CN105725263A - Preparation method of grape-flavor electronic cigarette liquid - Google Patents
Preparation method of grape-flavor electronic cigarette liquid Download PDFInfo
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- CN105725263A CN105725263A CN201610163472.8A CN201610163472A CN105725263A CN 105725263 A CN105725263 A CN 105725263A CN 201610163472 A CN201610163472 A CN 201610163472A CN 105725263 A CN105725263 A CN 105725263A
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- cigarette liquid
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- 239000007788 liquid Substances 0.000 title claims abstract description 48
- 239000003571 electronic cigarette Substances 0.000 title claims abstract description 42
- 239000000796 flavoring agent Substances 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 51
- 241000219095 Vitis Species 0.000 claims abstract description 49
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 27
- 235000009754 Vitis X bourquina Nutrition 0.000 claims abstract description 23
- 235000012333 Vitis X labruscana Nutrition 0.000 claims abstract description 23
- 235000014787 Vitis vinifera Nutrition 0.000 claims abstract description 23
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 claims abstract description 16
- 235000019674 grape juice Nutrition 0.000 claims abstract description 14
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 claims abstract description 10
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000000811 xylitol Substances 0.000 claims abstract description 10
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 claims abstract description 10
- 229960002675 xylitol Drugs 0.000 claims abstract description 10
- 235000010447 xylitol Nutrition 0.000 claims abstract description 10
- 238000001704 evaporation Methods 0.000 claims abstract description 8
- 235000009392 Vitis Nutrition 0.000 claims description 26
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 21
- 235000019634 flavors Nutrition 0.000 claims description 19
- ZCHHRLHTBGRGOT-SNAWJCMRSA-N (E)-hex-2-en-1-ol Chemical compound CCC\C=C\CO ZCHHRLHTBGRGOT-SNAWJCMRSA-N 0.000 claims description 14
- XPCTZQVDEJYUGT-UHFFFAOYSA-N 3-hydroxy-2-methyl-4-pyrone Chemical compound CC=1OC=CC(=O)C=1O XPCTZQVDEJYUGT-UHFFFAOYSA-N 0.000 claims description 14
- MLFHJEHSLIIPHL-UHFFFAOYSA-N isoamyl acetate Chemical compound CC(C)CCOC(C)=O MLFHJEHSLIIPHL-UHFFFAOYSA-N 0.000 claims description 14
- GVOWHGSUZUUUDR-UHFFFAOYSA-N methyl N-methylanthranilate Chemical compound CNC1=CC=CC=C1C(=O)OC GVOWHGSUZUUUDR-UHFFFAOYSA-N 0.000 claims description 14
- VAMXMNNIEUEQDV-UHFFFAOYSA-N methyl anthranilate Chemical compound COC(=O)C1=CC=CC=C1N VAMXMNNIEUEQDV-UHFFFAOYSA-N 0.000 claims description 14
- QPRQEDXDYOZYLA-UHFFFAOYSA-N 2-methylbutan-1-ol Chemical compound CCC(C)CO QPRQEDXDYOZYLA-UHFFFAOYSA-N 0.000 claims description 13
- 241000219094 Vitaceae Species 0.000 claims description 13
- 235000021021 grapes Nutrition 0.000 claims description 13
- HCRBXQFHJMCTLF-ZCFIWIBFSA-N ethyl (2r)-2-methylbutanoate Chemical compound CCOC(=O)[C@H](C)CC HCRBXQFHJMCTLF-ZCFIWIBFSA-N 0.000 claims description 12
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 claims description 8
- 239000003921 oil Substances 0.000 claims description 8
- 235000019198 oils Nutrition 0.000 claims description 8
- 229940058015 1,3-butylene glycol Drugs 0.000 claims description 7
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 claims description 7
- WTEVQBCEXWBHNA-UHFFFAOYSA-N Citral Natural products CC(C)=CCCC(C)=CC=O WTEVQBCEXWBHNA-UHFFFAOYSA-N 0.000 claims description 7
- HYMLWHLQFGRFIY-UHFFFAOYSA-N Maltol Natural products CC1OC=CC(=O)C1=O HYMLWHLQFGRFIY-UHFFFAOYSA-N 0.000 claims description 7
- 150000001298 alcohols Chemical class 0.000 claims description 7
- 235000019437 butane-1,3-diol Nutrition 0.000 claims description 7
- 229940043350 citral Drugs 0.000 claims description 7
- 235000020057 cognac Nutrition 0.000 claims description 7
- 230000008020 evaporation Effects 0.000 claims description 7
- WTEVQBCEXWBHNA-JXMROGBWSA-N geranial Chemical compound CC(C)=CCC\C(C)=C\C=O WTEVQBCEXWBHNA-JXMROGBWSA-N 0.000 claims description 7
- 229940117955 isoamyl acetate Drugs 0.000 claims description 7
- 229940043353 maltol Drugs 0.000 claims description 7
- 150000003505 terpenes Chemical class 0.000 claims description 7
- 235000007586 terpenes Nutrition 0.000 claims description 7
- 235000019501 Lemon oil Nutrition 0.000 claims description 6
- 230000006837 decompression Effects 0.000 claims description 6
- 239000001813 ethyl (2R)-2-methylbutanoate Substances 0.000 claims description 6
- 229940090910 ethyl 2-methylbutyrate Drugs 0.000 claims description 6
- 239000010501 lemon oil Substances 0.000 claims description 6
- 238000002390 rotary evaporation Methods 0.000 claims description 5
- 125000004494 ethyl ester group Chemical group 0.000 claims description 4
- 238000005360 mashing Methods 0.000 claims description 4
- 235000009508 confectionery Nutrition 0.000 abstract description 8
- 239000012141 concentrate Substances 0.000 abstract description 3
- 230000000391 smoking effect Effects 0.000 abstract description 2
- 239000000243 solution Substances 0.000 description 8
- 235000019504 cigarettes Nutrition 0.000 description 6
- OBNCKNCVKJNDBV-UHFFFAOYSA-N ethyl butyrate Chemical compound CCCC(=O)OCC OBNCKNCVKJNDBV-UHFFFAOYSA-N 0.000 description 6
- 239000003205 fragrance Substances 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 4
- 239000003546 flue gas Substances 0.000 description 4
- 235000019640 taste Nutrition 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 244000061176 Nicotiana tabacum Species 0.000 description 3
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 3
- 230000035807 sensation Effects 0.000 description 2
- 235000019615 sensations Nutrition 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 244000299461 Theobroma cacao Species 0.000 description 1
- 235000009470 Theobroma cacao Nutrition 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- XYIBRDXRRQCHLP-UHFFFAOYSA-N ethyl acetoacetate Chemical compound CCOC(=O)CC(C)=O XYIBRDXRRQCHLP-UHFFFAOYSA-N 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 229960005150 glycerol Drugs 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 229960004063 propylene glycol Drugs 0.000 description 1
- 235000013772 propylene glycol Nutrition 0.000 description 1
- 238000013441 quality evaluation Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
- C11B9/0034—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing six carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0069—Heterocyclic compounds
- C11B9/0073—Heterocyclic compounds containing only O or S as heteroatoms
- C11B9/008—Heterocyclic compounds containing only O or S as heteroatoms the hetero rings containing six atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Seasonings (AREA)
Abstract
The invention provides a preparation method of grape-flavor electronic cigarette liquid. The grape-flavor electronic cigarette liquid is obtained by uniformly mixing, by weight, 1-80 parts of propylene glycol, 1-60 parts of glycerol, 1-50 parts of 1,3-butanediol, 1-30 parts of xylitol liquid, 5-10 parts of grape juice concentrate, 0.1-2 parts of edible grape essence and the like in proportion, wherein the grape juice concentrate is obtained through squeezing and extracting and reduced-pressure rotary evaporating and concentrating. The electronic cigarette liquid has the better grape aroma and the fresh and sweet mouthfeel and can meet the smoking requirement of consumers on fruity electronic cigarettes.
Description
Technical field
The invention belongs to flavouring essence for tobacco field, relate to a kind of electronic cigarette liquid and preparation method thereof, particularly relate to a kind of Portugal
Electronic cigarette liquid of grape local flavor and preparation method thereof.
Background technology
Electronic cigarette has another name called electronic cigarette, has the outward appearance similar to Medicated cigarette and the taste of medicated cigarette approximation, the same also like Medicated cigarette
Energy sucking-off cigarette, sucking-off taste and sensation are come.Electronic cigarette does not has other harmful components such as the tar in Medicated cigarette, suspended particulates, the most several
Do not produce second hand smoking.
The fragrance of electronic cigarette and mouthfeel derive from electronic cigarette liquid, and the composition of electronic cigarette liquid is mainly essence and flavoring agent, and Nicotiana tabacum L. carries
Take thing and propylene glycol, glycerol equal solvent.In order to cater to the consumption habit of consumer's diversification, during the electronic cigarette on market has
The brand cigarette tastes such as China, Yuxi, also have the non-tobacco tastes such as Herba Menthae, cocoa, Rhizoma et radix valerianae.At present, the fruity without nicotine
Electronic cigarette is quite welcome by consumer with its pure and fresh sweet mouthfeel.
Summary of the invention
Solve the technical problem that: fruity electronic cigarette mainly brings sense by its pure and fresh sweet mouthfeel to consumer
Pleasurable sensation on official, but the mouthfeel of fruity electronic cigarette in the market is universal sweet greasy, and pleasant impression is the cleanest, it is impossible to meets and disappears
The requirement of sense of the person of expense.
Technical scheme: for above-mentioned technical problem, the invention discloses the electronic cigarette liquid of a kind of grape flavor, described Portugal
The electronic cigarette liquid of grape local flavor consists of the following composition: propylene glycol, glycerol, 1,3 butylene glycol, xylitol liquid, Sucus Vitis viniferae concentrated solution and
Table grapes essence.
Preferably, in the electronic cigarette liquid of described a kind of grape flavor, the parts by weight of each component are: propylene glycol is 1-80
Part, glycerol be 1-60 part, 1,3 butylene glycol be 1-50 part, xylitol liquid be 1-30 part, Sucus Vitis viniferae concentrated solution be 5-10 part, edible
Grape essence is 0.1-2 part.
Preferably, the electronic cigarette liquid of described a kind of grape flavor is sundown.
Preferably, the electronic cigarette liquid of described a kind of grape flavor, described table grapes essence is composed of the following components:
Methyl 2-aminobenzoate, N-methyl anthranilic acid methyl ester, ethyl acetate, ethyl n-butyrate., isoamyl acetate, 2-methyl fourth
Acetoacetic ester, maltol, 2-methyl butanol, phenethanol, trans-2-hexenol, citral, Alcohols,fusel, white lemon oil, oranger terpene,
Cognac green oil and propylene glycol.
Preferably, the electronic cigarette liquid of described a kind of grape flavor, the weight of each component in described table grapes essence
Number is: methyl 2-aminobenzoate be 3-6 part, N-methyl anthranilic acid methyl ester be 2-7 part, ethyl acetate be 1-5 part,
Ethyl n-butyrate. be 0.1-1 part, isoamyl acetate be 0.1-1 part, ethyl 2-methylbutyrate be 0.1-1 part, maltol be 0.1-1
Part, 2-methyl butanol be 1-5 part, phenethanol be 0.1-1 part, trans-2-hexenol be 0.01-1 part, citral be 0.01-1 part,
Alcohols,fusel be 1-5 part, white lemon oil be 0.1-1 part, oranger terpene be 0.1-1 part, cognac green oil be 0.1-1 part, propylene glycol
For 70-90 part.
Preferably, the electronic cigarette liquid of described a kind of grape flavor, described Sucus Vitis viniferae concentrated solution is that Fructus Vitis viniferae squeezing is extracted
After the Sucus Vitis viniferae concentrated solution that is concentrated to give.
Preferably, described Sucus Vitis viniferae concentrated solution preparation method comprises the following steps: (1) weighs clean Fructus Vitis viniferae, uses group
Knit bruisher to smash to pieces；(2) carry out squeezing with small-sized basket squeezer and obtain original grape juice；(3) original grape juice decompression is rotated
Evaporation and concentration becomes thick liquid, standby.
Preferably, the temperature that the rotary evaporation that reduces pressure in the preparation method of described Sucus Vitis viniferae concentrated solution concentrates is 50 DEG C, very
Reciprocal of duty cycle is 0.095 Mpa, and the Baume degrees of final gained Sucus Vitis viniferae concentrated solution is at 50-55 ° of Bx.
The preparation method of the electronic cigarette liquid of a kind of grape flavor, comprises the steps: that (1) weighs clean Fructus Vitis viniferae, uses group
Knit bruisher to smash to pieces；(2) carry out squeezing with small-sized basket squeezer and obtain original grape juice；(3) original grape juice decompression is rotated
Evaporation and concentration becomes thick liquid, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095 Mpa, is concentrated into Baume degrees and reaches 50-
After 55 ° of Bx standby；(4) methyl 2-aminobenzoate 3-6 part, N-methyl anthranilic acid methyl ester 2-7 part, ethyl acetate 1-are taken
5 parts, ethyl n-butyrate. 0.1-1 part, isoamyl acetate 0.1-1 part, ethyl 2-methylbutyrate 0.1-1 part, maltol 0.1-1 part, 2-
Methyl butanol 1-5 part, phenethanol 0.1-1 part, trans-2-hexenol 0.01-1 part, citral 0.01-1 part, Alcohols,fusel 1-5 part, white
Fructus Citri Limoniae oil 0.1-1 part, oranger terpene 0.1-1 part, cognac green oil 0.1-1 part, propylene glycol 70-90 part, mix mentioned component
After obtain table grapes essence；(5) propylene glycol 1-80 part, glycerol 1-60 part, 1,3 butylene glycol 1-50 part, xylitol liquid 1-30 are taken
Part, Sucus Vitis viniferae concentrated solution 5-10 part, Fructus Vitis viniferae edible essence 0.1-2 part, prepare grape flavor after being mixed by mentioned component
Electronic cigarette liquid.
The described xylitol aqueous solution that xylitol liquid is 20wt% to 50wt%.
Beneficial effect: the electronic cigarette liquid of the grape flavor prepared by the preparation method of the present invention is sundown,
Overcome fruity electronic cigarette mouthfeel universal sweet greasy, pleasant impression is the cleanest, it is impossible to the shortcoming meeting consumer sensory's demand, the present invention
Electronic cigarette liquid suction time be provided that fresh and sweet Fructus Vitis viniferae fragrance, mouthfeel is soft and moist and pleasant impression is the most comfortable, and described electronic cigarette
The preparation method of liquid is easy, and constant product quality can be widely applied in electronic cigarette product.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further described.
Embodiment 1
(1) weigh clean Fructus Vitis viniferae, smash to pieces with tissue mashing machine；Carry out squeezing with small-sized basket squeezer and obtain original grape juice；
Original grape juice decompression rotary evaporation is condensed into thick liquid, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095
Mpa, is concentrated into after Baume degrees reaches 50-55 ° of Bx standby；
(2) methyl 2-aminobenzoate 4 parts, N-methyl anthranilic acid methyl ester 5 parts, ethyl acetate 2 parts, butanoic acid are taken by weight
Ethyl ester 0.4 part, isoamyl acetate 0.5 part, ethyl 2-methylbutyrate 0.5 part, maltol 0.6 part, 2-methyl butanol 1 part, benzene second
Alcohol 0.1 part, trans-2-hexenol 0.05 part, citral 0.01 part, Alcohols,fusel 1 part, white lemon oil 0.1 part, oranger terpene 0.1 part,
Cognac green oil 0.1 part, propylene glycol 80 parts, obtain table grapes essence after being mixed by mentioned component；
(3) propylene glycol 50 parts, glycerol 20 parts, 1,3 butylene glycol 10 parts, the xylitol liquid 5 parts of 20wt%, Sucus Vitis viniferae are taken by weight dense
Contracting liquid 9.5 parts, 0.5 part of mix homogeneously of table grapes essence, obtain the electronic cigarette liquid of grape flavor.
Embodiment 2
(1) weigh clean Fructus Vitis viniferae, smash to pieces with tissue mashing machine；Carry out squeezing with small-sized basket squeezer and obtain original grape juice；
Original grape juice decompression rotary evaporation is condensed into thick liquid, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095
Mpa, is concentrated into after Baume degrees reaches 50-55 ° of Bx standby；
(2) methyl 2-aminobenzoate 3 parts, N-methyl anthranilic acid methyl ester 7 parts, ethyl acetate 5 parts, butanoic acid are taken by weight
Ethyl ester 0.1 part, isoamyl acetate 0.1 part, ethyl 2-methylbutyrate 0.1 part, maltol 0.1 part, 2-methyl butanol 2.5 parts, benzene
Ethanol 0.5 part, trans-2-hexenol 0.01 part, citral 0.03 part, Alcohols,fusel 2 parts, white lemon oil 0.4 part, oranger terpene 0.2
Part, cognac green oil 0.5 part, propylene glycol 70 parts, obtain table grapes essence after being mixed by mentioned component；
(3) propylene glycol 80 parts, glycerol 1 part, 1,3 butylene glycol 1 part, the xylitol liquid 30 parts of 40wt%, Sucus Vitis viniferae are taken by weight dense
Contracting liquid 10 parts, 0.1 part of mix homogeneously of table grapes essence, obtain the electronic cigarette liquid of grape flavor.
Embodiment 3
(1) weigh clean Fructus Vitis viniferae, smash to pieces with tissue mashing machine；Carry out squeezing with small-sized basket squeezer and obtain original grape juice；
Original grape juice decompression rotary evaporation is condensed into thick liquid, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095
Mpa, is concentrated into after Baume degrees reaches 50-55 ° of Bx standby；
(2) methyl 2-aminobenzoate 6 parts, N-methyl anthranilic acid methyl ester 2 parts, ethyl acetate 1 part, butanoic acid are taken by weight
Ethyl ester 1 part, isoamyl acetate 1 part, ethyl 2-methylbutyrate 1 part, maltol 1 part, 2-methyl butanol 5 parts, phenethanol 1 part, trans-
2-hexenol 1 part, citral 1 part, Alcohols,fusel 5 parts, white lemon oil 1 part, oranger terpene 1 part, cognac green oil 1 part, propylene glycol
90 parts, after being mixed by mentioned component, obtain table grapes essence；
(3) propylene glycol 1 part, glycerol 60 parts, 1,3 butylene glycol 50 parts, the xylitol liquid 1 part of 50wt%, Sucus Vitis viniferae are taken by weight dense
Contracting liquid 5 parts, 2 parts of mix homogeneously of table grapes essence, obtain the electronic cigarette liquid of grape flavor.
The embodiment 1 prepared, embodiment 2, the grape flavor electronic cigarette liquid of embodiment 3 are taken 0.5mL and add to electricity
In sub-cigarette, and separately take after commercially available table grapes essence propylene glycol is diluted to 0.3wt%, take the commercially available edible Portugal of 0.3wt% of 0.5mL
Grape essence diluent adds to electronic cigarette, as a comparison case, carries out integrated sensory's quality evaluation.Result is as follows:
Embodiment 1: flue gas is full, Fructus Vitis viniferae gives off a strong fragrance, mouthfeel is soft, pleasant impression is comfortable.
Embodiment 2: exquisiteness that flue gas is strong, Fructus Vitis viniferae fragrance is soft and moist, mouthfeel is fresh and sweet, pleasant impression are clean.
Embodiment 3: flue gas is strong, Fructus Vitis viniferae soft aroma and, delicate mouthfeel, pleasant impression clean.
Comparative example: flue gas is strong, Fructus Vitis viniferae fragrance coordinate, mouthfeel sweet greasy, pleasant impression is not good enough.
Can be seen that from result, the electronic cigarette liquid of the grape flavor prepared by the preparation method of the present invention is had clearly
Sweet Fructus Vitis viniferae fragrance, mouthfeel is soft and moist and pleasant impression is the most comfortable, and the preparation method of described electronic cigarette liquid is easy, and product quality is steady
Fixed, can be widely applied in electronic cigarette product.
Claims (1)
1. the preparation method of the electronic cigarette liquid of a grape flavor, it is characterised in that comprise the steps:
(1) weigh clean Fructus Vitis viniferae, smash to pieces with tissue mashing machine；Carry out squeezing with small-sized basket squeezer and obtain original grape juice；
Original grape juice decompression rotary evaporation is condensed into thick liquid, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095
Mpa, is concentrated into after Baume degrees reaches 50-55 ° of Bx standby；
(2) methyl 2-aminobenzoate 6 parts, N-methyl anthranilic acid methyl ester 2 parts, ethyl acetate 1 part, butanoic acid are taken by weight
Ethyl ester 1 part, isoamyl acetate 1 part, ethyl 2-methylbutyrate 1 part, maltol 1 part, 2-methyl butanol 5 parts, phenethanol 1 part, trans-
2-hexenol 1 part, citral 1 part, Alcohols,fusel 5 parts, white lemon oil 1 part, oranger terpene 1 part, cognac green oil 1 part, propylene glycol
90 parts, after being mixed by mentioned component, obtain table grapes essence；
(3) propylene glycol 1 part, glycerol 60 parts, 1,3 butylene glycol 50 parts, the xylitol liquid 1 part of 50wt%, Sucus Vitis viniferae are taken by weight dense
Contracting liquid 5 parts, 2 parts of mix homogeneously of table grapes essence, obtain the electronic cigarette liquid of grape flavor.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610163472.8A CN105725263A (en) | 2014-07-28 | 2014-07-28 | Preparation method of grape-flavor electronic cigarette liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610163472.8A CN105725263A (en) | 2014-07-28 | 2014-07-28 | Preparation method of grape-flavor electronic cigarette liquid |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410360460.5A Division CN104087415B (en) | 2014-07-28 | 2014-07-28 | A grape-flavored electronic cigarette liquid and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105725263A true CN105725263A (en) | 2016-07-06 |
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| CN201610163472.8A Pending CN105725263A (en) | 2014-07-28 | 2014-07-28 | Preparation method of grape-flavor electronic cigarette liquid |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2004041007A2 (en) * | 2002-10-31 | 2004-05-21 | Philip Morris Products S.A. | Electrically heated cigarette including controlled-release flavoring |
| US20100300466A1 (en) * | 2008-11-30 | 2010-12-02 | Mckamy Collin | Smoking Accessory |
| CN103436362A (en) * | 2013-08-16 | 2013-12-11 | 德利宝(广州)香料有限公司 | Essence with natural grape extract and preparation method of toothpaste |
| CN103622161A (en) * | 2013-11-28 | 2014-03-12 | 刘秋明 | Electronic cigarette tobacco juice solvent and electronic cigarette tobacco juice |
| CN103932383A (en) * | 2014-05-12 | 2014-07-23 | 华健 | Electronic mouth cavity atomized liquid using multi-element ethanediol series lower alcohols as base solution |
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2014
- 2014-07-28 CN CN201610163472.8A patent/CN105725263A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2004041007A2 (en) * | 2002-10-31 | 2004-05-21 | Philip Morris Products S.A. | Electrically heated cigarette including controlled-release flavoring |
| US20100300466A1 (en) * | 2008-11-30 | 2010-12-02 | Mckamy Collin | Smoking Accessory |
| CN103436362A (en) * | 2013-08-16 | 2013-12-11 | 德利宝(广州)香料有限公司 | Essence with natural grape extract and preparation method of toothpaste |
| CN103622161A (en) * | 2013-11-28 | 2014-03-12 | 刘秋明 | Electronic cigarette tobacco juice solvent and electronic cigarette tobacco juice |
| CN103932383A (en) * | 2014-05-12 | 2014-07-23 | 华健 | Electronic mouth cavity atomized liquid using multi-element ethanediol series lower alcohols as base solution |
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Application publication date: 20160706 |