US20030056572A1 - Detection of leaks in heat exchangers - Google Patents
Detection of leaks in heat exchangers Download PDFInfo
- Publication number
- US20030056572A1 US20030056572A1 US10/149,184 US14918402A US2003056572A1 US 20030056572 A1 US20030056572 A1 US 20030056572A1 US 14918402 A US14918402 A US 14918402A US 2003056572 A1 US2003056572 A1 US 2003056572A1
- Authority
- US
- United States
- Prior art keywords
- flow path
- helium
- pressure
- flow
- detector probe
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- 238000001514 detection method Methods 0.000 title claims abstract description 13
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 claims abstract description 40
- 239000001307 helium Substances 0.000 claims abstract description 39
- 229910052734 helium Inorganic materials 0.000 claims abstract description 39
- 238000000034 method Methods 0.000 claims abstract description 20
- 239000000523 sample Substances 0.000 claims abstract description 14
- 239000007788 liquid Substances 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 239000007789 gas Substances 0.000 description 3
- 230000003134 recirculating effect Effects 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Images
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01M—TESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
- G01M3/00—Investigating fluid-tightness of structures
- G01M3/02—Investigating fluid-tightness of structures by using fluid or vacuum
- G01M3/04—Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point
- G01M3/20—Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point using special tracer materials, e.g. dye, fluorescent material, radioactive material
- G01M3/22—Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point using special tracer materials, e.g. dye, fluorescent material, radioactive material for pipes, cables or tubes; for pipe joints or seals; for valves; for welds; for containers, e.g. radiators
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01M—TESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
- G01M3/00—Investigating fluid-tightness of structures
- G01M3/02—Investigating fluid-tightness of structures by using fluid or vacuum
- G01M3/04—Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point
- G01M3/20—Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point using special tracer materials, e.g. dye, fluorescent material, radioactive material
- G01M3/22—Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point using special tracer materials, e.g. dye, fluorescent material, radioactive material for pipes, cables or tubes; for pipe joints or seals; for valves; for welds; for containers, e.g. radiators
- G01M3/226—Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point using special tracer materials, e.g. dye, fluorescent material, radioactive material for pipes, cables or tubes; for pipe joints or seals; for valves; for welds; for containers, e.g. radiators for containers, e.g. radiators
- G01M3/228—Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point using special tracer materials, e.g. dye, fluorescent material, radioactive material for pipes, cables or tubes; for pipe joints or seals; for valves; for welds; for containers, e.g. radiators for containers, e.g. radiators for radiators
Definitions
- This invention relates to heat exchangers and in particular provides an improved method for detection of leaks in plate flack heat exchangers, especially for use in the food and drinks industry.
- British Patent No. 2314421 describes a method of testing a plate pack heat exchanger for leaks, the heat exchanger having discrete first and second flow paths in thermal contact, the method comprising connecting a gas circulation system including a helium detector probe across the first flow path; emptying the second flow path of any liquid and introducing helium; and using the helium detection probe to detect any helium in the first flow path.
- the present invention provides a method for detection of leaks in a plate pack heat exchanger having respective discrete first and second flow paths in mutual thermal contract, the method comprising connecting a helium detector probe at one end of said first flow path and an air compressor means at the other end of said first flow path, introducing helium to said second flow path, allowing air to pass through said first flow path under the influence of the compressor means and detecting any helium present therein by the helium detector probe, the pressure of the second flow path being higher than that of the first flow path.
- the air compressor preferably operates at relatively low pressures, sufficient to drive air at from 15 to 30 cu. ft./min. through the first flow path against an outlet of atmospheric pressure.
- both flow paths are emptied of as much liquid as possible before carrying out the method of the invention although fast response times are still achieved in the presence of water.
- the second flow path, containing the introduced helium is also preferably open-ended, more preferably with a flow restrictor or throttle, at the downstream end, whereby the helium or helium-containing gas bleeds through the secondary flow path under a positive pressure, to enhance leak-detection effectiveness while forming a dynamic rather than a static system.
- the pressure at which the helium is introduced preferably does not exceed 20 psig.
- the helium detector probe preferably detects helium present in the primary flow path on the basis of thermal conductivity.
- the heat exchanger is shown generally at 10 and includes heat exchange elements in the form of plates 11 extending between primary and secondary chambers 12 , 13 respectively.
- the chambers have inlets and outlets (not shown) for supply and removal of heat exchange liquids.
- the chambers are in thermal contact with each other via the plates but are intended to be isolated from each other for mass transfer.
- the primary chamber 12 is provided at one end with a source of helium gas 14 and a supply line 16 . At the other end of the chamber 12 is provided a tap 18 disposed in a take-off line 20 .
- the secondary chamber 13 is provided at one end with an air pressure supply line 22 connected to a compressor 24 and at the other end with a helium detector probe 26 .
- the compressor 24 In use and following removal of the heat exchange liquids from the primary and secondary chambers, the compressor 24 is started and flow of air at atmospheric pressure through the secondary chamber is established. Helium is them introduced in the primary chamber and allowed to flow out though the tap 18 in the open condition. The tap is then partially closed so that helium continues to flow through the primary chamber under a moderate positive pressure. Helium will flow through any leaks between the primary and secondary chambers under the influence of the differential pressure therebetween and will be detected by the detector probe 26 . Detection of any leaked helium can be expected to take place after approximately 5 minutes of operation, even in the presence of water.
Landscapes
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Examining Or Testing Airtightness (AREA)
- Separation By Low-Temperature Treatments (AREA)
- Heat-Exchange Devices With Radiators And Conduit Assemblies (AREA)
Abstract
A method for detection of leaks in a plate pack heat exchanger having respective discrete first and second flow paths in mutual thermal contract comprises connecting a helium detector probe at one end of the first flow path and an air compressor means at the other end of the first flow path, introducing helium to the second flow path, allowing air to pass through the first flow path under the influence of the compressor means and detecting any helium present therein by the helium detector probe, the pressure of the second flow path being higher than that of the first flow path.
Description
- This invention relates to heat exchangers and in particular provides an improved method for detection of leaks in plate flack heat exchangers, especially for use in the food and drinks industry.
- British Patent No. 2314421 describes a method of testing a plate pack heat exchanger for leaks, the heat exchanger having discrete first and second flow paths in thermal contact, the method comprising connecting a gas circulation system including a helium detector probe across the first flow path; emptying the second flow path of any liquid and introducing helium; and using the helium detection probe to detect any helium in the first flow path.
- While the method described in my earlier British patent represents a way of using commercially-available helium detectors to test heat exchangers for leaks in a simple and economical manner, it has been found in practice that detection times are slow, typically around 20 minutes from introduction of the helium, or even several times longer if any residual water is present in the second flow path, requiring the helium to diffuse through the water or other liquid.
- It is an object of the present invention to provide a method for detection of leaks in heat exchangers and which provides a faster result, in that the absence of leaks can be reliably determined after only a few minutes, rather than having to wait for at least 20 minutes, especially when used in the presence of water or other liquid.
- Accordingly, the present invention provides a method for detection of leaks in a plate pack heat exchanger having respective discrete first and second flow paths in mutual thermal contract, the method comprising connecting a helium detector probe at one end of said first flow path and an air compressor means at the other end of said first flow path, introducing helium to said second flow path, allowing air to pass through said first flow path under the influence of the compressor means and detecting any helium present therein by the helium detector probe, the pressure of the second flow path being higher than that of the first flow path.
- In using the method of the present invention, the air compressor preferably operates at relatively low pressures, sufficient to drive air at from 15 to 30 cu. ft./min. through the first flow path against an outlet of atmospheric pressure. By using an open-ended flow path for the detection probe, a faster and more accurate result is achieved compared with the prior art method in that the helium detected is quantitatively representative of the scale of the leak, whereas in the prior art method the helium concentration increases as it accumulates in the closed recirculating system.
- Desirably, both flow paths are emptied of as much liquid as possible before carrying out the method of the invention although fast response times are still achieved in the presence of water. The second flow path, containing the introduced helium, is also preferably open-ended, more preferably with a flow restrictor or throttle, at the downstream end, whereby the helium or helium-containing gas bleeds through the secondary flow path under a positive pressure, to enhance leak-detection effectiveness while forming a dynamic rather than a static system. The pressure at which the helium is introduced preferably does not exceed 20 psig.
- The helium detector probe preferably detects helium present in the primary flow path on the basis of thermal conductivity.
- An embodiment of the invention will now be described by way of example with reference to the accompanying drawing, which illustrates schematically one form of leak detection apparatus applied to a heat exchanger.
- In the drawing, the heat exchanger is shown generally at10 and includes heat exchange elements in the form of
plates 11 extending between primary andsecondary chambers - For the purpose of leak detection, the
primary chamber 12 is provided at one end with a source of helium gas 14 and asupply line 16. At the other end of thechamber 12 is provided atap 18 disposed in a take-off line 20. Thesecondary chamber 13 is provided at one end with an airpressure supply line 22 connected to acompressor 24 and at the other end with ahelium detector probe 26. - In use and following removal of the heat exchange liquids from the primary and secondary chambers, the
compressor 24 is started and flow of air at atmospheric pressure through the secondary chamber is established. Helium is them introduced in the primary chamber and allowed to flow out though thetap 18 in the open condition. The tap is then partially closed so that helium continues to flow through the primary chamber under a moderate positive pressure. Helium will flow through any leaks between the primary and secondary chambers under the influence of the differential pressure therebetween and will be detected by thedetector probe 26. Detection of any leaked helium can be expected to take place after approximately 5 minutes of operation, even in the presence of water.
Claims (10)
1. A method for detection of leaks in a plate pack heat exchanger (10) having respective discrete first (13, 22) and second (12, 16) flow paths in mutual thermal contact, the method comprising connecting a helium detector probe (26) at one end of said first flow path and an air compressor means (24) at the other end of said first flow path, said first flow path being open to atmosphere at each end, introducing helium to said second flow path, allowing air to pass through said first flow path under the influence of the compressor means and detecting any helium present therein by the helium detector probe, the pressure of the second flow path being higher than that of the first flow path.
2. A method according to claim 1 , in which the air compressor (24) operates at a pressure sufficient to drive air at from 15 to 30 cu. ft./min. through the first flow path against an outlet of atmospheric pressure.
3. A method according to claim 1 or claim 2 , in which the second flow path (12, 16) is substantially emptied of liquid before introduction of helium therein.
4. A method according to claim 1 or claim 2 , in which both flow paths are substantially emptied of liquid.
5. A method according to any preceding claim, in which the second flow path (12, 16) is also open-ended.
6. A method according to claim 5 , in which the second flow path (12, 16) is provided with a flow restrictor or throttle (18) at the downstream end.
7. A method according to any preceding claim, in which the pressure at which the helium is introduced does not exceed 20 psig.
8. A method according to any preceding claim, in which the helium detector probe (26) detects helium present in the first flow path (13, 22) on the basis of thermal conductivity.
9. A heat exchanger (10) comprising discrete first (13, 22) and second (12, 16) flow paths in mutual thermal contact, said first flow path being open to atmosphere at each end, the heat exchanger including a helium detector probe (26) at one end of said first flow path and an air compressor means (24) at the other end of said first flow path and a source of helium (14) connected to said second flow path.
10. A heat exchanger according to claim 9 , including means (18) to maintain the pressure in said second flow path higher than the pressure in said first flow path.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US11/018,510 US7150180B2 (en) | 1999-12-08 | 2004-12-22 | Detection of leaks in heat exchangers |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GBGB9929062.9A GB9929062D0 (en) | 1999-12-08 | 1999-12-08 | Heat exchangers |
GB9929062.9 | 1999-12-08 |
Publications (1)
Publication Number | Publication Date |
---|---|
US20030056572A1 true US20030056572A1 (en) | 2003-03-27 |
Family
ID=10865963
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US10/149,184 Abandoned US20030056572A1 (en) | 1999-12-08 | 2000-12-08 | Detection of leaks in heat exchangers |
US11/018,510 Expired - Lifetime US7150180B2 (en) | 1999-12-08 | 2004-12-22 | Detection of leaks in heat exchangers |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US11/018,510 Expired - Lifetime US7150180B2 (en) | 1999-12-08 | 2004-12-22 | Detection of leaks in heat exchangers |
Country Status (7)
Country | Link |
---|---|
US (2) | US20030056572A1 (en) |
EP (1) | EP1236028B1 (en) |
AT (1) | ATE292279T1 (en) |
AU (1) | AU2194701A (en) |
DE (1) | DE60019160D1 (en) |
GB (1) | GB9929062D0 (en) |
WO (1) | WO2001042756A1 (en) |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6662633B2 (en) * | 2001-12-19 | 2003-12-16 | Ballard Power Systems Inc. | Method and apparatus for locating internal transfer leaks within fuel cell stacks |
US20070125156A1 (en) * | 2003-04-01 | 2007-06-07 | Thomas Werner | Detection of leaks in heat exchangers |
US20120036823A1 (en) * | 2010-08-11 | 2012-02-16 | General Electric Company | Methods and systems for monitoring a seal assembly |
WO2012051525A2 (en) * | 2010-10-14 | 2012-04-19 | William Robert Martindale | High efficiency cascade-style heat exchanger |
US20120270324A1 (en) * | 2009-11-27 | 2012-10-25 | Inflcon GmbH | Method for testing the tightness of water conducting components in a housing |
US10458879B2 (en) * | 2014-10-24 | 2019-10-29 | Proactive Analytics Limited | Leak testing method and apparatus for use with heat exchangers |
US10914652B2 (en) * | 2018-05-31 | 2021-02-09 | Wcr, Inc. | Leak detection for heat exchanger plate |
US11268877B2 (en) * | 2017-10-31 | 2022-03-08 | Chart Energy & Chemicals, Inc. | Plate fin fluid processing device, system and method |
US20240060735A1 (en) * | 2019-10-07 | 2024-02-22 | Accutest International, Ltd | Detection of leaks in heat exchangers |
Families Citing this family (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DK175691B1 (en) * | 2002-09-11 | 2005-01-17 | Bactoforce As | Method of Examining a Heat Exchanger for Leakage |
US20060016249A1 (en) * | 2004-06-30 | 2006-01-26 | Ache Lani G | Heat recovery test apparatus and method for making and testing the same |
US7454956B1 (en) * | 2005-09-22 | 2008-11-25 | Lopresti William J | Heat exchanger leak detection using mass gas flow metering |
JP4793258B2 (en) * | 2006-12-26 | 2011-10-12 | 株式会社デンソー | Manufacturing method for sealed products |
US7886580B2 (en) * | 2007-12-06 | 2011-02-15 | Apv North America, Inc. | Heat exchanger leak testing method and apparatus |
WO2011030340A2 (en) | 2009-09-09 | 2011-03-17 | Strauss Water Ltd | Liquid filter device |
CN102539081B (en) * | 2011-12-16 | 2014-05-07 | 杭州中泰深冷技术股份有限公司 | Method for detecting sealability of multi-cavity container by using helium gas |
WO2016151568A1 (en) | 2015-03-23 | 2016-09-29 | Strauss Water Ltd. | Water filter and assembly thereof |
RU2670222C1 (en) * | 2017-11-17 | 2018-10-19 | Федеральное казенное военное образовательное учреждение высшего образования "Военная академия Ракетных войск стратегического назначения имени Петра Великого" МО РФ | Method for detecting leakage in a coupling tube heat exchanger |
FI128387B (en) * | 2018-05-11 | 2020-04-15 | Varo Teollisuuspalvelut Oy | Detecting leakage in a soda recovery boiler |
RU2701457C1 (en) * | 2018-05-21 | 2019-09-26 | Общество с ограниченной ответственностью "КОНТУР-НИИРС" | Method of detecting leaks in an air-to-air heat exchanger and a device for its implementation |
DE102022123313B3 (en) | 2022-09-13 | 2023-10-12 | Kassubek Yannik | Method and testing device for detecting leaks in a heat exchanger |
Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3087327A (en) * | 1959-07-24 | 1963-04-30 | Sulzer Ag | Method and device for locating leaks in a heat exchanger |
US3425264A (en) * | 1965-10-05 | 1969-02-04 | Sulzer Ag | Method and apparatus for detecting a leak in a heat exchanger |
US5022265A (en) * | 1987-03-31 | 1991-06-11 | Finn-Aqua | Method and apparatus for leak testing fluid conducting freeze-drying apparatus |
US5835976A (en) * | 1997-06-19 | 1998-11-10 | General Motors Corporation | Non pressurized method for heat exchanger internal leak detection |
US6009745A (en) * | 1997-10-10 | 2000-01-04 | Apv Corporation | Method of leak testing an assembled plate type heat exchanger |
US6035700A (en) * | 1997-10-10 | 2000-03-14 | Apv Corporation | Method of leak testing an assembled plate type heat exchanger |
US6050133A (en) * | 1996-12-02 | 2000-04-18 | True Technology, Inc. | Method and apparatus for detecting leaks in packaging |
US6062068A (en) * | 1993-12-14 | 2000-05-16 | Somerset Technical Laboratories Ltd. | Leakage testing method for a plate heat exchanger |
US6314794B1 (en) * | 1998-11-26 | 2001-11-13 | Alcatel | Method and apparatus for detecting leaks in heat exchangers for motor vehicles |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2574545B1 (en) * | 1984-12-06 | 1987-02-13 | Electricite De France | METHOD FOR DETECTING LEAKS IN AN OPERATING HEAT EXCHANGER |
US5872308A (en) * | 1993-10-02 | 1999-02-16 | Somerset Technical Laboratories Limited | Method of testing a plate heat exchanger for leakage |
GB9612677D0 (en) * | 1996-06-18 | 1996-08-21 | Werner Thomas | Leak detection in heat exchangers |
-
1999
- 1999-12-08 GB GBGB9929062.9A patent/GB9929062D0/en not_active Ceased
-
2000
- 2000-12-08 EP EP00985534A patent/EP1236028B1/en not_active Expired - Lifetime
- 2000-12-08 US US10/149,184 patent/US20030056572A1/en not_active Abandoned
- 2000-12-08 AU AU21947/01A patent/AU2194701A/en not_active Abandoned
- 2000-12-08 DE DE60019160T patent/DE60019160D1/en not_active Expired - Lifetime
- 2000-12-08 AT AT00985534T patent/ATE292279T1/en not_active IP Right Cessation
- 2000-12-08 WO PCT/GB2000/004745 patent/WO2001042756A1/en active IP Right Grant
-
2004
- 2004-12-22 US US11/018,510 patent/US7150180B2/en not_active Expired - Lifetime
Patent Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3087327A (en) * | 1959-07-24 | 1963-04-30 | Sulzer Ag | Method and device for locating leaks in a heat exchanger |
US3425264A (en) * | 1965-10-05 | 1969-02-04 | Sulzer Ag | Method and apparatus for detecting a leak in a heat exchanger |
US5022265A (en) * | 1987-03-31 | 1991-06-11 | Finn-Aqua | Method and apparatus for leak testing fluid conducting freeze-drying apparatus |
US6062068A (en) * | 1993-12-14 | 2000-05-16 | Somerset Technical Laboratories Ltd. | Leakage testing method for a plate heat exchanger |
US6050133A (en) * | 1996-12-02 | 2000-04-18 | True Technology, Inc. | Method and apparatus for detecting leaks in packaging |
US5835976A (en) * | 1997-06-19 | 1998-11-10 | General Motors Corporation | Non pressurized method for heat exchanger internal leak detection |
US6009745A (en) * | 1997-10-10 | 2000-01-04 | Apv Corporation | Method of leak testing an assembled plate type heat exchanger |
US6035700A (en) * | 1997-10-10 | 2000-03-14 | Apv Corporation | Method of leak testing an assembled plate type heat exchanger |
US6314794B1 (en) * | 1998-11-26 | 2001-11-13 | Alcatel | Method and apparatus for detecting leaks in heat exchangers for motor vehicles |
Cited By (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6662633B2 (en) * | 2001-12-19 | 2003-12-16 | Ballard Power Systems Inc. | Method and apparatus for locating internal transfer leaks within fuel cell stacks |
US20070125156A1 (en) * | 2003-04-01 | 2007-06-07 | Thomas Werner | Detection of leaks in heat exchangers |
US7500382B2 (en) * | 2003-04-01 | 2009-03-10 | Accusense Systems Limited | Detection of leaks in heat exchangers |
US9188501B2 (en) * | 2009-11-27 | 2015-11-17 | Inficon Gmbh | Method for testing the tightness of water conducting components in a housing |
US20120270324A1 (en) * | 2009-11-27 | 2012-10-25 | Inflcon GmbH | Method for testing the tightness of water conducting components in a housing |
US8869598B2 (en) * | 2010-08-11 | 2014-10-28 | General Electric Company | Methods and systems for monitoring a seal assembly |
US9170174B2 (en) | 2010-08-11 | 2015-10-27 | General Electric Company | Methods for monitoring a seal assembly |
US20120036823A1 (en) * | 2010-08-11 | 2012-02-16 | General Electric Company | Methods and systems for monitoring a seal assembly |
WO2012051525A2 (en) * | 2010-10-14 | 2012-04-19 | William Robert Martindale | High efficiency cascade-style heat exchanger |
WO2012051525A3 (en) * | 2010-10-14 | 2012-06-21 | William Robert Martindale | High efficiency cascade-style heat exchanger |
US10458879B2 (en) * | 2014-10-24 | 2019-10-29 | Proactive Analytics Limited | Leak testing method and apparatus for use with heat exchangers |
US11268877B2 (en) * | 2017-10-31 | 2022-03-08 | Chart Energy & Chemicals, Inc. | Plate fin fluid processing device, system and method |
US10914652B2 (en) * | 2018-05-31 | 2021-02-09 | Wcr, Inc. | Leak detection for heat exchanger plate |
US20240060735A1 (en) * | 2019-10-07 | 2024-02-22 | Accutest International, Ltd | Detection of leaks in heat exchangers |
Also Published As
Publication number | Publication date |
---|---|
GB9929062D0 (en) | 2000-02-02 |
ATE292279T1 (en) | 2005-04-15 |
EP1236028B1 (en) | 2005-03-30 |
US7150180B2 (en) | 2006-12-19 |
WO2001042756A1 (en) | 2001-06-14 |
DE60019160D1 (en) | 2005-05-04 |
AU2194701A (en) | 2001-06-18 |
EP1236028A1 (en) | 2002-09-04 |
US20050109083A1 (en) | 2005-05-26 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
STCB | Information on status: application discontinuation |
Free format text: ABANDONED -- FAILURE TO RESPOND TO AN OFFICE ACTION |