CN108559839A - Rare earth oxide extraction equipment and its working method - Google Patents
Rare earth oxide extraction equipment and its working method Download PDFInfo
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- CN108559839A CN108559839A CN201810082807.2A CN201810082807A CN108559839A CN 108559839 A CN108559839 A CN 108559839A CN 201810082807 A CN201810082807 A CN 201810082807A CN 108559839 A CN108559839 A CN 108559839A
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/02—Apparatus therefor
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
- C22B7/006—Wet processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0215—Solid material in other stationary receptacles
- B01D11/0253—Fluidised bed of solid materials
- B01D11/0257—Fluidised bed of solid materials using mixing mechanisms, e.g. stirrers, jets
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B59/00—Obtaining rare earth metals
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
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- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Environmental & Geological Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Metallurgy (AREA)
- Geochemistry & Mineralogy (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Apparatus For Making Beverages (AREA)
- Accessories For Mixers (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
The present invention relates to a kind of rare earth oxide extraction equipment more particularly to a kind of rare earth oxide extraction equipment and its working methods.That the technical problem to be solved in the present invention is to provide a kind of effect of extracting is good, rate of extraction is fast and can precisely observe the rare earth oxide extraction equipment of ratio of two solution in allotment recycled for rare earth waste.In order to solve the above-mentioned technical problem, include to place table, the first valve, the first outlet tube, the second outlet tube, third outlet tube, the first the storage box, the second the storage box, the first storage box, the 4th outlet tube etc. the present invention provides such a rare earth oxide extraction equipment recycled for rare earth waste；It places table trailing flank and is welded with back side panel.A kind of rare earth oxide extraction equipment recycled for rare earth waste provided by the present invention, the amount of mother liquor and extract liquor can be accurately controlled by the second amount expects pipe and the first amount expects pipe.
Description
Technical field
The present invention relates to a kind of rare earth oxide extraction equipment more particularly to a kind of rare earth oxide extraction equipment and its works
Make method.
Background technology
Rare earth has the laudatory title of " industrial vitamin ".Nowadays extremely important strategic resource is had become.Rare earth element aoxidizes
Object refer to period of element atom ordinal number be 57 to 71 15 kinds of lanthanide oxides, and with lanthanide series chemical property
Similar scandium（Sc）And yttrium（Y）The oxide of totally 17 kinds of elements.Rare earth element is in oil, chemical industry, metallurgy, weaving, ceramics, glass
The fields such as glass, permanent-magnet material, which are obtained for, to be widely applied.
Extraction, also known as solvent extraction or liquid-liquid extraction also known as extracts, and is different in a solvent using component in system
Solubility carrys out the unit operation of separating mixture.That is, being immiscible at two kinds using substance（Or slightly soluble）Solvent in dissolve
The difference of degree or distribution coefficient, makes solute substance from a kind of method being transferred in solvent in another solvent.Extensive use
In the industry such as chemistry, metallurgy, food, it is common to petroleum refining industry.In addition the immiscible liquid of latter two will be extracted to separate
Operation, be called liquid separation.
At present when being recycled to rare earth waste, the substance in it can be extracted first, so usually require two kinds mutually not
When mixing, and the solution that distribution coefficient is different, and now being mixed to its two kinds of solution, it will not be stirred, so be made
Obtaining two kinds of solution will not adequately contact, so that effect of extracting is bad, rate of extraction is slow, and distribute two kinds of coefficient differences
Solution when in the presence of the ratio that can not be controlled well between solution, therefore there is an urgent need for researching and developing, a kind of effect of extracting is good, rate of extraction
Soon and can precisely observe two solution allotment when ratio for rare earth waste recycle rare earth oxide extraction set
It is standby.
Invention content
（1）Technical problems to be solved
Effect of extracting is bad, rate of extraction is slow in order to overcome by the present invention, and exists not when distributing two kinds of different solution of coefficient
The shortcomings that ratio between solution can be controlled well, that the technical problem to be solved in the present invention is to provide a kind of effect of extracting is good,
Rate of extraction is fast and can precisely observe the rare earth oxide of ratio of two solution in allotment recycled for rare earth waste
Extraction equipment.
（2）Technical solution
In order to solve the above technical problem, the present invention provides such a rare earth oxides recycled for rare earth waste
Extraction equipment includes to place table, the first valve, the first outlet tube, the second outlet tube, third outlet tube, the first the storage box, the
Two the storage box, the first storage box, the 4th outlet tube, the second valve, motor, third valve, the first inlet tube, mixing drum, stirring
Blade, the 4th valve, shaft, stands case, the first transparent glass, the second storage box and back side panel at the second inlet tube, after placing table
Side is welded with back side panel, and the leading flank lower part of back side panel is connected with mixing drum and stands case by bolted connection, quiet
It sets case and is located at mixing drum lower part, mixing drum top left side is welded with the second inlet tube, and the second inlet tube is equipped with the 4th valve, mixes
It closes cylinder top right side and is welded with the first inlet tube, the first inlet tube is equipped with third valve, and the right side of mixing drum passes through bolt
The mode of connection is connected with motor, and shaft is connected with by shaft coupling on the output shaft of motor, is located in the shaft in mixing drum
It is evenly spaced to be welded with stirring blade, among mixing drum bottom and stands and be welded with the 4th outlet tube between box top, the 4th
Outlet tube is equipped with the second valve, and the leading flank for standing case is equipped with the first transparent glass, stands and is welded with third among bottom portion
Outlet tube stands and is welded with the second outlet tube in the middle part of the leading flank of case, and the other end of the second outlet tube is welded with the first outlet tube,
First outlet tube and third outlet tube are equipped with the first valve, place be welded among the table top of table the second storage box and
First storage box, the first storage box are located on rear side of the second storage box, and the first the storage box, the first storage box are equipped in the second storage box
Inside be equipped with the second the storage box, the other end of third outlet tube is connect with the first storage box top center, the first outlet tube it is another
End is connect with the second storage box top center.
Preferably, further include having baiting proportioning device, baiting proportioning device include the first feed hopper, the second feed hopper,
Fixed plate, the 5th valve, third inlet tube, the first amount expects pipe, the 6th valve, the second amount expects pipe and the 4th inlet tube, back side panel
Leading flank be welded with the second amount expects pipe and the first amount expects pipe, the first amount expects pipe is located at the second amount expects pipe right side, the second amount expects pipe
With scale label is carved in the first amount expects pipe, the second amount expects pipe bottom end is connect with the second inlet tube top welded type, the first amount
Expects pipe bottom end is connect with the first inlet tube top welded type, and fixed plate, fixed plate left side are welded at the top of the leading flank of back side panel
It is welded with the first feed hopper, for the first feed hopper on the left of fixed plate, the first feed hopper bottom end is welded with the 4th inlet tube, and the 4th
Inlet tube is equipped with the 6th valve, and the 4th inlet tube bottom end is connect with welded type at the top of the second amount expects pipe, welding on the right side of fixed plate
There are the second feed hopper, the second feed hopper bottom end to be welded with third inlet tube, third inlet tube is equipped with the 5th valve, third feed liquor
Tube bottom end is connect with welded type at the top of the first amount expects pipe.
Preferably, further include having pumping equipment, pumping equipment includes drain pipe, collecting vessel, fixed block, connector and the 7th
Valve is welded with fixed block at left and right sides of the leading flank top of back side panel, is provided with card slot in two fixed blocks, in two card slots
It is placed with collecting vessel, two collecting vessel tops are connected with connector by welding, under the second amount expects pipe and the first amount expects pipe
Portion is connected with drain pipe by way of flanged joint, and drain pipe is equipped with the 7th valve, the other end of drain pipe respectively with
Connector connects.
Preferably, further include having lid and handle, be stamped lid on the first feed hopper, lid is by the top of the first feed hopper
It blocks, lid is also stamped on the second feed hopper, lid will block at the top of the second feed hopper, and handle is welded among cap top
Hand.
Preferably, further include having magnet, the fixed block in card slot is equipped with magnet, and magnet is located at the fixed block in card slot
Top center, the mode that magnet is connected by screw are connect with fixed block, and the shape of magnet is circle.
Preferably, further include having the second transparent glass, the leading flank of collecting vessel is equipped with the second transparent glass, the second transparent glass
Glass is connected to the front side of collecting vessel by way of glue bonding, and the shape of the second transparent glass is rectangle.
Preferably, the material of stirring blade is Q235 steel, and shaft is equipped with multiple stirring blades, stirring blade uniform intervals
Be distributed in shaft, stirring blade is connect with shaft by welding, and the shape of stirring blade is S-shaped.
Preferably, the material of fixed plate is Q235 steel, and back side panel forward upper is connected with fixed plate by welding,
The trailing flank of fixed plate and the fixed connection of back side panel forward upper, fixed plate are located in the second amount expects pipe and the first amount expects pipe
Portion.
Preferably, the material of back side panel is Q235 steel, and the trailing flank for placing table is connected with back side panel by welding,
The leading flank lower part of back side panel and the fixed connection in trailing flank for placing table, back side panel are in be vertically arranged.
Operation principle：When using this equipment, staff opens the 4th valve and third valve first, then passes through again
Second inlet tube and the first inlet tube pour into a certain amount of mother liquor and extract liquor in mixing drum respectively, after respectively pouring into right amount, work
People stops batch turning, and the 4th valve and third valve are closed.Then motor rotation is controlled again, and then drives shaft rotation, from
And drive stirring blade to rotate, at this time stirring blade in mixing drum mother liquor and extract liquor mix, when in mixing drum
After mixing, control motor is stopped for mother liquor and extract liquor.Then the second valve is opened again, it is mixed in mixing drum
Mother liquor and extract liquor, which are then entered by the 4th outlet tube, to be stood in case, when mixed mother liquor in mixing drum and extract liquor all into
After entering to stand in case, worker closes the second valve.A period of time is stood, mother liquor and extract liquor are during standing, for more
Standing situation including facilitating staff to understand it, staff can be observed by the first transparent glass, and solution occurs
After apparent layering, the first valve on third outlet tube is opened if lower layer is required solution, it is quiet to stand bottom in case at this time
It sets complete solution to flow into the first storage box by third outlet tube, complete solution is stood by the when standing bottom in case
After three outlet tubes all flow into the first storage box, staff closes the first valve on third outlet tube, then works
Personnel again open the first valve on the first outlet tube, stand remaining unwanted solution in case at this time and then go out liquid by first
Pipe flows into the second storage box, and the second storage box is all flowed by the first outlet tube when standing remaining unwanted solution in case
After interior, staff closes the first valve on the first outlet tube.Then staff respectively will be in the second storage box and the
The second the storage box in one storage box and the extraction of the first the storage box.
Because further including having baiting proportioning device, baiting proportioning device includes the first feed hopper, the second feed hopper, fixation
Plate, the 5th valve, third inlet tube, the first amount expects pipe, the 6th valve, the second amount expects pipe and the 4th inlet tube, before back side panel
Side is welded with the second amount expects pipe and the first amount expects pipe, and the first amount expects pipe is located at the second amount expects pipe right side, the second amount expects pipe and the
Scale label is carved in one amount expects pipe, the second amount expects pipe bottom end is connect with the second inlet tube top welded type, the first amount expects pipe
Bottom end is connect with the first inlet tube top welded type, and fixed plate is welded at the top of the leading flank of back side panel, is welded on the left of fixed plate
There is the first feed hopper, for the first feed hopper on the left of fixed plate, the first feed hopper bottom end is welded with the 4th inlet tube, the 4th feed liquor
Pipe is equipped with the 6th valve, and the 4th inlet tube bottom end is connect with the second amount expects pipe top welded type, and fixed plate right side is welded with the
Two feed hoppers, the second feed hopper bottom end are welded with third inlet tube, and third inlet tube is equipped with the 5th valve, third inlet tube bottom
End is connect with welded type at the top of the first amount expects pipe, and staff opens the 6th valve and the 5th valve first, then passes through again
First feed hopper pours into a certain amount of mother liquor in the second amount expects pipe, and pours into a certain amount of extract liquor by the second feed hopper and exist
In first amount expects pipe, staff can accurately determine according to the scale label in the second amount expects pipe and the first amount expects pipe at this time
The amount of mother liquor, after respectively pouring into right amount, staff stops batch turning.
Because further including having pumping equipment, pumping equipment includes drain pipe, collecting vessel, fixed block, connector and the 7th valve
Door, is welded with fixed block at left and right sides of the leading flank top of back side panel, in two fixed blocks in be provided with card slot, in two card slots
It is placed with collecting vessel, two collecting vessel tops are connected with connector by welding, under the second amount expects pipe and the first amount expects pipe
Portion is connected with drain pipe by way of flanged joint, and drain pipe is equipped with the 7th valve, the other end of drain pipe respectively with
Connector connects, to avoid staff from not paying attention to slightly pouring into the second amount expects pipe and the first amount expects pipe respectively excessively at work
Mother liquor and extract liquor when, staff can open the 7th valve at this time, the mother liquor in the second amount expects pipe and the first amount expects pipe
Entered in collecting vessel by two drain pipes respectively with extract liquor, after the mother liquor or extract liquor arrival standard of discharge, worker is by
Seven valves close, then again by the drain pipe being connect with connector extract, and by two collecting vessels mother liquor and extract liquor processing be
It can.
Because further including having lid and handle, lid is stamped on the first feed hopper, lid keeps off the top of the first feed hopper
Firmly, lid is also stamped on the second feed hopper, lid will block at the top of the second feed hopper, and handle is welded among cap top
Hand covers after staff pours into suitable mother liquor and extract liquor in the first feed hopper and the second feed hopper respectively, and by two
Son covers, and can so prevent mother liquor and the too fast volatilization of extract liquor, influences the quality of extraction.
Because further including having magnet, the fixed block in card slot is equipped with magnet, and magnet is located at the top of the fixed block in card slot
Among portion, the mode that magnet is connected by screw is connect with fixed block, and the shape of magnet is circle, because collecting vessel material is iron
Matter, under the action of magnet, collecting vessel attracts each other with magnet, so can preferably fix collecting vessel.
Because further including having the second transparent glass, the leading flank of collecting vessel is equipped with the second transparent glass, the second transparent glass
The front side of collecting vessel is connected to by way of glue bonding, the shape of the second transparent glass is rectangle, in the second transparent glass
Under the action of, staff can observe the amount of mother liquor or extract liquor in collecting vessel by the second transparent glass.
Because the material of stirring blade is Q235 steel, shaft is equipped with multiple stirring blades, and stirring blade is evenly spaced
It is distributed in shaft, stirring blade is connect with shaft by welding, and the shape of stirring blade is S-shaped, Q235 steel hardness
Height, and be unlikely to deform, making this equipment, the service life is longer.
Because the material of fixed plate is Q235 steel, back side panel forward upper is connected with fixed plate by welding, Gu
The trailing flank of fixed board and the fixed connection of back side panel forward upper, fixed plate are located at the second amount expects pipe and the first amount expects pipe top,
Q235 steel hardness is high, and is unlikely to deform, and making this equipment, the service life is longer.
Because the material of back side panel is Q235 steel, the trailing flank for placing table is connected with back side panel by welding, after
The leading flank lower part of side plate and the fixed connection in trailing flank for placing table, back side panel is in being vertically arranged, and Q235 steel hardness is high, and not
Yielding, making this equipment, the service life is longer.
（3）Advantageous effect
A kind of rare earth oxide extraction equipment recycled for rare earth waste provided by the present invention, passes through the second amount expects pipe
The amount of mother liquor and extract liquor can be accurately controlled with the first amount expects pipe, its two kinds of substances can be stirred later, be made two kinds of objects
It is adequately fused between matter, has reached that effect of extracting is good, rate of extraction is fast and can precisely observe ratio of two solution in allotment
Effect.
Description of the drawings
Fig. 1 is the first dimensional structure diagram of the present invention.
Fig. 2 is second of dimensional structure diagram of the present invention.
Fig. 3 is the third dimensional structure diagram of the present invention.
Fig. 4 is the first dimensional structure diagram of fixed block of the present invention.
Fig. 5 is the 4th kind of dimensional structure diagram of the present invention.
Fig. 6 is second of dimensional structure diagram of fixed block of the present invention.
Fig. 7 is the dimensional structure diagram of collecting vessel of the present invention.
Label in attached drawing be：1- placement tables, the first valves of 2-, the first outlet tubes of 3-, the second outlet tubes of 4-, 5- thirds go out
Liquid pipe, the first the storage box of 6-, the second the storage box of 7-, the first storage boxes of 8-, the 4th outlet tubes of 9-, the second valves of 10-, 11- motors,
12- third valves, the first inlet tubes of 13-, 14- mixing drums, 15- stirring blades, the second inlet tubes of 16-, the 4th valves of 17-, 18-
Shaft, 19- stand case, the first transparent glass of 20-, the second storage boxes of 21-, 22- back side panels, 23- baiting proportioning devices, 231- the
One feed hopper, the second feed hoppers of 232-, 233- fixed plates, the 5th valves of 234-, 235- third inlet tubes, the first amounts of 236- material
Pipe, the 6th valves of 237-, 238- the second amount expects pipes, the 4th inlet tubes of 239-, 24- pumping equipments, 241- drain pipes, 242- are collected
Bucket, 243- fixed blocks, 244- connectors, the 7th valves of 245-, 25- lids, 26- handles, 27- magnet, the second transparent glass of 28-.
Specific implementation mode
The present invention is further illustrated with reference to the accompanying drawings and examples.
Embodiment 1
A kind of rare earth oxide extraction equipment recycled for rare earth waste includes as shown in figs. 1-7 to place table 1, the
One valve 2, the first outlet tube 3, the second outlet tube 4, third outlet tube 5, the first the storage box 6, the storage of the second the storage box 7, first
Case 8, the 4th outlet tube 9, the second valve 10, motor 11, third valve 12, the first inlet tube 13, mixing drum 14, stirring blade
15, the second inlet tube 16, the 4th valve 17, shaft 18, standing case 19, the first transparent glass 20, the second storage box 21 and rear side
Plate 22 places 1 trailing flank of table and is welded with back side panel 22, and the leading flank lower part of back side panel 22 is connected with by bolted connection
Mixing drum 14 and standing case 19, stand case 19 and are located at 14 lower part of mixing drum, 14 top left side of mixing drum is welded with the second inlet tube
16, the second inlet tube 16 is equipped with the 4th valve 17, and 14 top right side of mixing drum is welded with the first inlet tube 13, the first inlet tube
13 are equipped with third valve 12, and the right side of mixing drum 14 is connected with motor 11 by bolted connection, motor 11 it is defeated
Shaft 18 is connected with by shaft coupling on shaft, it is evenly spaced in the shaft 18 in mixing drum 14 to be welded with stirring blade
15, it is welded with the 4th outlet tube 9 between 14 bottom of mixing drum centre and 19 top of standing case, the 4th outlet tube 9 is equipped with second
Valve 10, the leading flank for standing case 19 are equipped with the first transparent glass 20, stand and are welded with third outlet tube 5 among 19 bottom of case,
It standing and is welded with the second outlet tube 4 in the middle part of the leading flank of case 19, the other end of the second outlet tube 4 is welded with the first outlet tube 3, the
One outlet tube 3 and third outlet tube 5 are equipped with the first valve 2, place and are welded with the second storage box among the table top of table 1
21 and first storage box 8, the first storage box 8 be located at 21 rear side of the second storage box, the first the storage box be equipped in the second storage box 21
6, the first storage box 8 is interior equipped with the second the storage box 7, and the other end of third outlet tube 5 is connect with 8 top center of the first storage box,
The other end of first outlet tube 3 is connect with 21 top center of the second storage box.
Embodiment 2
A kind of rare earth oxide extraction equipment recycled for rare earth waste includes as shown in figs. 1-7 to place table 1, the
One valve 2, the first outlet tube 3, the second outlet tube 4, third outlet tube 5, the first the storage box 6, the storage of the second the storage box 7, first
Case 8, the 4th outlet tube 9, the second valve 10, motor 11, third valve 12, the first inlet tube 13, mixing drum 14, stirring blade
15, the second inlet tube 16, the 4th valve 17, shaft 18, standing case 19, the first transparent glass 20, the second storage box 21 and rear side
Plate 22 places 1 trailing flank of table and is welded with back side panel 22, and the leading flank lower part of back side panel 22 is connected with by bolted connection
Mixing drum 14 and standing case 19, stand case 19 and are located at 14 lower part of mixing drum, 14 top left side of mixing drum is welded with the second inlet tube
16, the second inlet tube 16 is equipped with the 4th valve 17, and 14 top right side of mixing drum is welded with the first inlet tube 13, the first inlet tube
13 are equipped with third valve 12, and the right side of mixing drum 14 is connected with motor 11 by bolted connection, motor 11 it is defeated
Shaft 18 is connected with by shaft coupling on shaft, it is evenly spaced in the shaft 18 in mixing drum 14 to be welded with stirring blade
15, it is welded with the 4th outlet tube 9 between 14 bottom of mixing drum centre and 19 top of standing case, the 4th outlet tube 9 is equipped with second
Valve 10, the leading flank for standing case 19 are equipped with the first transparent glass 20, stand and are welded with third outlet tube 5 among 19 bottom of case,
It standing and is welded with the second outlet tube 4 in the middle part of the leading flank of case 19, the other end of the second outlet tube 4 is welded with the first outlet tube 3, the
One outlet tube 3 and third outlet tube 5 are equipped with the first valve 2, place and are welded with the second storage box among the table top of table 1
21 and first storage box 8, the first storage box 8 be located at 21 rear side of the second storage box, the first the storage box be equipped in the second storage box 21
6, the first storage box 8 is interior equipped with the second the storage box 7, and the other end of third outlet tube 5 is connect with 8 top center of the first storage box,
The other end of first outlet tube 3 is connect with 21 top center of the second storage box.
Further include having baiting proportioning device 23, baiting proportioning device 23 includes the first feed hopper 231, the second feed hopper
232, fixed plate 233, the 5th valve 234, third inlet tube 235, the first amount expects pipe 236, the 6th valve 237, the second amount expects pipe
238 and the 4th inlet tube 239, the leading flank of back side panel 22 be welded with the second amount expects pipe 238 and the first amount expects pipe 236, the first amount
Expects pipe 236 is located at 238 right side of the second amount expects pipe, and scale label is carved in the second amount expects pipe 238 and the first amount expects pipe 236, the
Two amount expects pipes, 238 bottom end is connect with 16 top welded type of the second inlet tube, and 236 bottom end of the first amount expects pipe is pushed up with the first inlet tube 13
Welded type connection is held, fixed plate 233 is welded at the top of the leading flank of back side panel 22,233 left side of fixed plate is welded with the first charging
Bucket 231, the first feed hopper 231 are welded with the 4th inlet tube 239 through 233 left side of fixed plate, 231 bottom end of the first feed hopper, the
Four inlet tubes 239 are equipped with the 6th valve 237, and 239 bottom end of the 4th inlet tube is connect with 238 top welded type of the second amount expects pipe,
The right side of fixed plate 233 is welded with the second feed hopper 232, and 232 bottom end of the second feed hopper is welded with third inlet tube 235, third into
Liquid pipe 235 is equipped with the 5th valve 234, and 235 bottom end of third inlet tube is connect with 236 top welded type of the first amount expects pipe.
Further include having pumping equipment 24, pumping equipment 24 includes drain pipe 241, collecting vessel 242, fixed block 243, connector
244 and the 7th valve 245, fixed block 243 is welded at left and right sides of the leading flank top of back side panel 22, in two fixed blocks 243
It is provided with card slot, collecting vessel 242 is placed in two card slots, two collecting vessels, 242 top is connected with by welding to be connect
First 244, the second amount expects pipe 238 and 236 lower part of the first amount expects pipe are connected with drain pipe 241 by way of flanged joint, row
Liquid pipe 241 is equipped with the 7th valve 245, and the other end of drain pipe 241 is connect with connector 244 respectively.
Further include having lid 25 and handle 26, be stamped lid 25 on the first feed hopper 231, lid 25 is by the first feed hopper
231 top is blocked, and lid 25 is also stamped on the second feed hopper 232, and lid 25 blocks the top of the second feed hopper 232, lid
Sub 25 top centers are welded with handle 26.
Further include having magnet 27, the fixed block 243 in card slot is equipped with magnet 27, and magnet 27 is located at the fixed block in card slot
243 top center, the mode that magnet 27 is connected by screw are connect with fixed block 243, and the shape of magnet 27 is circle.
Further include having the second transparent glass 28, the leading flank of collecting vessel 242 is equipped with the second transparent glass 28, the second transparent glass
Glass 28 is connected to the front side of collecting vessel 242 by way of glue bonding, and the shape of the second transparent glass 28 is rectangle.
The material of stirring blade 15 is Q235 steel, and shaft 18 is equipped with multiple stirring blades 15, between stirring blade 15 is uniform
Every be distributed in shaft 18, stirring blade 15 is connect with shaft 18 by welding, and the shape of stirring blade 15 is S
Shape.
The material of fixed plate 233 is Q235 steel, and 22 forward upper of back side panel is connected with fixed plate by welding
233, trailing flank and the fixed connection of 22 forward upper of back side panel of fixed plate 233, fixed plate 233 are located at the second amount expects pipe 238
With 236 top of the first amount expects pipe.
The material of back side panel 22 is Q235 steel, and the trailing flank for placing table 1 is connected with back side panel 22 by welding, after
The leading flank lower part of side plate 22 and the fixed connection in trailing flank for placing table 1, back side panel 22 are in be vertically arranged.
Operation principle：When using this equipment, staff opens the 4th valve 17 and third valve 12 first, then again
A certain amount of mother liquor and extract liquor are poured into respectively in mixing drum 14 by the second inlet tube 16 and the first inlet tube 13, are respectively poured into
After appropriate, worker stops batch turning, and the 4th valve 17 and third valve 12 are closed.Then the rotation of motor 11 is controlled again, in turn
Drive shaft 18 rotate, to drive stirring blade 15 rotate, at this time stirring blade 15 in mixing drum 14 mother liquor and extraction
Liquid is mixed, when in mixing drum 14 mother liquor and extract liquor after mixing, control motor 11 be stopped.Then again by
Two valves 10 are opened, and mixed mother liquor and extract liquor, which are then entered by the 4th outlet tube 9, in mixing drum 14 stands in case 19, when
After mixed mother liquor and extract liquor fully enter in standing case 19 in mixing drum 14, worker closes the second valve 10.It stands
For a period of time, mother liquor and extract liquor understand the standing situation including it for more convenient staff, work during standing
Personnel can be observed by the first transparent glass 20, after apparent layering occurs in solution, by third if lower layer is required solution
The first valve 2 on outlet tube 5 is opened, and is stood the complete solution of bottom standing in case 19 at this time and is passed through the inflow of third outlet tube 5
In first storage box 8, pass through all the first storage boxes of inflow of third outlet tube 5 when standing the bottom complete solution of standing in case 19
After in 8, staff closes the first valve 2 on third outlet tube 5, and subsequent staff again will be on the first outlet tube 3
First valve 2 is opened, and is stood remaining unwanted solution in case 19 at this time and is then flowed into the second storage box 21 by the first outlet tube 3
Interior, after standing remaining the interior unwanted solution of case 19 by the first outlet tube 3 all the second storage boxes of inflow 21, work people
Member closes the first valve 2 on the first outlet tube 3.Then staff is respectively by 21 interior and the first storage box of the second storage box
The second the storage box 7 in 8 and the extraction of the first the storage box 6.
Because further including having baiting proportioning device 23, baiting proportioning device 23 includes the charging of the first feed hopper 231, second
Bucket 232, fixed plate 233, the 5th valve 234, third inlet tube 235, the first amount expects pipe 236, the 6th valve 237, the second amount material
Pipe 238 and the 4th inlet tube 239, the leading flank of back side panel 22 are welded with the second amount expects pipe 238 and the first amount expects pipe 236, and first
Amount expects pipe 236 is located at 238 right side of the second amount expects pipe, and scale label is carved in the second amount expects pipe 238 and the first amount expects pipe 236,
Second amount expects pipe, 238 bottom end is connect with 16 top welded type of the second inlet tube, 236 bottom end of the first amount expects pipe and the first inlet tube 13
The connection of top welded type, is welded with fixed plate 233 at the top of the leading flank of back side panel 22,233 left side of fixed plate be welded with first into
Hopper 231, the first feed hopper 231 are welded with the 4th inlet tube 239 through 233 left side of fixed plate, 231 bottom end of the first feed hopper,
4th inlet tube 239 is equipped with the 6th valve 237, and 239 bottom end of the 4th inlet tube connects with 238 top welded type of the second amount expects pipe
It connects, 233 right side of fixed plate is welded with the second feed hopper 232, and 232 bottom end of the second feed hopper is welded with third inlet tube 235, third
Inlet tube 235 is equipped with the 5th valve 234, and 235 bottom end of third inlet tube is connect with 236 top welded type of the first amount expects pipe, first
First staff opens the 6th valve 237 and the 5th valve 234, is then poured into again by the first feed hopper 231 a certain amount of
Mother liquor pours into a certain amount of extract liquor in the first amount expects pipe 236 in the second amount expects pipe 238, and by the second feed hopper 232,
Staff can accurately determine mother liquor according to the scale label in the second amount expects pipe 238 and the first amount expects pipe 236 at this time
Amount, after respectively pouring into right amount, staff stops batch turning.
Because further including having pumping equipment 24, pumping equipment 24 include drain pipe 241, collecting vessel 242, fixed block 243,
The leading flank top left and right sides of connector 244 and the 7th valve 245, back side panel 22 is welded with fixed block 243, two fixed blocks
It is provided with card slot in 243, collecting vessel 242 is placed in two card slots, two collecting vessels, 242 top connects by welding
It is connected to connector 244, the second amount expects pipe 238 and 236 lower part of the first amount expects pipe are connected with drain pipe by way of flanged joint
241, drain pipe 241 is equipped with the 7th valve 245, and the other end of drain pipe 241 is connect with connector 244 respectively, to avoid work
Personnel do not pay attention to slightly pouring into excessive mother liquor and extraction in the second amount expects pipe 238 and the first amount expects pipe 236 respectively at work
When liquid, staff can open the 7th valve 245 at this time, the second amount expects pipe 238 and the mother liquor in the first amount expects pipe 236 and extraction
Liquid is taken to enter in collecting vessel 242 by two drain pipes 241 respectively, after the mother liquor or extract liquor arrival standard of discharge, worker will
7th valve 245 is closed, and then again extracts the drain pipe 241 being connect with connector 244, and by the mother liquor in two collecting vessels 242
With extract liquor processing.
Because further including having lid 25 and handle 26, lid 25 is stamped on the first feed hopper 231, lid 25 is fed first
The top of bucket 231 is blocked, and lid 25 is also stamped on the second feed hopper 232, and lid 25 blocks the top of the second feed hopper 232,
25 top center of lid is welded with handle 26, when staff pours into suitable mother liquor and extract liquor in the first feed hopper respectively
231 and second in feed hopper 232 after, and two lids 25 are covered, can so prevent mother liquor and the too fast volatilization of extract liquor, influence
The quality of extraction.
Because further including having magnet 27, the fixed block 243 in card slot is equipped with magnet 27, and magnet 27 is located at consolidating in card slot
Determine the top center of block 243, the mode that magnet 27 is connected by screw is connect with fixed block 243, and the shape of magnet 27 is circle,
Because 242 material of collecting vessel is irony, under the action of magnet 27, collecting vessel 242 attracts each other with magnet 27, so can be better
Fixed collecting vessel 242.
Because further including having the second transparent glass 28, the leading flank of collecting vessel 242 is equipped with the second transparent glass 28, and second thoroughly
Bright glass 28 is connected to the front side of collecting vessel 242 by way of glue bonding, and the shape of the second transparent glass 28 is rectangle,
Under the action of second transparent glass 28, staff can observe mother liquor or extraction in collecting vessel 242 by the second transparent glass 28
Take the amount of liquid.
Because the material of stirring blade 15 is Q235 steel, shaft 18 is equipped with multiple stirring blades 15, and stirring blade 15 is equal
Even interval is distributed in shaft 18, and stirring blade 15 is connect with shaft 18 by welding, the shape of stirring blade 15
For S-shaped, Q235 steel hardness is high, and is unlikely to deform, and making this equipment, the service life is longer.
Because the material of fixed plate 233 is Q235 steel, 22 forward upper of back side panel is connected with fixation by welding
Plate 233, trailing flank and the fixed connection of 22 forward upper of back side panel of fixed plate 233, fixed plate 233 are located at the second amount expects pipe
238 and 236 top of the first amount expects pipe, Q235 steel hardness is high, and is unlikely to deform, and making this equipment, the service life is longer.
Because the material of back side panel 22 is Q235 steel, the trailing flank for placing table 1 is connected with back side panel by welding
22, the leading flank lower part of back side panel 22 and the fixed connection in trailing flank for placing table 1, back side panel 22 are in be vertically arranged, Q235 steel
Hardness is high, and is unlikely to deform, and making this equipment, the service life is longer.
The preferred embodiment of the present invention above described embodiment only expresses, the description thereof is more specific and detailed, but simultaneously
Cannot the limitation to the scope of the claims of the present invention therefore be interpreted as.It should be pointed out that for those of ordinary skill in the art
For, without departing from the inventive concept of the premise, several deformations can also be made, improves and substitutes, these belong to this hair
Bright protection domain.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.
Claims (1)
1. a kind of working method of the rare earth oxide extraction equipment recycled for rare earth waste, which is characterized in that described
Rare earth oxide extraction equipment include：Place table（1）, the first valve（2）, the first outlet tube（3）, the second outlet tube（4）,
Three outlet tubes（5）, the first the storage box（6）, the second the storage box（7）, the first storage box（8）, the 4th outlet tube（9）, the second valve
（10）, motor（11）, third valve（12）, the first inlet tube（13）, mixing drum（14）, stirring blade（15）, the second inlet tube
（16）, the 4th valve（17）, shaft（18）, stand case（19）, the first transparent glass（20）, the second storage box（21）And back side panel
（22）, place table（1）Trailing flank is welded with back side panel（22）, back side panel（22）Leading flank lower part by bolted connection
It is connected with mixing drum（14）With standing case（19）, stand case（19）Positioned at mixing drum（14）Lower part, mixing drum（14）Top left side
It is welded with the second inlet tube（16）, the second inlet tube（16）It is equipped with the 4th valve（17）, mixing drum（14）Top right side is welded
There is the first inlet tube（13）, the first inlet tube（13）It is equipped with third valve（12）, mixing drum（14）Right side pass through bolt
The mode of connection is connected with motor（11）, motor（11）Output shaft on shaft is connected with by shaft coupling（18）, it is located at mixing
Cylinder（14）Interior shaft（18）It is above evenly spaced to be welded with stirring blade（15）, mixing drum（14）Bottom centre and standing case
（19）The 4th outlet tube is welded between top（9）, the 4th outlet tube（9）It is equipped with the second valve（10）, stand case（19）'s
Leading flank is equipped with the first transparent glass（20）, stand case（19）Third outlet tube is welded among bottom（5）, stand case（19）'s
It is welded with the second outlet tube in the middle part of leading flank（4）, the second outlet tube（4）The other end be welded with the first outlet tube（3）, first goes out
Liquid pipe（3）With third outlet tube（5）It is equipped with the first valve（2）, place table（1）Table top among be welded with second and deposit
Storage tank（21）With the first storage box（8）, the first storage box（8）Positioned at the second storage box（21）Rear side, the second storage box（21）It is interior
Equipped with the first the storage box（6）, the first storage box（8）Inside it is equipped with the second the storage box（7）, third outlet tube（5）The other end and
One storage box（8）Top center connects, the first outlet tube（3）The other end and the second storage box（21）Top center connects；
The rare earth oxide extraction equipment further includes having baiting proportioning device（23）, baiting proportioning device（23）Include
One feed hopper（231）, the second feed hopper（232）, fixed plate（233）, the 5th valve（234）, third inlet tube（235）, first
Measure expects pipe（236）, the 6th valve（237）, the second amount expects pipe（238）With the 4th inlet tube（239）, back side panel（22）Leading flank
It is welded with the second amount expects pipe（238）With the first amount expects pipe（236）, the first amount expects pipe（236）Positioned at the second amount expects pipe（238）It is right
Side, the second amount expects pipe（238）With the first amount expects pipe（236）On be carved with scale label, the second amount expects pipe（238）Bottom end and second
Inlet tube（16）Top welded type connection, the first amount expects pipe（236）Bottom end and the first inlet tube（13）Top welded type connection, after
Side plate（22）Leading flank at the top of be welded with fixed plate（233）, fixed plate（233）Left side is welded with the first feed hopper（231）, the
One feed hopper（231）Through fixed plate（233）Left side, the first feed hopper（231）Bottom end is welded with the 4th inlet tube（239）, the
Four inlet tubes（239）It is equipped with the 6th valve（237）, the 4th inlet tube（239）Bottom end and the second amount expects pipe（238）It welds at top
Formula connects, fixed plate（233）Right side is welded with the second feed hopper（232）, the second feed hopper（232）Bottom end is welded with third feed liquor
Pipe（235）, third inlet tube（235）It is equipped with the 5th valve（234）, third inlet tube（235）Bottom end and the first amount expects pipe
（236）Top welded type connection；
The working method, including：Staff is by the 6th valve（237）With the 5th valve（234）It opens, then passes through again
First feed hopper（231）A certain amount of mother liquor is poured into the second amount expects pipe（238）It is interior, and pass through the second feed hopper（232）It pours into
A certain amount of extract liquor is in the first amount expects pipe（236）Interior, staff is according to the second amount expects pipe at this time（238）With the first amount expects pipe
（236）On scale label accurately determine the amount of mother liquor, respectively pour into it is appropriate after, staff stops batch turning.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810082807.2A CN108559839A (en) | 2016-12-18 | 2016-12-18 | Rare earth oxide extraction equipment and its working method |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611173247.9A CN106521149A (en) | 2016-12-18 | 2016-12-18 | Rare earth oxide extraction equipment for rare earth waste recycling |
| CN201810082807.2A CN108559839A (en) | 2016-12-18 | 2016-12-18 | Rare earth oxide extraction equipment and its working method |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611173247.9A Division CN106521149A (en) | 2016-12-18 | 2016-12-18 | Rare earth oxide extraction equipment for rare earth waste recycling |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108559839A true CN108559839A (en) | 2018-09-21 |
Family
ID=58341033
Family Applications (7)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810082807.2A Withdrawn CN108559839A (en) | 2016-12-18 | 2016-12-18 | Rare earth oxide extraction equipment and its working method |
| CN201810302798.3A Withdrawn CN108396140A (en) | 2016-12-18 | 2016-12-18 | Rare earth oxide extraction equipment and its working method |
| CN201810083422.8A Withdrawn CN108588421A (en) | 2016-12-18 | 2016-12-18 | The rare earth oxide extraction equipment and its working method of rare earth waste recycling |
| CN201810302792.6A Withdrawn CN108559847A (en) | 2016-12-18 | 2016-12-18 | Rare earth oxide extraction equipment |
| CN201810083344.1A Withdrawn CN108251641A (en) | 2016-12-18 | 2016-12-18 | A kind of rare earth oxide extraction equipment |
| CN201810083360.0A Withdrawn CN108559840A (en) | 2016-12-18 | 2016-12-18 | The rare earth oxide extraction equipment recycled for rare earth waste |
| CN201611173247.9A Pending CN106521149A (en) | 2016-12-18 | 2016-12-18 | Rare earth oxide extraction equipment for rare earth waste recycling |
Family Applications After (6)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810302798.3A Withdrawn CN108396140A (en) | 2016-12-18 | 2016-12-18 | Rare earth oxide extraction equipment and its working method |
| CN201810083422.8A Withdrawn CN108588421A (en) | 2016-12-18 | 2016-12-18 | The rare earth oxide extraction equipment and its working method of rare earth waste recycling |
| CN201810302792.6A Withdrawn CN108559847A (en) | 2016-12-18 | 2016-12-18 | Rare earth oxide extraction equipment |
| CN201810083344.1A Withdrawn CN108251641A (en) | 2016-12-18 | 2016-12-18 | A kind of rare earth oxide extraction equipment |
| CN201810083360.0A Withdrawn CN108559840A (en) | 2016-12-18 | 2016-12-18 | The rare earth oxide extraction equipment recycled for rare earth waste |
| CN201611173247.9A Pending CN106521149A (en) | 2016-12-18 | 2016-12-18 | Rare earth oxide extraction equipment for rare earth waste recycling |
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| CN (7) | CN108559839A (en) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109666806B (en) * | 2017-07-19 | 2020-11-10 | 东阳市川泽户外用品有限公司 | Horizontal extraction device for rare earth feed liquid |
| CN113265537B (en) * | 2021-05-19 | 2023-03-24 | 福建省华裕天恒科技有限公司 | Rare earth oxide extraction equipment for recycling rare earth waste |
| CN113249569B (en) * | 2021-05-19 | 2022-08-26 | 福建省华裕天恒科技有限公司 | Rare earth waste recycling oxide extraction equipment's measuring device |
| CN116002915B (en) * | 2023-01-05 | 2023-07-18 | 江西理工大学 | A device and method for recovering high-purity molybdenum trioxide from molybdenum-containing wastewater |
| CN116499853B (en) * | 2023-06-19 | 2023-08-18 | 北京建工环境修复股份有限公司 | Soil heavy metal ion extractor |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6036630A (en) * | 1999-03-26 | 2000-03-14 | Praxair Technology, Inc. | Centrifugal extraction process |
| US7964029B2 (en) * | 2006-07-17 | 2011-06-21 | Thar Instrument, Inc. | Process flowstream collection system |
| CN203451594U (en) * | 2013-08-19 | 2014-02-26 | 中铝稀土（常州）有限公司 | Extraction tank of rare earth oxide production line |
| CN204237845U (en) * | 2013-12-19 | 2015-04-01 | 宜兴新威利成稀土有限公司 | Rare earth chloride extraction plant |
| JP6197051B2 (en) * | 2014-02-05 | 2017-09-13 | 株式会社日立製作所 | Rare earth element separation method and separation apparatus |
| CN104353375A (en) * | 2014-11-06 | 2015-02-18 | 内蒙古包钢稀土(集团)高科技股份有限公司 | Automatic preparing device and method for organic saponification alkaline liquor in rare earth wet-process smelting process |
| CN204745733U (en) * | 2015-05-20 | 2015-11-11 | 赣州通诚稀土新材料有限公司 | Full -automatic extraction device of high -purity praseodymia neodymium |
| CN104946895B (en) * | 2015-06-29 | 2017-04-26 | 包头市新世纪稀土有限责任公司 | Rare earth compound recycling method utilizing waste rare earth polishing powder |
| CN204981998U (en) * | 2015-09-18 | 2016-01-20 | 赣州齐飞新材料有限公司 | Rare earth extraction groove device |
| CN204959010U (en) * | 2015-09-24 | 2016-01-13 | 深圳市汇丰泰机电设备有限公司 | Noble metal electroplating effluent enriching recovery equipment |
| CN205473922U (en) * | 2016-03-07 | 2016-08-17 | 赣州齐飞新材料有限公司 | High -efficient rare earth extraction splitter |
| CN205516618U (en) * | 2016-03-07 | 2016-08-31 | 广东华科检测技术服务有限公司 | Automatic extraction apparatus |
| CN205774721U (en) * | 2016-05-12 | 2016-12-07 | 赣州齐飞新材料有限公司 | A kind of energy-conservation rare earth extraction slot device |
| CN205672854U (en) * | 2016-05-27 | 2016-11-09 | 栾景臻 | A kind of chemical experiment material mixing device |
| CN205760921U (en) * | 2016-06-23 | 2016-12-07 | 信丰县包钢新利稀土有限责任公司 | A rare earth high-efficiency batching device |
-
2016
- 2016-12-18 CN CN201810082807.2A patent/CN108559839A/en not_active Withdrawn
- 2016-12-18 CN CN201810302798.3A patent/CN108396140A/en not_active Withdrawn
- 2016-12-18 CN CN201810083422.8A patent/CN108588421A/en not_active Withdrawn
- 2016-12-18 CN CN201810302792.6A patent/CN108559847A/en not_active Withdrawn
- 2016-12-18 CN CN201810083344.1A patent/CN108251641A/en not_active Withdrawn
- 2016-12-18 CN CN201810083360.0A patent/CN108559840A/en not_active Withdrawn
- 2016-12-18 CN CN201611173247.9A patent/CN106521149A/en active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| CN108396140A (en) | 2018-08-14 |
| CN108588421A (en) | 2018-09-28 |
| CN108559847A (en) | 2018-09-21 |
| CN106521149A (en) | 2017-03-22 |
| CN108559840A (en) | 2018-09-21 |
| CN108251641A (en) | 2018-07-06 |
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Application publication date: 20180921 |