicate a deterioration in the quality of the steel, but it is undesirable commercially. After the wheel has I been used to an extent where the so-called temper color shows in the steel, it is necessary to redress the grinding wheel, 1. e., toresurface it by running a diamond point over the wheel surface to even out rough and worn spots.
The prior art commercial grinding o'ils do not allow the use of .a grinding wheel to an extent where the surface of the wheel is so rough that it is no longer useful for precision grinding. Long before this point is reached, the wheelwili have caused the steel to become discolored. In. order to maintain the appearance of the finished piece the wheel must be resurfaced long before its otherwise useful life is expended. It is customary, therefore, to appraise grinding oil in terms of the amount of grinding that can be done with a wheel before it must be redressed.
It has been found, in accordance with the in vention, that the efllciency of grinding operations may be considerably increased by the use of a new grinding oil composition, so that considerably more grinding can be done before redressing the grinding tool. The oil of this invention, moreover, delays the temper color formation sumciently to allow grinding to'proceed to a point where the wheel approaches more nearly its limit of usefulness as far as its surface is concerned. This oil, therefore, allows grinding to a point of greater deterioration of the wheel, because it helps prolong the use of .the wheel before formation of temper color and need for redressing.
Grinding oils are to be distinguished from cutting oils. Some oils which are good for cutting purposes are not good for grinding and vice versa. steel or other metal with a cutting tool, such as A cutting oil is generally used in cutting Application November 13, 1945, Serial No. 628,352
- 2 Claims. (Cl. 51 2s1) divergent viscosities, gives much superior results when used as a grinding oil. One of the oils has a relatively low viscosity in the range of 50 to 100 SUS at 100 F. and may be, for example, a straw oil. The other oil. has a very high viscosity in the range of 2000 to 6000 SUS at 100 F. This heavier oil may be, for example, a so-called "bright stock"v and the following are given as examples with' the viscosities (SUSLat 100 F. and 210 F. Generally the viscosity is measured at 210 F. and that at 100 F. calculated in a manner well known in the art:
sUs at 210 F, 165
185 11 3 160 sUs at 1005s. 3740 4300 2100 3500 2218 have a viscosity in the range of 150 to 300 SUS in a lathe, whereas a grinding oil is used in .grindtion by the use of which a great increase in grinding emciency is obtained; and other objects which will become apparent as the invention is described hereinafter.
It has been found, unexpectedly, that a composition comprising a mixture of two oils of widely at 100 F., in order that the oil may flow properly as it is fed to the wheel during grinding. In order to evaluate the efficiency of a grinding oil, a test was developed in which a commercial shop grinder was mounted with a dynamometer so as to measure the horizontal component of the' grinding force as the steel is moved in contact with the grinding wheel. The grinding wheel speed, the speed of table traverse of the steel against the wheel, and the rate of oil application are constant. The horizontal component of force measured in this test is an indication of the grinding efficiency, which is in turn related to' the practicalpperating considerations such as wheel life, number of cuts made before wheel dressing,
amount of heat generated during operation, permissible cutting speeds, etc.v
In grinding tests on "Momax steel grinding out a section 10" in length and 0.040" deep, the following results were obtained with different oils:
Weight Per Weight For Weight Per" i g t eav e lum see 4300 Us s gggggs at F at 100 F. at 100 F 100 None None 76 4, 300 65 35 None 210 3,380 None 100 None 4, 300 None None 100 200 3, 720
1 Oil too viscous to be used as grlndlng oil:
The mixture of light'and heavy oils shows a lower force component than any of theothers, and may be viewed merely as illustrative of one .of the preferred embodiments of the invention.
Other tests indicate the range of proportions and g Q volatilized by the intense heat developed during viscosities suitable as described heretofore as comprising the generic scope of the invention.
In .the above tests the numerical difference in the force may not appear large and the grinding emeiency is not directly proportional to the difference in force. The oils were checked in practical grinding tests by industrial companies using grinding oils and it was found that even an apparently small difference in the force measured in our test is indicative of marked superiority in practical grinding operations.
The marked efliciency of the new grinding oil composition as compared with twoof the best commercial grinding oils available on the open market, is illustrated by the f following tests. These tests were made by grinding twist drills of the same size with automatic machines under identical conditions. A grinding oil composition was made up in accordance with the invention and consisted of 65 weight percent of straw paraflln oilhavinga viscosity of 75 SUS at 100 F. and weight percent of bright stock having a viscosity of 4300 SUS at 100 F.; the viscosity of the grinding oil composition was 210 SUS at 100.
F. The following results are typical.
Vi it Dru Brain; 5008 y Oil SUB at of the 100 F. Grinding Wheel at Series F 6..
4300 sus at 1009 F. 33% 2m 1 P Commercial Grinding Oil No. 250 60-70 Commercial Grinding Oil No. 2 I 90 40-60 ing comments may be of aid in understanding the operation of the oil.
0115 having ordinary vlseoslties in the range of 175-275 SUS at 100 E, which might becompared with the mixture of -oilsimade in accordance with the invention, have a limited effectiveness because they are too light in body to lubricate effectively under the intense conditions encountered in grinding.
The heavy oil in our composition is believed to be the-active-lubrieant which lubricates the abrasive and steel surfaces because a major or substantial portion has a boiling point higher than that of the grinding temperature, and it is not the grinding. The heavyoil itself, however, is
too viscous to flow. into the very fine *space between the abrasive and the metal, Therefore; if a heavy oil alone were used,-there will be a failure of lubrication at the points where it is needed most.. r i
The light oil alone would not be a very efllcient ,1 lubricant, and furthermore, it is sufilciently volatile so that it flashes ,off to a certain extent at the very point where the abrasive touches the metal, dueto the heat generated in the grinding operation. However, the light oil is light enough to flow into the fine space between the two surfaces.
In the mixture the light oil carries the heavy lubricating oil into the space to perform its lubricating function. The vaporization of the light cil'is not sufiicient to cause any appreciable thickening of the grinding oil. The oil is recycled in the grinding operation, losses being replenished by the addition of'new 011% The grinding wheel, hereinbefore referred to is illustrative of a bonded abrasive.
In view of the foregoing disclosure, variations" and modifications-of the invention will be apparent to one skilled in the art. The invention contemplates all such variations and modifications as come within the scope of the appended claims.
We. claim:
1. A method of grinding which comprises grinding steel with a bonded abrasive in the presence of an oil-at least 90 weight per cent of which is composed of a mixture of an amount 'of a mineral oil of to 100 SUs at 100 F. within the range of 53 to 78 weight per cent and an amount of a mineral oil of 2000 to 6000 SUS at 100 F. within the range of 47 to 22 weight per cent to provide a mixture having a viscosity in the range of 150 to\ 300 SUS at 100 F.
2. A method of grinding which comprises grinding steel with a bonded abrasive in the presence of anoil at least, 90 weight per cent of which is composed oi a mixture of about weight per cent of a mineral oil of viscosity of about SUS at F. and about 35 weight percent of a mineral oil of viscosity of about 4300 BUS at 100' R. which mixture has a viscosity of about 210 sUs at 100 F.
EVERETT C. HUGHES. FRANKLIN VEATCH.
narnanncns crran The following references are of record in the file of this patent:
' UNITED STATES PATENTS Number 'Name Date Re. 21,432 Lupo ..I. Apr. 23, 1940 00 1,076,118 Hill Oct. 21, 1913 1,473,947 Bailey Nov. 13, 1923 2,384,225 Wilson Sept. 4, 1945 Certificate of Correction Patent No. 2,453,709. November 16, 1948.
EVERETT C. HUGHES ET AL.
It is hereby certified that error appears in the printed specification of the above numbered patent requiring correction as follows:
Column 4, following line 62, list of references cited, add the following:
2,183,783 Bray -Dec. 19, 1939 2,360,446 Reid Oct. 17, 1944 and that the said Letters Patent should be read with this correction therein that the same may conform to the record of the case in the Patent Ofiice.
Signed and sealed this 31st day of May, A. D. 1949.
THOMAS F. MURPHY,
Assistant Commissioner of Patents.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US628352A US2453709A (en) | 1945-11-13 | 1945-11-13 | Grinding oil composition |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US628352A US2453709A (en) | 1945-11-13 | 1945-11-13 | Grinding oil composition |
Publications (1)
Publication Number | Publication Date |
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US2453709A true US2453709A (en) | 1948-11-16 |
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ID=24518518
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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US628352A Expired - Lifetime US2453709A (en) | 1945-11-13 | 1945-11-13 | Grinding oil composition |
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US (1) | US2453709A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3073690A (en) * | 1960-04-07 | 1963-01-15 | Republic Steel Corp | Method of grinding diamond-shaped recesses in metal-embossing roll |
US3281167A (en) * | 1962-01-08 | 1966-10-25 | Kollmorgen Corp | Method and apparatus for positioning parts to extreme accuracies |
US4599827A (en) * | 1985-06-24 | 1986-07-15 | The United States Of America As Represented By The Secretary Of The Army | Metallographic preparation of particulate filled aluminum metal matrix composite material |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1076118A (en) * | 1913-06-10 | 1913-10-21 | Elmer W Hill | Compound. |
US1473947A (en) * | 1920-11-23 | 1923-11-13 | Bailey Tillman | Composition for polishes |
USRE21432E (en) * | 1940-04-23 | Process and compound for polishing | ||
US2384225A (en) * | 1944-11-22 | 1945-09-04 | Thompson Grinder Co | Method and apparatus for maintaining uniform temperature of diverse fluids in machine tools |
-
1945
- 1945-11-13 US US628352A patent/US2453709A/en not_active Expired - Lifetime
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
USRE21432E (en) * | 1940-04-23 | Process and compound for polishing | ||
US1076118A (en) * | 1913-06-10 | 1913-10-21 | Elmer W Hill | Compound. |
US1473947A (en) * | 1920-11-23 | 1923-11-13 | Bailey Tillman | Composition for polishes |
US2384225A (en) * | 1944-11-22 | 1945-09-04 | Thompson Grinder Co | Method and apparatus for maintaining uniform temperature of diverse fluids in machine tools |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3073690A (en) * | 1960-04-07 | 1963-01-15 | Republic Steel Corp | Method of grinding diamond-shaped recesses in metal-embossing roll |
US3281167A (en) * | 1962-01-08 | 1966-10-25 | Kollmorgen Corp | Method and apparatus for positioning parts to extreme accuracies |
US4599827A (en) * | 1985-06-24 | 1986-07-15 | The United States Of America As Represented By The Secretary Of The Army | Metallographic preparation of particulate filled aluminum metal matrix composite material |
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