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US20080317916A1 - Process for Preparing Nutritional Compositions - Google Patents

Process for Preparing Nutritional Compositions Download PDF

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Publication number
US20080317916A1
US20080317916A1 US11/908,115 US90811506A US2008317916A1 US 20080317916 A1 US20080317916 A1 US 20080317916A1 US 90811506 A US90811506 A US 90811506A US 2008317916 A1 US2008317916 A1 US 2008317916A1
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United States
Prior art keywords
emulsion
fat
matrix
water
mixture
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Abandoned
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US11/908,115
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English (en)
Inventor
Peter Erdmann
Werner Pfaller
Peter Fankhauser
Claudia Caroline Weiss
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Nestec SA
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Nestec SA
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Application filed by Nestec SA filed Critical Nestec SA
Assigned to NESTEC S.A. reassignment NESTEC S.A. ASSIGNMENT OF ASSIGNORS INTEREST (SEE DOCUMENT FOR DETAILS). Assignors: ERDMANN, PETER, FANKHAUSER, PETER, PFALLER, WERNER, WEISS, CLAUDIA CAROLINE
Publication of US20080317916A1 publication Critical patent/US20080317916A1/en
Abandoned legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23DEDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS OR COOKING OILS
    • A23D9/00Other edible oils or fats, e.g. shortenings or cooking oils
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23DEDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS OR COOKING OILS
    • A23D7/00Edible oil or fat compositions containing an aqueous phase, e.g. margarines
    • A23D7/02Edible oil or fat compositions containing an aqueous phase, e.g. margarines characterised by the production or working-up
    • A23D7/04Working-up
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING OR TREATMENT THEREOF
    • A23C11/00Milk substitutes, e.g. coffee whitener compositions
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING OR TREATMENT THEREOF
    • A23C11/00Milk substitutes, e.g. coffee whitener compositions
    • A23C11/02Milk substitutes, e.g. coffee whitener compositions containing at least one non-milk component as source of fats or proteins
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING OR TREATMENT THEREOF
    • A23C9/00Milk preparations; Milk powder or milk powder preparations
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23DEDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS OR COOKING OILS
    • A23D9/00Other edible oils or fats, e.g. shortenings or cooking oils
    • A23D9/02Other edible oils or fats, e.g. shortenings or cooking oils characterised by the production or working-up
    • A23D9/04Working-up
    • A23D9/05Forming free-flowing pieces
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/17Amino acids, peptides or proteins
    • A23L33/19Dairy proteins
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/40Complete food formulations for specific consumer groups or specific purposes, e.g. infant formula
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23PSHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
    • A23P30/00Shaping or working of foodstuffs characterised by the process or apparatus
    • A23P30/20Extruding

Definitions

  • This invention relates to a process for preparing nutritional compositions by extrusion and to nutritional compositions so prepared.
  • Powdered nutritional compositions containing the macronutrients protein, fat and carbohydrate are well known. They are intended to be reconstituted prior to consumption with a liquid which is usually water but may alternatively be liquid milk or fruit juice.
  • a liquid which is usually water but may alternatively be liquid milk or fruit juice.
  • Such products include infant formula, growing up milks and compositions used in clinical nutrition, for example for enteral feeding. Conventionally, such products are manufactured by mixing all the ingredients with water, subjecting the liquid mixture to a thermal treatment to reduce bacterial loads, homogenising the mixture and then spray drying it.
  • the present inventors have found that it is possible to extrude a mixture comprising an oil in water emulsion without leading to coalescence or inversion of the emulsion.
  • the emulsion is stable under high shear, high temperatures, high pressures and minimal amount of water in the extruder.
  • the present invention provides a process for preparing a nutritional composition including protein, fat and carbohydrate which process comprises emulsifying the fat in water with an emulsifier to form an emulsion having a solids content of at least 70%, homogenising the emulsion and extruding the emulsion together with a solid matrix comprising the protein and the carbohydrate in a ratio between 1 part emulsion:0.5 parts matrix to 1 part emulsion:5 parts matrix into a vacuum chamber at a temperature at or above the melting point of the mixture of emulsion and matrix to obtain a solid product having a maximum water content of 10%.
  • the process of the invention provides a solid product that is easily dispersible upon addition to water or another liquid to give a homogeneous liquid mixture of protein, fat and carbohydrate with no discernible separation of aqueous and non-aqueous phases.
  • the nutritional composition is an infant formula.
  • the process may additionally include a drying step to remove any remaining moisture from the extruded product.
  • the process may optionally include a milling step whereby the extruded product, which is typically in the form of porous pellets, is reduced to a powder with a higher density.
  • stable used to describe the emulsion means that the emulsion is stable with respect to coalescence and/or inversion, both visually determined.
  • solid matrix means a mixture of solid ingredients without added liquids
  • ily disperses means disperses with a minimum of agitation or stirring.
  • the properties and constitution of the emulsion are crucial in order to achieve the desired result with respect to dispersibility. Accordingly, the emulsion has a water content of at the most about 30% w/w. It is stable towards coalescence and inversion when extruded with a solid matrix of protein and carbohydrate in a weight ratio of from 1:0.5 to about 1:5 at a temperature at or above the melting point of the mixture of the emulsion and the solid matrix. The thus obtained extruded product is expanded into a vacuum chamber to obtain a solid product having at the most about 10% water content.
  • the emulsifier may be water soluble or fat soluble.
  • Suitable water soluble emulsifiers include caseinates such as sodium caseinate and potassium caseinate, acid caseinate, other milk fractions that are commonly used as emulsifiers and sugar esters.
  • Suitable fat soluble emulsifiers include lecithins and mono- and diglycerides such as CITREM®.
  • Preferably both water soluble and fat soluble emulsifiers are used.
  • both the water soluble emulsifier and the fat soluble emulsifier are added to the fat prior to emulsification.
  • the weight ratio between fat and emulsifier may be in the range of from about 10:1 to about 18:1 depending on the amount of water employed.
  • a preferred ratio between fat and emulsifier is about 14:1 at 26% water (ideally 69% fat, 5% emulsifier and 26% water). If the ratio is too low, there is a risk that the emulsion inverts during homogenisation. If, however, the ratio is too high, it is difficult to stabilise small fat particles during the extrusion step.
  • the fat component may constitute from 50 to 75% w/w of the emulsion. Any fat or mixture of fats generally suitable for nutritional compositions may be used. For example, if the composition is an infant formula, palm olein, coconut oil, canola oil, milk fat and mixtures thereof may be used. Long chain polyunsaturated fatty acids may also be incorporated such as docosahexaenoic acid (from fish oil) and arachidonic acid (from fungal oils such as that obtained from Mortierella alpina ). Oil soluble vitamins such as Vitamin E may also be included in the emulsion if desired.
  • the emulsion may be homogenized by any method known in the art to reach a mean particle size D [0.5] in the range from 0.2 to 10 ⁇ m.
  • D [0.5] preferably lies in the range from 0.2 to 1.5 ⁇ m.
  • carbohydrate content of the nutritional composition will also be selected with reference to the type of composition being produced.
  • suitable carbohydrates include lactose, maltodextrin and starch and mixtures thereof.
  • the content of carbohydrate in the nutritional composition will vary according to the type of composition and is generally expressed in terms of the contribution made by carbohydrate to the overall energy of the composition.
  • an infant formula generally contains from 7 to 15 g carbohydrate per 100 kcal of formula depending upon the type of product and the age group for which it is intended.
  • Prebiotic fibres may also be included if desired.
  • the term prebiotic is used to designate a non-digestible food ingredient that beneficially affects the host by selectively stimulating the growth and/or activity of one or a limited number of bacteria in the colon, and thus improves host health.
  • Such ingredients are non-digestible in the sense that they are not broken down and absorbed in the stomach or small intestine and thus pass intact to the colon where they are selectively fermented by the beneficial bacteria.
  • Examples of prebiotics suitable for addition to infant formula include certain oligosaccharides, such as fructooligosaccharides, galactooligosaccharides, sialyl-lactose and oligosaccharides derived from animal milk.
  • the protein component of the nutritional composition will likewise be selected with reference to the type of composition being produced.
  • suitable proteins include milk proteins such as casein and whey, soy proteins, rice proteins and mixtures thereof. A mixture of 70% whey to 30% casein is particularly preferred.
  • the proteins may be intact or partially hydrolysed.
  • the content of protein in the nutritional composition will vary according to the type of composition and is generally expressed in terms of the contribution made by protein to the overall energy of the composition.
  • an infant formula generally contains from 1.8 to 4.5 g protein per 100 kcal of formula depending upon the type of product and the age group for which it is intended.
  • the weight ratio between the emulsion and the solid matrix is from 1:0.5 to 1:5. Within this range, the selected weight ratio will depend on the type of nutritional composition desired.
  • the water content of the mixture of emulsion and solid matrix entering the extruder may be 15% or less.
  • nucleotides may be added to the solid matrix prior to extrusion (or to the fat prior to emulsification if fat soluble). Alternatively, some or all of these ingredients may be added after extrusion by dry mixing.
  • any suitable extruder may be used such as, e.g. single screw, twin screw, multi screw, ring screw, planetary gear extruder, etc. or any other continuous or discontinuous mixing system with the possibility to shape the melt (melted mixture).
  • vacuum used in the present context is intended to denote a pressure between 0.01 and 250 mbar, preferably between 1 and 50 mbar. A particularly preferred range is between 10 and 25 mbar.
  • Extrusion is carried out at a temperature at or above the melting point of the mixture of the emulsion and the solid matrix. Typically, this temperature will lie in the range between 80 and 90° C. and the extrusion will be carried out at a temperature in the range between 80 and 120° C. Extruding at a temperature below the melting point tends to lead to instability of the emulsion during extrusion, which may in turn lead to a product with reduced solubility, flocculation or other unwanted effects such as complete phase separation when the product is reconstituted. Conversely, extruding at an elevated temperature can adversely affect the nutritional quality of the product as measured for example by increased lysine blockage and browning of the product.
  • the water content of the solid product leaving the vacuum chamber is 10% or less. If desired, this may be subjected to a further drying step. For example, if it is desired to produce an infant formula containing probiotic bacteria, it will be necessary to further dry the product to a final water content of around 1%. This may be effected by passing the extruded product from the vacuum chamber to a fluidised bed dryer for example. Alternatively, or additionally, a source of heat such as a source of infra-red radiation may be provided in the vacuum chamber itself.
  • the product of the extrusion process is typically in the form of porous pellets or aggregates of relatively low density.
  • compositions produced according to the process of the present invention contain air trapped within the solid product.
  • the incorporated air pockets have a non-circular shape as observed by fluorescence confocal microscopy.
  • the structure can thus be compared to a frozen foam in which the air bubbles or pockets are non-spherical. If it is desired to produce a powder of higher density which takes up less room as well as looking more like the spray dried powders to which consumers are accustomed, the pellets/aggregates may be milled into a finely divided powder.
  • Nutritional compositions produced according to the process of the invention are found to have generally improved solubility/dispersibility compared to the same products produced by spray drying. At the same time, the nutritional quality of products made by the process of the invention (expressed for example in terms of lysine blockage) is found to be comparable to the same products produced by spray drying.
  • implementing the process of the invention has a lower investment cost than the spray drying technology conventionally used to produce such products (no requirement for spray drying towers or air heaters means less requirement for space) and the process is simpler than spray drying making it overall more cost-efficient.
  • FIG. 1 shows a schematic set-up of the process
  • the screw configuration for Examples 1 and 2 was as shown in Table 1 below
  • Fat phase Water phase: 420 g vegetable fat blend 160 g Water 3 g CITREM ® 1.5 g Sodium citrate 30.8 g Potassium caseinate
  • Preparation of the fat phase The vegetable fat blend is melted and mixed with the CITREM at 65° C. Then the potassium caseinate is sieved through a sieve of 1 mm and added to the fat mixture with stirring. A yellow suspension is obtained.
  • Preparation of the water phase The water is heated to 65° C., the sodium citrate is added and the solution is stirred for 10 min.
  • Preparation and homogenisation of the emulsion The fat phase is added to the water phase with vigorous stirring until all the fat is incorporated. An increase in viscosity is noted. The pre-emulsion is stirred for another 5 min then the temperature is raised to 95° C. and a multi-stage homogenisation is carried out at 85° C. under a pressure of 300 bar. The resulting highly viscous emulsion is pumped directly into the extruder.
  • Extrusion of infant formula formulation 37.5 kg/h of an emulsion prepared as described above together with 70 kg/h of a solid matrix comprising 78.87% Maltodextrin DE29, 0.8% K 2 HPO 4 , 12.22% Lacprodan DI-9224 whey protein isolate, 5.77% potassium caseinate and 2.34% calcium citrate, together with vitamin and trace element premixes are supplied to the extruder.
  • Barrel 1 of the extruder is maintained at 21° C.
  • barrel 2 at 60° C.
  • barrel 3 at 106° C.
  • barrel 4 at 109° C.
  • the die plate is maintained at 110° C.
  • the mixture is extruded at a pressure of 0.4 bar and a temperature of 103° C. into a vacuum chamber at a pressure of 24 mbar yielding a solid product with a moisture content of 2.9%.
  • the mean size of the fat particles D [0.5] is 1.72 ⁇ m.
  • the lysine blockage is 8%.
  • Fat phase Water phase: 420 g anhydrous milk fat 160 g Water 3 g CITREM ® 1.5 g Sodium citrate 40 g Milk protein concentrate
  • Preparation of the fat phase The milk fat is melted and mixed with the CITREM and milk protein concentrate at 65° C. A yellow suspension is obtained.
  • Preparation of the water phase The water is heated to 65° C., the sodium citrate is added and the solution is stirred for 10 min.
  • Preparation and homogenisation of the emulsion The fat phase is added to the water phase with vigorous stirring until all the fat is incorporated. An increase in viscosity is noted. The pre-emulsion is stirred for another 5 min then the temperature is raised to 95° C. and a multi-stage homogenisation is carried out at 85° C. under a pressure of 300 bar. The resulting highly viscous emulsion is pumped directly into the extruder.
  • Extrusion of growing up milk formulation 37.5 kg/h of the emulsion together with 70 kg/h of a solid matrix with the composition 39.2% Maltodextrin DE 29, 0.8% K 2 HPO 4 , 15% milk protein concentrate 20%, 22.5% lactose and 2.5% calcium citrate together with vitamin and trace element premixes are supplied to the extruder.
  • the extrusion conditions are the same as for Example 1 except that the die plate is heated to 105° C.
  • the extruded product has a moisture content of 2.9%.
  • D [0.5] is 0.952 ⁇ m. Lysine blockage is 11.8%.
  • Fat phase Water phase: 420 g vegetable fat blend 160 g Water 30.8 g Potassium caseinate
  • Preparation of the water phase The water is heated to 65° C.
  • Preparation and homogenisation of the emulsion The fat phase is added to the water phase with vigorous stirring until all the fat is incorporated. An increase in viscosity is noted. The pre-emulsion is stirred for another 5 minutes then the temperature is raised to 95° C. and a multi-stage homogenisation is carried out at 85° C. under a pressure between 50-200 bar. The resulting highly viscous emulsion is pumped directly into the extruder.
  • Extrusion of infant formula formulation 35 kg/h of an emulsion prepared as described above together with 72 kg/h of a solid matrix comprising 25.39% Maltodextrin DE29, 30.57% skim milk powder, 16.02% demineralised whey powder DWP28, 26.68% lactose, 2.34% salts and minerals, together with vitamin and trace element premixes are supplied to the extruder.
  • Barrel 1 of the extruder is maintained at 30° C.
  • barrel 2 at 60° C.
  • barrel 3 at 110° C.
  • barrel 4 at 110° C.
  • the die plate is maintained at 110° C.
  • the mixture is extruded at a pressure of 0.4 bar and a temperature of 105° C. into a vacuum chamber at a pressure of 24 mbar yielding a solid product with a moisture content of about 8%.
  • the mean size of the fat particles D [0.5] is around 2 ⁇ m.
  • the lysine blockage is less than 11%.

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Nutrition Science (AREA)
  • Mycology (AREA)
  • Pediatric Medicine (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Manufacturing & Machinery (AREA)
  • Edible Oils And Fats (AREA)
  • Grain Derivatives (AREA)
  • Dairy Products (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Tea And Coffee (AREA)
  • Fodder In General (AREA)
US11/908,115 2005-03-08 2006-03-08 Process for Preparing Nutritional Compositions Abandoned US20080317916A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP05005064.0 2005-03-08
EP05005064 2005-03-08
PCT/EP2006/060558 WO2006094995A1 (fr) 2005-03-08 2006-03-08 Procede de preparation de compositions nutritives

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US20080317916A1 true US20080317916A1 (en) 2008-12-25

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Family Applications (2)

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US11/908,116 Expired - Fee Related US8101226B2 (en) 2005-03-08 2006-03-08 Extruded solid product for use in foodstuffs
US11/908,115 Abandoned US20080317916A1 (en) 2005-03-08 2006-03-08 Process for Preparing Nutritional Compositions

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Application Number Title Priority Date Filing Date
US11/908,116 Expired - Fee Related US8101226B2 (en) 2005-03-08 2006-03-08 Extruded solid product for use in foodstuffs

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US (2) US8101226B2 (fr)
EP (2) EP1865787A1 (fr)
JP (1) JP4764477B2 (fr)
KR (1) KR101355850B1 (fr)
CN (2) CN101170910B (fr)
AR (1) AR052597A1 (fr)
AT (1) ATE430480T1 (fr)
AU (2) AU2006221943B2 (fr)
BR (2) BRPI0609024A2 (fr)
CA (2) CA2600670C (fr)
DE (1) DE602006006654D1 (fr)
DK (1) DK1858342T3 (fr)
MX (2) MX2007010956A (fr)
RU (2) RU2395975C2 (fr)
SG (1) SG160378A1 (fr)
WO (2) WO2006094999A1 (fr)
ZA (2) ZA200708538B (fr)

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US20090142442A1 (en) * 2007-12-04 2009-06-04 Nestec S.A. Gut microbiota in infants
WO2012056006A1 (fr) * 2010-10-29 2012-05-03 Nestec S.A. Produit alimentaire déshydraté
US20140228429A1 (en) * 2011-05-27 2014-08-14 Dsm Ip Assets B.V Extrusion process
WO2015050429A1 (fr) * 2013-10-03 2015-04-09 Malaysian Palm Oil Board (Mpob) Procédé de libération de nutriments lipophiles issus d'oléine de palme rouge
EP3982740A1 (fr) * 2019-06-13 2022-04-20 N.V. Nutricia Procédé de fabrication d'un produit de préparation pour nourrissons avec une protéine hydrolysée

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DE102009014137A1 (de) * 2009-03-24 2010-09-30 Josera Gmbh & Co. Kg Verfahren zur Herstellung eines Nahrungsmittels, sowie ein Tierfuttermittel und ein Humanernährungsmittel
RU2012126631A (ru) * 2009-11-27 2014-01-10 Нестек С.А. Пищевой продукт на зерновой основе, содержащий молочный белок
BR112012020064B1 (pt) 2010-02-12 2018-04-03 Arla Foods Amba Produto de leite e produto de leite envazado
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ITMI20111050A1 (it) 2011-06-10 2012-12-11 Sevecom Spa Uso di emulsionanti in associazione con oleine vegetali in un alimento per animali.
IN2014DN07058A (fr) * 2012-02-28 2015-04-10 Dsm Ip Assets Bv
US20150118352A1 (en) * 2012-04-20 2015-04-30 Intercontinental Great Brands Llc System and method for manufacturing chewing gum
WO2014026313A1 (fr) * 2012-08-13 2014-02-20 Nestec S.A. Procédé de production d'un précurseur de boisson de café
CN104540392A (zh) * 2012-08-13 2015-04-22 雀巢产品技术援助有限公司 制备咖啡饮料前体的方法
US20150305394A1 (en) * 2012-10-24 2015-10-29 Abbott Laboratories Extruded nutritional powders having improved emulsion stability and dispersibility and methods of manufacturing same
BR112015012038A2 (pt) * 2012-11-27 2017-07-11 Dsm Ip Assets Bv processo para a produção de partículas extrudidas sólidas discretas
UA105987C2 (uk) * 2013-04-01 2014-07-10 Кристина Борисівна Нечепуренко Спосіб одержання твердої емульсії та тверда емульсія
EP3057435A4 (fr) * 2013-10-17 2017-06-21 The University Of Georgia Research Foundation, Inc Triacylglycérols structurés et procédés de préparation
RU2662282C2 (ru) 2013-11-01 2018-07-25 Н.В. Нютрисиа Липидная композиция для улучшения состава тела во время догоняющего роста
WO2015171906A1 (fr) * 2014-05-08 2015-11-12 Abbott Laboratories Composition nutritionnelle à base de poudre extrudée et procédés de production associés
AU2015293628B2 (en) 2014-07-21 2019-06-20 Sevecom S.P.A. Powdered emulsion for animal feed
MX391907B (es) 2015-05-16 2025-03-21 Big Heart Pet Inc Productos alimenticios expandidos apetitosos y metodos para fabricar los mismos.
US9907323B2 (en) 2015-09-25 2018-03-06 Mead Johnson Nutrition Co. Infant formula tablets
BR112018007095B1 (pt) 2015-10-15 2022-07-05 N.V. Nutricia Composição nutricional
FI3874959T3 (fi) 2016-12-09 2024-08-09 Nutricia Nv Ravintokoostumus käytettäväksi kognitiivisen toimintakyvyn parantamisessa ja/tai kognitiivisen heikentymisen ehkäisemisessä
WO2019117705A1 (fr) 2017-12-13 2019-06-20 N.V. Nutricia Extrusion
CN111629599A (zh) * 2018-02-19 2020-09-04 雅培制药有限公司 脂质乳剂营养产品
US20210360955A1 (en) * 2019-02-19 2021-11-25 Paragon Flavors, Inc. System and method for flavor encapsulation
EP3982741A1 (fr) * 2019-06-13 2022-04-20 N.V. Nutricia Procédé de fabrication d'un produit de préparation fermenté pour nourrissons
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WO2020251352A1 (fr) 2019-06-13 2020-12-17 N.V. Nutricia Extrusion par injection de gaz pour la production de produits de préparation pour nourrissons
US20220232879A1 (en) 2019-06-13 2022-07-28 N.V. Nutricia Extrusion process for making infant formula with large lipid globules
CN115226785B (zh) * 2022-07-29 2023-07-25 江南大学 一种o/w类脂肪凝胶及其制备方法和3d打印应用
WO2024102712A1 (fr) * 2022-11-07 2024-05-16 Rich Products Corporation Garnitures, crèmes et compositions culinaires contenant de la caséine micellaire

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4177574A (en) * 1977-03-12 1979-12-11 Kanesa Miso Kabushiki-Kaisha Method and apparatus for granulating hydrated materials including food stuffs
US5125168A (en) * 1989-07-03 1992-06-30 Zwag Zschokke Wartmann Ag Apparatus for processing a pasty product in a vacuum
US5284674A (en) * 1992-05-11 1994-02-08 Fazio Susan C Powdered dairy creamer
US5338559A (en) * 1991-08-22 1994-08-16 Schaaf Heinz Josef Method and apparatus for making expanded food stuffs
US5750173A (en) * 1996-11-05 1998-05-12 Mjm Technologies, L.L.P. Method of manufacturing syrup-infused food pieces
US6136353A (en) * 1996-07-23 2000-10-24 Buhler Ag Method of incorporating fatty matter into granulated products
US20010055636A1 (en) * 1999-09-22 2001-12-27 Osvaldo Geromini Impregnated composite extrusion product
US6468579B1 (en) * 1999-06-11 2002-10-22 Bongrain S.A. Food product with a fibrous texture obtained from whey proteins
US20050042329A1 (en) * 2003-08-18 2005-02-24 Chmura James N. Calcium fortified, soy based, infant nutritional formulas

Family Cites Families (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3434843A (en) * 1967-03-08 1969-03-25 Pillsbury Co Stable food pieces
US3852487A (en) * 1969-08-28 1974-12-03 Lever Brothers Ltd Meat paste product and process for preparing same
US3718485A (en) * 1970-07-01 1973-02-27 Vacu Dry Food dehydration method
SU805986A1 (ru) 1979-01-19 1981-02-23 Ордена Ленина Институт Элементоорга-Нических Соединений Ah Cccp Пищева эмульси с низким содержа-НиЕМ жиРА
JPS5916749B2 (ja) 1981-08-20 1984-04-17 日本油脂株式会社 水中油型乳化液
US5011855A (en) 1982-04-16 1991-04-30 Nestec S.A. Cosmetic and dermatological compositions containing γ-linolenic acid
FR2561916B1 (fr) * 1984-03-30 1987-12-11 Lafon Labor Forme galenique pour administration orale et son procede de preparation par lyophilisation d'une emission huile dans eau
DE3629526A1 (de) * 1986-08-29 1988-03-10 Werner & Pfleiderer Verfahren und vorrichtung zur herstellung einer schokolademasse
US4853236A (en) * 1988-03-18 1989-08-01 General Mills, Inc. Dual textured food piece of enhanced stability
US5411756A (en) * 1989-09-20 1995-05-02 Nabisco, Inc. Reduced calorie triglyceride mixtures
IT1247102B (it) * 1991-02-21 1994-12-12 Orlando Nuovi Investimenti Ali Prodotto dolciario aereato spalmabile del genere costituito da un' emulsione acqua in olio
JPH0741793A (ja) 1993-07-27 1995-02-10 Nippon Suisan Kaisha Ltd 粉末油脂及びその製造方法
CH686479A5 (fr) * 1993-08-11 1996-04-15 Nestle Sa Produit alimentaire a rehydratation rapide et son procede de preparation.
FR2712188B1 (fr) * 1993-11-08 1996-01-26 Oreal Composition cosmétique destinée au maquillage de la peau, son procédé de préparation et produit de maquillage obtenu à partir de ladite composition.
JP3118155B2 (ja) * 1994-12-01 2000-12-18 アサヒフーズ株式会社 低脂肪分、耐酸性および凍結耐性を有するホイップクリーム組成物並びにその製造方法
EP0796567A1 (fr) * 1996-02-07 1997-09-24 Societe Des Produits Nestle S.A. Produit alimentaire granulaire
US5741538A (en) * 1996-02-22 1998-04-21 The Procter & Gamble Company Low density soluble coffee products having increased particle strength and rapid hot water solubility
CH690351A5 (it) 1996-07-08 2000-08-15 Soremartec Sa Composizione alimentare in forma di massa plastica schiumosa.
WO2000023038A1 (fr) 1998-10-21 2000-04-27 Revlon Consumer Products Corporation Compositions cosmetiques contenant des complexes polysaccharide/proteine
US6177119B1 (en) 1998-11-10 2001-01-23 Kraft Foods, Inc. Self-Whitening coffee and method of manufacture therefor
US6129943A (en) 1999-06-22 2000-10-10 Kraft Foods, Inc. Foaming cappuccino creamer containing gasified carbohydrate
AU7247000A (en) * 2000-01-11 2001-07-19 Givaudan Sa Composite materials
JP4195545B2 (ja) 2000-06-08 2008-12-10 ミヨシ油脂株式会社 水中油型乳化物
IES20010488A2 (en) 2001-05-21 2002-10-30 Kerry Group Services Int Ltd Food product
US6432463B1 (en) * 2001-10-31 2002-08-13 Recot, Inc. Process for producing expandable pellets

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4177574A (en) * 1977-03-12 1979-12-11 Kanesa Miso Kabushiki-Kaisha Method and apparatus for granulating hydrated materials including food stuffs
US5125168A (en) * 1989-07-03 1992-06-30 Zwag Zschokke Wartmann Ag Apparatus for processing a pasty product in a vacuum
US5338559A (en) * 1991-08-22 1994-08-16 Schaaf Heinz Josef Method and apparatus for making expanded food stuffs
US5284674A (en) * 1992-05-11 1994-02-08 Fazio Susan C Powdered dairy creamer
US6136353A (en) * 1996-07-23 2000-10-24 Buhler Ag Method of incorporating fatty matter into granulated products
US5750173A (en) * 1996-11-05 1998-05-12 Mjm Technologies, L.L.P. Method of manufacturing syrup-infused food pieces
US6468579B1 (en) * 1999-06-11 2002-10-22 Bongrain S.A. Food product with a fibrous texture obtained from whey proteins
US20010055636A1 (en) * 1999-09-22 2001-12-27 Osvaldo Geromini Impregnated composite extrusion product
US20050042329A1 (en) * 2003-08-18 2005-02-24 Chmura James N. Calcium fortified, soy based, infant nutritional formulas

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Fellows, P. "Food Processing Technology". 2000. CRC Press, Woodhead Publishing LTD. Pages 1-48. *

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20090142442A1 (en) * 2007-12-04 2009-06-04 Nestec S.A. Gut microbiota in infants
US9131721B2 (en) * 2007-12-04 2015-09-15 Nestec S.A. Gut microbiota in infants
WO2012056006A1 (fr) * 2010-10-29 2012-05-03 Nestec S.A. Produit alimentaire déshydraté
US20140228429A1 (en) * 2011-05-27 2014-08-14 Dsm Ip Assets B.V Extrusion process
WO2015050429A1 (fr) * 2013-10-03 2015-04-09 Malaysian Palm Oil Board (Mpob) Procédé de libération de nutriments lipophiles issus d'oléine de palme rouge
EP3982740A1 (fr) * 2019-06-13 2022-04-20 N.V. Nutricia Procédé de fabrication d'un produit de préparation pour nourrissons avec une protéine hydrolysée

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